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41.
Pinning effect of lead lanthanum titanate (PLT) ferroelectric thin films with excess PbO of 20 mol% has been studied for deposition on diffe rent substrates. Silicon, sapphire and quartz were used as substrates on which P t/Ti or LaNiO3 thin films were deposited as bottom electrodes. Electron probe analysis results showed that there was still a certain amount of excess Pb in PLT films after annealing at 550 ℃ for 1 h, and the amount of it was dependent on the substrate used. The distribution of excess Pb in the films was investig ated by Auger electron spectroscopy depth profile. It was shown that the substrates and the bottom electrodes had significant effects on the content and distrib ution of excess Pb in PLT films. The excess Pb and its accumulation at the inter face between the film and bottom electrode may act as pinning centers and have a pinning effect on domains, which can be observed by abnormal P-E hysteresis loops and abnormal C-V curves. The excess Pb content in the films and the accumulation of Pb at the interface were high in PLT films deposited on Pt/Ti/S i, and considerable pinning effect was observed. As LaNiO3 would absorb most part of the excess Pb in PLT films, the content of excess Pb in the films deposited on LaNiO3/Si was very low and the pinning effect was hardly observed. 相似文献
42.
Reduction of Dislocations in GaN Epilayer Grown on Si (111) Substrates using a GaN Intermedial Layer 下载免费PDF全文
GaN intermedial layers grown under different pressures are inserted between GaN epilayers and AIN/Si(111) substrates. In situ optical reflectivity measurements show that a transition from the three-dimensional (3D) mode to the 2I) one occurs during the GaN epilayer growth when a higher growth pressure is used during the preceding GaN intermedial layer growth, and an improvement of the crystalline quality of GaN epilayer will be made. Combining the in situ reflectivity and transmission electron microscopy (TEM) measurements, it is suggested that the lateral growth at the transition of growth mode is favourable for bending of dislocation lines, thus reducing the density of threading dislocations in the epilayer. 相似文献
43.
提出了一种非刚性点匹配的算法并把其运用于医学图像配准.该算法采用信号滤波的方法来获得点集间的匹配信息,并运用松弛标记法将各点邻域关系对模糊的匹配信息进行迭代获得明确的匹配关系.在此基础上,利用高斯径向基函数来描述点模式间的弹性形变,在基本的迭代框架下实现问题的求解.实验结果显示在形变程度为5%、出格点比率50%和噪声标准差为5%的情况下该算法的匹配误差能控制在0.13以下,表明了该算法的鲁棒性和有效性,较好地解决了医学非刚性形变的点匹配问题. 相似文献
44.
Effect of Molecular Weight on Liquid Crystal Photoalignment by Photosensitive Polyester Containing Thrifluoromethyl Moieties 下载免费PDF全文
We investigate the liquid-crystal (LC) alignment direction on photoalignment films formed from photosensitive polyester containing thrifluoromethyl moieties (PPDA) with various molecular weights by crossed polarized optical microscopy. It is found that LC alignment behaviour changes with molecular weight of PPDA. The LC alignment on PPDA irradiated films with the highest molecular weight is homogeneous, while those with low and intermediate molecular weights are homeotropic. However, surface morphologies show weak dependence on molecular weight. The surfaces are smooth and there is no clear morphological anisotropy on these aligned films observed by an atomic force microscope. The surface energies of the irradiated films are also measured by using an indirect contact-angle method where both surface energy and its polar component, increase with increasing molecular weight. Different polar surface energies can be considered as a main reason for different alignment characteristics. 相似文献
45.
半正二阶三点边值问题的解和正解 总被引:8,自引:0,他引:8
考察了非线性二阶三点边值问题的n个解和正解的存在性,其中允许非线性项有一个负的下界并且n是一个任意的自然数.主要结论表明该问题可以具有n个解或者正解,只要非线性项在某些有界集上的“高度”是适当的. 相似文献
46.
卡尔曼滤波法用于ICP-AES分析时,在白色噪音情况下能给出准确的分析结果,当试样的某些组分未知时,测量噪音将不是白色的,分析结果将不准确。本文提出了一种加权增量卡尔曼滤波法来解决这个问题。 相似文献
47.
The nanoparticles of a spirooxazine (SPO) and its photomerocyanine (PMC) were prepared through the reprecipitation method. Two distinct features were observed. One is that the decaying lifetime for PMC nanoparticles was 600 times of that for the dispersed molecules, and the other is that the fluorescence intensity of SPO nanoparticles was enhanced by 240 times of that of the dispersed monomer. 相似文献
48.
舒兰褐煤树脂组分中某些分离物的化学研究 总被引:3,自引:0,他引:3
我国褐煤资源丰富 ,分布于云南、吉林、黑龙江、山东和内蒙古等地。褐煤除作燃料和腐植肥料外 ,还应用于轻化工和机械工业 ,如从褐煤制取褐煤蜡。褐煤蜡中含有较多的树脂物质 ,影响了褐煤蜡的质量 ,因此通常褐煤蜡树脂作为废弃物脱除 ,以提高褐煤蜡的质量。褐煤蜡的化学组成为纯蜡和树脂 ,前者为高碳脂肪酸和脂肪醇的酯类、游离脂肪酸和脂肪醇 ,以及烃类物等 ;后者则以萜类为主 ,并含有甾醇、羟基酸和烃化合物[1~ 5] 。 1982年唐运千等采用红外光谱和氢核磁共振谱检定 ,褐煤树脂中含有 β 谷甾醇 ;柱层析和薄层层析检出雌二醇和雌酚酮[2 ] … 相似文献
49.
Xi Kui WANG* Guan Hong CHEN Zhong Yan YAO College of Chemistry Environmental Science University of Jinan Jinan 《中国化学快报》2003,14(2):205-208
Ultrasonic waves in a liquid induce the formation of cavitation bubbles. Submitted to an oscillating pressure field, cavities filled with vapor and dissolved gas pulsate, grow and implode violently when they reach a critical resonant size. According to the 慼ot spot?theory, extremely high temperature and pressure are produced during the collapse of cavitation bubbles1. Under these extreme conditions, the molecules vaporized in the bubbles as well as in the surrounding condensed layer could … 相似文献
50.
AnOscillationConditionforanElectrode-separatedPiezoelectricSensorinNon-electrolyteLiquidSHENDa-zhong,HUANGMing-shan,LINSong,N... 相似文献