优质立方六面体金刚石大单晶的生长研究

高温高压静压触媒法合成的金刚石单晶,往往呈现六八面体形貌,因为立方六面体单晶{100}面的生长区间相对较小.本研究利用高温高压温度梯度法,自制Fe-Ni合金触媒,通过对合成组装和工艺进行合理调整后,控制晶体在相对低温适合{100}面生长区域内生长,得到的晶体均呈现完整立方六面体形貌;同时为抑制包裹体和其他杂质的进入,人为的提高晶体的径向平铺生长速度,抑制其轴向生长速度.以在33 h内合成的优质立方六面体晶体为例,晶体最大方向尺寸达到7.3 mm,重1.2克拉,其径向生长速度达到0.22 mm/h,轴向生长速度仅为0.08 mm/h,增重速度为7.3 mg/h.     

Reflection and Refraction of Waves Across an Interface of Two-phase Flow

We investigate a hyperbolic system of one-dimensional isothermal fluid with liquid-vapor phase transition.The refraction-reflection phenomena are intensively analyzed when elementary waves travel across the two-phase interface.We apply the characteristic method and hodograph transform of Riemann to reduce the nonlinear PDEs to a concise form.Specially for the case of incident rarefaction wave,reduced linear equations are convenient to solve by Laplace transform.Then an integral formula in wave i...     

热处理温度对铜镍镀层的光谱性能的影响

采用电沉积法在镍表面制备铜镍镀层,并将该铜镍镀层在不同温度下进行热处理。分别用扫描电镜法(SEM)、能谱法(EDAX) 和X衍射法(XRD)等对热处理后的铜镍镀层进行表征,研究热处理温度对铜镍镀层的光谱性能的影响。用电镀的方法获得的铜镍镀层表面是由节瘤组成,热处理温度在25~600 ℃范围,随着热处理温度的升高,铜镍镀层表面的节瘤变小;热处理温度在600~900 ℃范围,随着热处理温度的升高,铜镍镀层表面的节瘤变小,铜镍镀层表面的节瘤间的分界线越不明显。热处理温度在25～900 ℃范围,随着热处理温度的升高,铜镍镀层中铜的含量减小,从82.52 at%减小到78.30 at%;镍的含量增加,从17.48 at%增加到21.70 at%。铜镍镀层为Cu_0.81Ni_0.19立方晶型结构,热处理温度在25～300 ℃范围,随着热处理温度的升高,Cu_0.81Ni_0.19的晶型结构更完整;热处理温度在600～900 ℃范围,铜镍镀层中可能有部分的Cu_0.81Ni_0.19立方晶型结构转变为Cu_3.8Ni立方晶型结构;随着热处理温度的升高,有利于Cu_3.8Ni(311)和Cu_0.81N_i0.19(311) 晶面的生长。     

Smooth Solution of Multi-dimensional Nonhomogeneous Conservation Law: Its Formula,and Necessary and Sufficient Blowup Criterion

In this paper, we are concerned with the necessary and sufficient condition of the global existence of smooth solutions of the Cauchy problem of the multi-dimensional scalar conservation law with source-term,where the initial data lies in W1,∞(Rn) ∩ C1(Rn). We obtain the solution formula for smooth solution, and then apply it to establish and prove the necessary and sufficient condition for the global existence of smooth solution. Moreover, if the smooth solution blows up at a finite time, the e...     

萃取分离-石墨炉原子吸收光谱法测定铁镍基高温合金中砷、铅、锡、锑、铋

基于砷、铅、锡、锑、铋与碘离子形成络合物,用MIBK萃取使其与基体分离, 用石墨炉原子吸收光谱法测定了铁镍基高温合金中这五种元素。文章主要对萃取条件及萃取后剩余基体对待测元素的影响进行了研究, 同时采用掩蔽的方法消除了合金中钨、铌、钽的干扰。在所选定的实验条件下,测得砷、铅、锡、锑、铋的回收率范围为93％～99％;相对标准偏差范围为8.8％～12％。     

HL-2M 支撑系统制造工艺研究

在 HL-2M 装置支撑组件的研制中,采用了特制控氮不锈钢、结合 GMS310 焊丝和 Ar(96%)+N2(4%) 保护气体的焊接工艺以及低速和大进给量的机加方式把磁导率控制在≤1.03 的设计范围内。为保障 HL-2M 装置装 配时线圈系统的精确定位和安装,在研制阶段对极向场线圈支撑子系统进行了预装。     

条件期望作为初等算子在冯-代数上的描述

定义并研究了冯-代数.条件期望基于冯-代数的描述,即作为初等算子的良好性质,会较之一般代数简洁许多.这是因为冯-代数包含一些特殊的子代数.给出了此类代数上置信的初等条件期望的描述及其最小存在的充要条件.并且定义了指标冯-有限条件期望.作为以上结果的推论,得出了条件期望指标有限的充分必要条件和一个重要不等式.     

Envelope and classification of global structures of solutions for a class of two-dimensional conservation laws

Two-dimensional Riemann problem for scalar conservation law are investigated and classification of global structure for its non-selfsimilar solution is given by analysis of structure and classification of envelope for non-selfsimilar 2D rarefaction wave. Initial data has two different constant states which are separated by initial discontinuity. We propose the concepts of plus envelope, minus envelope and mixed envelope, and some new structures and evolution phenomena are discovered by use of these concepts.     

规则波浪与强逆流作用的实验研究

针对规则波浪在强逆流作用下的阻塞现象进行实验研究,给出了不同波况下的波高与周期沿水槽的变化.实验结果表明,波浪的频率越低,所需的阻塞流速越强;波幅离散对阻塞的影响很大,不能被忽略;对于较大的入射波高,边带不稳定性会使波浪发生频率下移,进而增大阻塞所需的流速.     

Non-selfsimilar global solutions and their structure for the multi-dimensional combustion models

We investigate the Chapman-Jouguet model in multi-dimensional space, and construct explicitly its non-selfsimilar Riemann solutions. By the method we apply in this paper, general initial discontinuities can be dealt with, even for complex interaction of combustion waves. Furthermore, we analyze the way in which the area of unburnt gas shrinks.