悬浮液进样-火焰原子吸收光谱法测定怀山药中铜

怀山药、怀地黄、怀牛膝、怀菊花合称"四大怀药",是享誉海内外的名贵中药材,其中怀山药作为药食同源的滋补佳品,近年来被作为食品原料和成品在市场广泛流通.作为食品,其中金属元素铜是必测项目.食品中铜的测定,普遍采用原子吸收光谱法,样品的预处理有干法(灰化)、湿法(加酸消化)及微波消化法,前两种方法消化时间长、操作环节多,被测元素丢失或被污染的机会多;后种方法溶样不完全,重现性易受影响.     

薄层层析-光度法联用测定甲基对硫膦中o,o'-二甲基-对硝基苯基硫代膦酸酯

应用薄层色谱法(TLC)使对硫膦中的主成分,o,o'-二甲基-对硝基苯基硫代膦酸酯(DMNPTP),与以杂质共存的二硝基与邻硝基衍生物分离.TLC法中用硅胶(G254)作吸附剂,用石油醚与乙酸乙酯(8 2)的混合物作为展开溶剂,经TCL分离后,用刀片将样品(含DMNPTP)的色谱带括下,经蒸发除去有机溶剂,用硝酸-高氯酸加热消化并蒸发至干后,用硝酸溶解残渣.此时,溶液中原来以DMNPTP存在的化合物已转化为正磷酸盐,随即用磷钒钼杂多酸光度法测定其磷含量,测定波长为其吸收峰450 nm,由测定值换算为DMNPTP的含量.     

Distinguishable RGE Running Effects Between Dirac Neutrinos and Majorana Neutrinos with Vanishing Majorana CP-Violating Phases

In a novel parametrization of neutrino mixing and in the approximation of т-lepton dominance, we show that the one-loop renormalization-group equations (RGEs) of Dirac neutrinos are different from those of Majorana neutrinos even if two Majorana CP-violating phases vanish. As the latter can keep vanishing from the electroweak scale to the typical seesaw scale, it makes sense to distinguish between the RGE running effects of neutrino mixing parameters in Dirac and Majorana cases. The differences are found to be quite large in the minimal supersymmetric standard model with sizable tanβ, provided the masses of three neutrinos are nearly degenerate or have an inverted hierarchy.     

蝙蝠喉部发声组织建模及发声机理*

建立蝙蝠发声组织模型对超声机理研究及在智能设备的应用具有重要意义。根据蝙蝠喉部发声组织结构特点,通过有限元方法构建了蝙蝠的3种不同发声组织模型,分析了尺寸、材料力学参数、组织结构和张力4个因素对发声组织特征频率的影响。结果表明,如果用人类声带,按比例缩小构建蝙蝠喉部组织模型,蝙蝠无法发出超声波。构建组织结构含甲状软骨和声带的半鼓状模型和只含声带的条状模型,两种模型的特征频率相近且在合理的参数域内均无法达到超声范围。而含膜条状模型的特征频率可以通过张力进行超声频率的调节,这与文献的实验结果一致。因此,可基于含膜条状模型对蝙蝠喉管发声组织进行建模及其发声机理研究。     

Syntheses,Structures and Photocatalytic Degradation Properties of Two Copper(Ⅱ)Coordination Polymers with Flexible Bis(imidazole)Ligand

Two copper(Ⅱ)coordination polymers{[Cu(bib)(nip)]·1.5H2O}n(1)and[Cu2(bib)(glu)2]n(2)(bib= 1,4-bis(2-methyl-imidazol-1-yl)butane,H2nip = 5-nitroisophthalic acid,...     

铜电路板缝腐蚀过程缝隙中pH、Cl-浓度分布的测量

根据铜电路板缝腐蚀特征,研制了阵列式Ag/AgCl、IrO2电极,设计缝隙腐蚀模拟装置,在0.5mol.L-1的NaCl溶液中分别同时原位检测电子线路板缝隙腐蚀过程,缝隙内的氯离子浓度分布、pH分布及其随时间的变化.研究表明,在电子线路板发生缝隙腐蚀的过程中,缝隙内部不同深度的Cl-及H+浓度逐渐增大,且随着与缝口距离的增大而增大,从而导致缝隙腐蚀不断向纵深方向发展.     

A DIFFUSIVE SVEIR EPIDEMIC MODEL WITH TIME DELAY AND GENERAL INCIDENCE

In this paper,we consider a delayed diffusive SVEIR model with general inci-dence.We first establish the threshold dynamics of this model.Using a Nonstandard Fi...     

Weak Graph Map Homotopy and Its Applications∗

The authors introduce a notion of a weak graph map homotopy (they call it M-homotopy), discuss its properties and applications. They prove that the weak graph map homotopy equivalence between graphs coincides with the graph homotopy equivalence defined by Yau et al in 2001. The difference between them is that the weak graph map homotopy transformation is defined in terms of maps, while the graph homotopy transformation is defined by means of combinatorial operations. They discuss its advantages over the graph homotopy transformation. As its applications, they investigate the mapping class group of a graph and the 1-order MP-homotopy group of a pointed simple graph. Moreover, they show that the 1-order MP-homotopy group of a pointed simple graph is invariant up to the weak graph map homotopy equivalence.     

复数星图与单路的多染色拉姆齐数

对给定的简单图$H_1,H_2,\ldots,H_c$, 我们将使完全图$K_n$的任意边分解$\{G_i\}^c_{i=1}$都存在至少一个$G_i$有子图同构于$H_i$的最小正整数$n$称为多染色拉姆齐数 $R(H_1,H_2,\ldots,$ $H_c)$. 对正整数$m,n_1,n_2,\ldots,n_c$, 令$\Sigma=\sum_{i=1}^{c}(n_i-1)$. 在文献中,我们已经获得了$R(K_{1,n_1},\ldots,K_{1,n_c},P_m)$ 的一些界和精确值.Wang推测若$\Sigma\not\equiv 0\pmod{m-1}$且$\Sigma+1\ge (m-3)^2$, 则有$R(K_{1,n_1},\ldots, K_{1,n_c}, P_m)=\Sigma+m-1.$ 本文中, 我们给出了一个新的下界并给出$R(K_{1,n_1},\ldots,K_{1,n_c},P_m)$在$m\leq\Sigma$, $\Sigma\equiv k\pmod{m-1}$且$2\leq k \leq m-2$情况下的部分精确值. 这些结果部分证实了Wang的猜想.     

埋地热油管道正常运行的数值模拟研究

对高凝原油管道输送的水力热力问题进行分析研究,掌握管线运行规律,保证管线安全经济运行有着重要意义.本文建立了埋地热油管道正常运行的数学模型,采用非结构化网格和有限容积法对该问题进行了研究,计算结果与实验测量值吻合良好.