一种制备活性氧化铝的新方法

将结晶氯化铝与柠檬酸及淀粉等造孔剂混合,经直接干燥和焙烧制得了一种无定形活性氧化铝,并通过X射线粉末衍射、N2物理吸附及氨程序升温脱附等手段对活性氧化铝样品进行了表征,探讨了各组分对活性氧化铝样品性质所起的作用.与常规的活性氧化铝制备方法相比,这种制法省去了中和、老化、过滤和洗涤等步骤,缩短制备周期且过程容易控制.活性氧化铝具有适宜且可调节的比表面积和孔径分布,作为载体负载镍金属组分制成负载型催化剂后,对乙苯加氢饱和与加氢裂化表现出较高的催化活性.     

γ射线辐照人类正常肝细胞染色体损伤的动态修复

应用早熟染色体凝集技术对人类正常肝脏细胞经γ射线照射导致的染色体损伤后48h内的动态修复过程进行了研究。结果显示:照射后原初染色单体断裂和等点染色单体断裂数随着照射剂量的增加而增多，染色单体断裂显著多于等点染色单体断裂；经过24h的继续培养，这两种类型的损伤都有不同程度的修复，约50％染色单体断裂得到修复，而等点染色单体断裂的修复率最多为15％；经过48h的照射后培养，染色体损伤的水平与24h相比没有显著差异。说明肝细胞经γ射线照射后染色体损伤的主要形式是染色单体断裂，易于修复；虽然等点染色单体断裂数量较少，但修复困难。由此表明，等点染色体断裂是细胞经γ射线照射后死亡和癌变的一个重要因素。We employed the prematurely chromosome condensation （PCC） technique to investigate the 48 h kinetic repair of normal human liver cell line L02 exposed to γ-rays. The results showed that chromatidtype and isochromatid-type breaks increased with the dose at 0 h measured by PCC, the number of chromatid-type breaks was several times more than that of isochromatid-type breaks. Further 24 h incubationafter exposed to irradiation, both of these two type breaks decreased in different extent, 50% for chromatid-type one, change of the the main type easy to repair. 15% for isochromatid-type one at most, respectively. chromosome breaks compared with that of 24th h（p〉 0. 05 of the chromosome breaks was chromatid-type after exposed 48th h, there was a slightly ）. These results revealed that to low LET rays, also, it was Though the isochromatid-type breaks was obvioously less than that of the chromatid-type one, it was difficult to repair. It implied that the isochromatid-type breaks was the important factor causing cell death and canceration when cells were exposed to irradiations.     

高功率激光的三倍频高效转换实验

利用两块φ８０ｍｍ×１４ｍｍＫＤＰ晶体，采用“偏振失配”方案在“星光”装置φ７０输出光路上，进行了三倍频实验。在入射光功率密度约为１ＧＷ／ｃｍ￣２时，获得最高的二倍频外部能量转换效率为７６．９％，三倍频最高外部能量转换效率为６６．８％，并且转换重复性和稳定性很好。同时，也通过实验研究了影响三次谐波转换的诸因素。     

结晶紫内酯开环机理的￣（13）CNMR研究

报道了结晶紫内酯开环机理研究。通过测定开环前后及平衡混合物的￣（１３）ＣＮＭＲ谱，对结晶紫内酯开环形成的正碳离子结构及影响正碳离子稳定性因素进行了分析。利用开环前后及平衡体系的化学位移数据求得了平衡混合物中内酯态和正碳离子之间的平衡常数．对不同条件下结晶紫内酯开、闭环机制进行了讨论。     

介子波函数中非微扰效应的一个讨论

本文应用背景场方法计算了与介子分布振幅矩相关的两点关联函数的算符乘积展开. 其结果表明非微扰效应大小依赖于介子的自旋和夸克质量.     

A MBE ON-LINE OPTICAL MODULATION PHOTOREFLECTANCE ANALYSIS SYSTEM

An on-line optical modulation photoreflectance (PR) spectroscopy analysis system asso-cinted with the molecular beam epitaxy (MBE) system has been designed and established. This paper reports in detail the optical design, the experimental arrangement, and the adjust-ment of the system. GaAs film samples grown by MBE on Si-substrate have been measured with this on-line system. The results show that the on-line PR spectroscopy can characterize the quality of the as-grown film samples qualitatively and promptly.     

柯召、孙琦—单墫定理的拓广

一、引言人们容易证明任意3个整数中必有两个整数之和为2整除,任意5个整数中必有3个整数之和为3整除,柯老和孙琦教授在[1]中证明了任意7个整数中必有4个整数之和为4整除,并猜测任意2n-1(n>1)个整数中必有n个整数之和能为n整除。1983年单墫     

吉林市192名健康小儿血清锌的含量

本文用原子吸收法对吉林市192名2～6岁健康小儿血清锌的含量进行了测定。结果表明,女童血清锌值稍高于男童,且有随其年龄的增加而量值逐渐增加的规律。提出其正常值范围。建议小儿血清锌值在0.528mg/L以下者应补充锌剂,以促进其健康生长。     

基于角差法面形测量装置的测角误差研究

针对已有的角差法面形检测原理验证装置,分析采用相对测角法测量反射镜表面采样点的斜率并重构面形的测量方式中测角误差的传递方式。通过Matlab软件建立该传递方式的分析模型,并分析测角稳定性误差对面形测量的影响。实验证明该仿真分析的结果可靠有效。