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Martínez-Teipel B Teixidó J Pascual R Mora M Pujolà J Fujimoto T Borrell JI Michelotti EL 《Journal of combinatorial chemistry》2005,7(3):436-448
Heterocyclic demonstration libraries for agrochemical screening were prepared from the common intermediates 2-methoxy-6-oxo-1,4,5,6-tetrahydropyridine-3-carbonitriles (1), using standard solution-phase techniques. A total of 18 screening libraries were prepared in good to excellent yields. Several members of these libraries were active in the first level of agrochemical screening, especially in the fungicide screen. 相似文献
35.
Rotor-assisted population transfer (RAPT) was developed as a method for enhancing MAS NMR sensitivity of quadrupolar nuclei by transferring polarization associated with satellite transitions to the central m=12-->-12 transition. After a single RAPT transfer, there still remains polarization in the satellite transitions that can be transferred to the central transition. This polarization is available without having to wait for the spin system to return to thermal equilibrium. We describe a new RAPT scheme that uses the remaining polarization of the satellites to obtain a further enhancement of the central transition by performing RAPT-enhanced experiments multiple times before waiting for re-equilibration of the spin system. For 27Al (I=5/2) in albite we obtain a multiple RAPT enhancement of 3.02, a 48% increase over single RAPT. For 93Nb (I=9/2) in NaNbO(3) we obtain a multiple RAPT enhancement of 5.76, an 89% increase over single RAPT. We also describe a data processing procedure for obtaining the maximum possible signal-to-noise ratio. 相似文献
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Although the laws of thermodynamics are well established for black hole horizons, much less has been said in the literature to support the extension of these laws to more general settings such as an asymptotic de Sitter horizon or a Rindler horizon (the event horizon of an asymptotic uniformly accelerated observer). In the present paper we review the results that have been previously established and argue that the laws of black hole thermodynamics, as well as their underlying statistical mechanical content, extend quite generally to what we call here causal horizons. The root of this generalization is the local notion of horizon entropy density. 相似文献
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Jerry R. Muir Jr. Ted J. Suffridge 《Proceedings of the American Mathematical Society》2001,129(11):3389-3393
In this paper, we study univalent holomorphic mappings of the unit ball in that have the property that the image contains a line for some , . We show that under certain rather reasonable conditions, up to composition with a holomorphic automorphism of the ball, the mapping is an extension of the strip mapping in the plane to higher dimensions.
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Saskia Biskup Darren J Moore Alexis Rea Bettina Lorenz-Deperieux Candice E Coombes Valina L Dawson Ted M Dawson Andrew B West 《BMC neuroscience》2007,8(1):102
Background
Mutations within the leucine-rich repeat kinase 2 (LRRK2) gene account for a significant proportion of autosomal-dominant and some late-onset sporadic Parkinson's disease. Elucidation of LRRK2 protein function in health and disease provides an opportunity for deciphering molecular pathways important in neurodegeneration. In mammals, LRRK1 and LRRK2 protein comprise a unique family encoding a GTPase domain that controls intrinsic kinase activity. The expression profiles of the murine LRRK proteins have not been fully described and insufficiently characterized antibodies have produced conflicting results in the literature. 相似文献39.
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This article develops principles for an evaluation of the efficiency of a savings bank. It starts out from the observation that such a bank is less profit oriented than a commercial bank. The customer is a vital stakeholder to the savings bank implying a greater emphasis on customer service provision. We are using data envelopment analysis (DEA) as a method to consider the service orientation of savings banks. We thereby demonstrate how an evaluation of the performance of savings banks according to “service efficiency” differs from an evaluation based on the traditional “profit” or shareholder concept. We determine the number of Swedish savings banks being “service efficient” as well as the average degree of service efficiency in this industry. 相似文献