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61.
Experimental Techniques - In this study, aluminum metal matrix composites (Al-MMCs) reinforced with aluminum oxide (Al2O3) (5, 10, 15 wt%) were produced using the powder metallurgy (PM) process.... 相似文献
62.
Orhan Atakol Hasan Nazir Zehra Durmus Ingrid Svoboda Hartmut Fuess 《Analytical sciences》2002,18(4):493-494
63.
Coherent wave-wave coupling can produce radiation with a high efficiency. Recently, there has been a great deal of interest in the study of electro-magnetic wave generation in magnetized plasmas. We have investigated theoretically the effect of finite ion temperature on the parametric instability of an electro-static upperhybrid pump into an X-mode nonthermal radiation and low frequency ion waves in a two electron temperature plasma. The latter may include the lower-hybrid, the electron-acoustic and the ion-cyclotron waves. The loss cone distribution existing permanently at low altitudes acts as a free energy source generating the upper-hybrid waves. The upper-hybrid waves can also be present because of a linear instability produced by runaway electrons. Nonlinear dispersion relation and the growth rates are derived for each case using the hydrodynamical model. We find extra numerical factor arising due to the ions of finite temperature in the growth rate expression. This study may be useful in magnetosphere, auroral ionosphere, solar wind, solar radio bursts, and laboratory plasmas where ion has finite temperature and electrons have two distinct energy distributions. 相似文献
64.
In this study, an ammonia-gas-sensing liquid-state membrane electrode based on 1-[(2-oxyphenyl)iminomethyl]-2-oxybenzene-O,O',N-ammin-nickel(II) (Ni(II)-Schiff base) as an ionophore was developed. This membrane electrode gave a very good performance and exhibited linear response with near-Nernstian slope of 50.7+/-0.5 mV per decade, within a concentration range of 1.0x10(-1)-1.0x10(-3) M. The electrode performance depends on the pH of the test solution and the optimum pH range was 10.0-11.5. The effect of concentration of internal solutions in the electrode was also investigated. The selectivity properties of the electrode towards aliphatic amines at a pH value of 10.2 were investigated with the mixed-solution method. Furthermore, the response time and lifetime of the electrode prepared were determined. 相似文献
65.
Metal-Containing Phthalocyanines Substituted with One Branched Bulky Moiety and Six Alkylthio Groups
Zehra Altunta? Bay?r ?ebnur Merey Esin Hamuryudan 《Monatshefte für Chemie / Chemical Monthly》2003,400(3):1027-1031
Unsymmetrically substituted metal-phthalocyanines composed of three hexylthio groups and one 1-chloro-3,4-dicyano-6-[2-(2-pyridylmethylamino)phenylthio]benzene
moiety was prepared by cyclization of the reactants in the presence of the anhydrous metal salts Zn(CH3COO)2, NiCl2, and CoCl2. The new unsymmetric phthalocyanines are very soluble in common organic solvents. The compounds were characterised by their
elemental analyses, IR, 1H NMR, MS and UV/Vis spectra. 相似文献
66.
Sabira Begum SyedaQamar Zehra Aneela Wahab BinaShaheen Siddiqui 《Helvetica chimica acta》2006,89(9):1932-1941
Three new pentacyclic triterpenoids, camarin ( 1 ), lantacin ( 2 ), and camarinin ( 3 ) were isolated from the aerial parts of Lantana camara Linn ., together with seven known compounds. The structures of the new constituents were elucidated by chemical transformation, HR‐EI mass spectrometry, and NMR spectroscopy, including 1D (1H‐ and 13C‐NMR) and 2D (1H,1H‐COSY, NOESY, 1H,1H‐TOCSY, J‐resolved, HMQC, and HMBC) experiments. 相似文献
67.
Zeynep Gönül Dilara Altay Öztürk Fatümetüzzehra Küçükbay Suat Tekin Zehra Tekin Hasan Küçükbay 《Journal of heterocyclic chemistry》2023,60(1):86-95
In this study, 10 new indole-dipeptide conjugates were synthesized, and their anticancer activity was determined against on A2780 (ovarian cancer cell line) and MCF-7 (breast cancer cell line) cells. Among compounds, 5 and 10 showed better activity against A2780 cell lines than the standard drug docatexel at 0.1 and 1 μM concentrations, while only compound 5 showed better activity than docatexel, the MCF-7 cell line at 0.1 and 1 μM concentrations. The antioxidant potencies of the compounds were low in both the DPPH and iron reducing power methods tested when compared to standard antioxidants used in this work. 相似文献
68.
Two simple, sensitive and economical spectrophotometric methods have been developed for the determination of esomeprazole magnesium in commercial dosage forms. Method A is based on the reaction of esomeprazole magnesium with 5‐sulfosalicylic acid in methanol to form a yellow product, which absorbs maximally at 365 nm. Method B utilizes the reaction of esomeprazole magnesium with N‐bromosuccinimide in acetone‐chloroform medium to form α‐bromo derivative of the drug peaking at 380 nm. Under the optimized experimental conditions, Beer's law is obeyed in the concentration ranges of 2‐48 and 10‐100 μg mL?1 with molar absorptivity of 2.11 × 104 and 4.57 × 104L mol?1 cm?1 for methods A and B, respectively. The limits of detection for methods A and B are 0.35 and 0.46 μg mL?1, respectively. No interference was observed from excipients commonly present in tablet formulations. Methods A and B are successfully applied to the commercial tablets for the estimation of esomeprazole magnesium with good accuracy and precision. The results compare favorably with the reference spectrophotometric method indicating no significant difference between the methods compared. 相似文献
69.
Schwab KC Blencowe MP Roukes ML Cleland AN Girvin SM Milburn GJ Ekinci KL 《Physical review letters》2005,95(24):248901; author reply 248902
70.
Mediha Kök Şahin Ata Zehra Deniz Yakıncı Yıldırım Aydoğdu 《Journal of Thermal Analysis and Calorimetry》2018,133(2):845-850
In the present study, a ternary CuAl-based alloy was produced by adding 2% chromium, niobium, titanium and hafnium instead of 2% copper from the Cu88Al12 (% in mass) shape memory alloy, and the phase changes in the alloy were examined. As a result of the X-ray analyses performed at room temperature, the α phase, which is rich in copper, was detected in the main sample, i.e., the Cu88Al12 alloy, and the β 1 1 and γ 1 ? phases were detected in the four of the Cu86Al12Cr2, Cu86Al12Nb2, Cu86Al12Ti2 and Cu86Al12Hf2 alloys. All of phases were clearly seen in SEM images. As a result of the mapping performed during chemical analysis, it was observed clearly that there appeared a precipitation phase in the Cu86Al12Cr2, Cu86Al12Nb2, Cu86Al12Ti2 alloys due to the additions. It was also observed that the additions were effective in forming a martensite phase in the Cu88Al12 alloy. In differential scanning calorimetry (DSC) measurements, which were taken to support these measurements, no martensitic phase transformations were detected in dual primary alloy (Cu88Al12); however, a clear martensite phase transformation was detected in ternary alloys (Cu86Al12Cr2, Cu86Al12Nb2, Cu86Al12Ti2 and Cu86Al12Hf2) in the first DSC measurement. Then, when the DSC cycle was applied to the ternary alloy, both the austenite transformation and martensite transformation temperatures were clearly seen, and it was claimed that all the alloys showed high-temperature shape memory alloy properties. 相似文献