Small angle x—ray scattering study on the conformation of polystyrene in toluene during adding anti—solvent CO2

The conformatiopn of polystyrene in the anti-solvent process of supercritical fluids(compressed CO2 polystyrene toluene)has been studied by small angle x-ray scattering with synchrotron radiation as an x-ray source.Coilto-globule transformation of the polystyrene chain was observed with the increase of the anti-solvent CO2 pressure;i.e.polystrene coiled at a prssure lower than the cloud point pressure(Pc)and turned into a globle with a uniform density at pressures higher than Pc.Fractal behaviour was also found in the chain contraction.and the mass fractal dimension increased with increasing CO2 pressure.     

SBN:Cr晶体的光折变四波混频相位共轭特性实验研究

从实验上研究了同成分SBN:Cr晶体在He-Ne激光照射下的四波混频相位共轭特性.首先测量了在不同泵浦光与信号光光强比m及不同光束夹角2θ的情况下,晶体的四波混频相位共轭反射率R随泵浦光强比p的变化关系.其次测量了泵浦光束与信号光束耦合方向对SBN:Cr晶体的四波混频相位共轭特性的影响,并就两种不同掺杂浓度的晶体样品进行了对比,所得实验结果与理论分析基本一致.最后,利用SBN:Cr晶体四波混频相位共轭特性进行了图象畸变消除实验.     

丙氨酸咪唑钐的三维荧光激发和发射光谱

测量了新制丙氨酸咪唑钐水溶液的三维荧光激发和发射光谱,分析了在不同波长激发光作用下的荧光特征,与配体咪唑、α-丙氨酸及氯化钐的荧光谱进行了比较,讨论了模型化合物上转换荧光中的双光子和多光子加合现象并发现在10^-2-10^-4 mol/L 浓度范围内荧光强度与溶液浓度呈正相关.     

Real-time phase-resolved functional optical coherence tomography by use of optical Hilbert transformation

We have developed a novel real-time phase-resolved functional optical coherence tomography system that uses optical Hilbert transformation. When we use a resonant scanner in the reference arm of the interferometer, with an axial scanning speed of 4 kHz, the frame rate of both structural and Doppler blood-flow imaging with a size of 100 by 100 pixels is 10 Hz. The system has high sensitivity and a larger dynamic range for measuring the Doppler frequency shift that is due to moving red blood cells. Real-time images of in vivo blood flow in human skin obtained with this interferometer are presented.     

Mode Distribution and Bandwidth Characteristic of Arbitrarily Trapezoidal-Groove Guide for Millimeter Waves

The modes TE and TM of arbitrarily trapezoidal-groove guide are analyzed by using the mode-matching method. The mode TE₁₁ is the dominant mode of the trapezoidal-groove guide under different conditions. The bandwidth characteristic and the operation condition for the single dominant mode are discussed. The obtained conclusions are of very important significance in theoretical study and practical application of trapeziodal-groove guides for millimeter waves.     

强链回归集与强跟踪性

为了研究强跟踪性，本文给出了强链回归集的定义．证明了：若度量空间上的一个连续自映射有强跟踪性，则其强链回归集与极限集相同．     

Anisotropic interpolation and quasi-Wilson element for narrow quadrilateral meshes

In this paper an anisotropic interpolation theorem is presentedthat can be easily used to check the anisotropy of an element.A kind of quasi-Wilson element is considered for second-orderproblems on narrow quadrilateral meshes for which the usualregularity condition _K/h_K c₀ > 0 is not satisfied, whereh_K is the diameter of the element K and _K is the radius of thelargest inscribed circle in K. Anisotropic error estimates ofthe interpolation error and the consistency error in the energynorm and the L²-norm are given. Furthermore, we give a Poincaréinequality on a trapezoid which improves a result of eniek.     

Thermal lens determination of LD end-pumped solid-state laser with stable resonator by slit scanning method

A simple method to determine the thermal focal length of LD end-pumped solid-state laser with stable resonator is presented. The M² factor describing the quality of the beam can be obtained by scanning a slit through the multi-mode Gaussian beam field. The waist width of the beam and the corresponding TEM₀₀ under the same parameters of laser are then deduced through the law of multi-mode Gaussian beam propagation. Based on the standard matrix theory of stable resonator, the thermal focal length of the gain medium can be easily achieved. To show the application of this approach, the thermal focal length of an LD pumped Nd:YVO₄ laser is measured and the experimental results are in agreement with the theoretical prediction.     

Bubble-sort图和Modified Bubble-sort图的自同构群

Bubble-Sort图和Modified Bubble-Sort图是两类特殊的Cayley图,由于其在网络构建中的应用而受到广泛关注.本文完全确定了这两类图的自同构群.     

水合乙酸锌脱水反应的动力学

用等温热重法和非等温热重法研究了Zn(CH3COO) 2·2H2 O的脱水反应 .在 61.1、62 .8、66.2、69.9℃下的等温热重数据 ,由等转化率下的lnt=E/RT +ln[g(α) /A]进行拟合 ,确定了活化能的大小 ;升温速率为 10℃ /min的非等温热重曲线显示 ,Zn(CH3COO) 2·2H2 O的脱水反应发生在 71～ 10 2℃间 ,其数据通过Doyle Zsako法进行拟合 ,以线性相关系数为判据 ,并结合等温热分析拟合结果 ,得到该脱水反应的积分动力学模式函数g(α) =[-ln( 1-α) ]2 / 3、活化能E =10 0 .8kJ/mol、指前因子ln(A/s-1) =3 6.0 9、动力学补偿效应方程为lnA =0 .3 3 3 9E + 2 .0 10 .