高能飞秒激光系统中空间滤波器的研究和设计

 由于透镜传输时间延迟效应（PTD），飞秒激光脉冲经过空间滤波器产生脉冲波前变形。讨论了用双胶合透镜或双分离透镜代替空间滤波器中的单透镜，以消除或减小PTD效应，设计了适用于飞秒激光装置的空间滤波器。     

子空间上的对称正定及对称半正定阵的左右特征值反问题

文[1][2][3]中讨论AX＝B的对称阵逆特征值问题，文[4][5][6]中讨论了半正定阵的逆特征值问题。本文讨论了空间了子空间上的对称正定及对称半正定阵的左右特征值反问题，给出了解存在的充分条件及解的表达式。     

Structure Modification Function of g‐C3N4 for Al2O3 in the In Situ Hydrothermal Process for Enhanced Photocatalytic Activity

Heterojunctions of g‐C₃N₄/Al₂O₃ (g‐C₃N₄=graphitic carbon nitride) are constructed by an in situ one‐pot hydrothermal route based on the development of photoactive γ‐Al₂O₃ semiconductor with a mesoporous structure and a high surface area (188 m²g^?1) acting as electron acceptor. A structure modification function of g‐C₃N₄ for Al₂O₃ in the hydrothermal process is found, which can be attributed to the coordination between unoccupied orbitals of the Al ions and lone‐pair electrons of the N atoms. The as‐synthesized heterojunctions exhibit much higher photocatalytic activity than pure g‐C₃N₄. The hydrogen generation rate and the reaction rate constant for the degradation of methyl orange over 50 % g‐C₃N₄/Al₂O₃ under visible‐light irradiation (λ>420 nm) are 2.5 and 7.3 times, respectively, higher than those over pristine g‐C₃N₄. The enhanced activity of the heterojunctions is attributed to their large specific surface areas, their close contact, and the high interfacial areas between the components as well as their excellent adsorption performance, and efficient charge transfer ability.     

低阶C-Bézier曲线的升阶

C- Bézier曲线是在 Bézier曲线基础上作了改进 ,因此具有与 Bézier曲线类似的性质 .本文主要研究的是 C- Bézier曲线从 3阶到 4阶 ,4阶到 5阶 ,5阶到 6阶的升阶转换     

Effect of stability of internal standard on quantification of 15 flavonoids in Epimedium using CZE

A CZE method was developed for the simultaneous determination of 15 flavonoids, including epimedin B, epimedin A, hexandraside F, epimedin C, icariin, sagittatoside B, sagittatoside A, hexandraside E, 2′′‐O‐rhamnosyl icariside II, baohuoside VII, baohuoside I, caohuoside C, epimedoside C, baohuoside II, and kaempferol‐3‐O‐rhamnoside, in different species of Epimedium, and the effect of stability of internal standard (IS) on quantification was also investigated. As a result, rutin was not available for use as an IS because of its unstable property in sample solution, which suggested that the stability of IS both in standards and sample solution should be considered for the analysis. Using stable daidzein as IS, the analysis was performed within 35 min by using 50 mM borax buffer containing 20% ACN as a modifier (pH 10.0), while separation voltage was 25 kV and temperature was at 30°C. The method was validated to be accurate, simple, and repeatable, and was successfully applied to the analysis of 36 samples from 17 species of Epimedium.     

新型烷基醚型键合固定相的制备及评价

 首次将一种新型硅烷偶联剂 β (3,4 环氧环己基 )乙基三甲氧基硅烷 (β ECTS)与辛醇反应 ,然后再键合到硅胶上 ,得到了醚型键合固定相 ,并用元素分析、13 C固体核磁、红外光谱等对其进行了表征。以甲醇 水简单的二元流动相体系 ,对该固定相进行了色谱评价。结果表明 ,该固定相具有较好的色谱性能 ,且在 pH 2 5～ 7 5时化学稳定性能良好 ,硅醇基效应得到了很好地抑制 ,可有效地用于碱性化合物的分离分析     

蚕丝丝胶蛋白的结构、性能及利用

丝绸厂排放的废水中含有大量的丝胶蛋白。丝胶蛋白是一种球状蛋白,含有多种多肽,由18种氢基酸组成,含有较多的丝氨酸,天门冬氨酸和甘氨酸,极性侧链氨基酸占74．61％,丝胶蛋白具有易溶,吸水,凝胶化,可改性和抗氧化等特性,在化妆品,食品、医药和生物材料等方面具有良好的开发潜能。     

关于连接梁的最优衰减率问题

研究具有耗散结点的连接梁的最优指数衰减率问题,该系统由于能量的衰减而导致弯矩在结点处间断,我们的方法是证明系统的一组广义征元生成状态空间的Riesz基,从而证明最优指数衰减率可由系统的谱确定。     

合肥储存环相干谐波自由电子激光研究方法的改进

 根据简单的计算模型,导出辐射能量谱形状因子和相干谐波辐射表达式,用此表达式讨论了不对称光学速调管的相干谐波辐射;对于合肥储存环相干谐波自由电子激光,提出了一个不对称光学速调管相干谐波辐射的研究方案,并且作了详细的计算,结果表明在较高的电子束能量下,调整光学速调管和外激光参数,使辐射段波荡器的辐射基波与外激光的二次谐波共振,进行相干谐波产生实验,能获得10⁹量级相干加强因子。     

放电等离子体极紫外光源中的主脉冲电源

描述了Z箍缩放电等离子体极紫外光源系统中的主脉冲电源,给出了主电路拓扑结构,重点介绍了三级磁脉冲压缩网络,给出了关键参数的设计计算,并且介绍了新颖的末级磁脉冲压缩放电结构。实验结果显示:各级磁脉冲压缩效果达到设计指标,电源输出电压峰达30 kV,输出电流峰值大于40 kA,电流脉冲宽度200 ns,满足Z箍缩放电等离子极紫外光源对主脉冲的要求。