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101.
The physico-chemical properties and reactivity tested by hydrogen reduction have been studied for two series of NiO-ZnO mixed oxides of various composition. The solid nickel oxide or zinc oxide in interaction with the solution of nitrate of the second component were used as the precursors in each series. The differences in some physico-chemical parameters of the samples in both series were correlated with their reduction behaviour, followed both in iso- and non-isothermal regime. Moreower, the influence of various factors modifying the reactivity of mixed oxides was also investigated and the results were compared with those obtained from earlier studied analogous systems of quite different origin.This revised version was published online in November 2005 with corrections to the Cover Date. 相似文献
102.
D. Barrios Rolanía G. Lpez Lagomasino E. B. Saff 《Journal of Approximation Theory》2003,124(2):263-281
Using a convergence theorem for Fourier–Padé approximants constructed from orthogonal polynomials on the unit circle, we prove an analogue of Hadamard's theorem for determining the radius of m-meromorphy of a function analytic on the unit disk and apply this to the location of poles of the reciprocal of Szeg
functions. 相似文献
103.
Parameters of Gaussian multivariate models are often estimated using the maximum likelihood approach. In spite of its merits, this methodology is not practical when the sample size is very large, as, for example, in the case of massive georeferenced data sets. In this paper, we study the asymptotic properties of the estimators that minimize three alternatives to the likelihood function, designed to increase the computational efficiency. This is achieved by applying the information sandwich technique to expansions of the pseudo-likelihood functions as quadratic forms of independent normal random variables. Theoretical calculations are given for a first-order autoregressive time series and then extended to a two-dimensional autoregressive process on a lattice. We compare the efficiency of the three estimators to that of the maximum likelihood estimator as well as among themselves, using numerical calculations of the theoretical results and simulations. 相似文献
104.
Franc Forstnerič 《Mathematische Annalen》1992,292(1):163-180
105.
Pedro lvarez‐Boo Jos Sergio Casas Alfonso Castieiras María Delfina Couce Eduardo Freijanes Eva Novoa Jos Sordo 《应用有机金属化学》2003,17(9):725-729
Reaction of dichloro‐ and dibromodimethyltin(IV) with 2‐(pyrazol‐1‐ylmethyl)pyridine (PMP) afforded [SnMe2Cl2(PMP)] and [SnMe2Br2(PMP)] respectively. The new complexes were characterized by elemental analysis and mass spectrometry and by IR, Raman and NMR (1H, 13C) spectroscopies. Structural studies by X‐ray diffraction techniques show that the compounds consist of discrete units with the tin atom octahedrally coordinated to the carbon atoms of the two methyl groups in a trans disposition (Sn? C = 2.097(5), 2.120(5) Å and 2.110(6), 2.121(6) Å in the chloro and in the bromo compounds respectively), two cis halogen atoms (Sn? Cl = 2.4908(16), 2.5447(17) Å; Sn? Br = 2.6875(11), 2.7464(9) Å) and the two donor atoms of the ligand (Sn? N = 2.407(4), 2.471(4) Å and 2.360(5), 2.455(5) Å). In both cases, the Sn? N(pyridine) bond length is markedly longer than the Sn? N(pyrazole) distance. Copyright © 2003 John Wiley & Sons, Ltd. 相似文献
106.
Július Korbaš 《Acta Mathematica Hungarica》2004,105(1-2):129-137
We prove new results about the vector field problem on the real flag manifolds O(n)/O(1) x O(1) x O(n - 2). For some infinite families of these manifolds, we completely solve the vector field problem. 相似文献
107.
Summary. We introduce linear semi-implicit complementary volume numerical scheme for solving level set like nonlinear degenerate diffusion
equations arising in image processing and curve evolution problems. We study discretization of image selective smoothing equation
of mean curvature flow type given by Alvarez, Lions and Morel ([3]). Solution of the level set equation of Osher and Sethian
([26], \[30]) is also included in the study. We prove and estimates for the proposed scheme and give existence of its (generalized) solution in every discrete time-scale step. Efficiency
of the scheme is given by its linearity and stability. Preconditioned iterative solvers are used for computing arising linear
systems. We present computational results related to image processing and plane curve evolution.
Received April 25, 2000 / Revised version received June 11, 2001 / Published online November 15, 2001 相似文献
108.
Lubomír Kubáček 《Mathematica Slovaca》2007,57(6):571-588
The multivariate model, where not only parameters of the mean value of the observation matrix, but also some other parameters
occur in constraints, is considered in the paper. Some basic inference is presented under the condition that the covariance
matrix is either unknown, or partially unknown, or known.
Supported by the grant of the Council of Czech Republic MSM 6 198 959 214. 相似文献
109.
We prove that a locally compact ANR-space X is a Q-manifold if and only if it has the Disjoint Disk Property (DDP), all points of X are homological Z
∞-points and X has the countable-dimensional approximation property (cd-AP), which means that each map f: K → X of a compact polyhedron can be approximated by a map with the countable-dimensional image. As an application we prove that
a space X with DDP and cd-AP is a Q-manifold if some finite power of X is a Q-manifold. If some finite power of a space X with cd-AP is a Q-manifold, then X
2 and X × [0, 1] are Q-manifolds as well. We construct a countable family χ of spaces with DDP and cd-AP such that no space X ∈ χ is homeomorphic to the Hilbert cube Q whereas the product X × Y of any different spaces X, Y ∈ χ is homeomorphic to Q. We also show that no uncountable family χ with such properties exists.
This work was supported by the Slovenian-Ukrainian (Grant No. SLO-UKR 04-06/07) 相似文献
110.
The presented one-capacitor pinch driver, designed as a compact coaxial structure (including spark-gap and discharge section) consistent with the capacitor output, generates a current of 200 kA with 700 ns quarter-period, suitable for studying the optimization of Z-pinch radiative characteristics. The driver is described, measurements of its parameters summarized, and relations to our previous and future activities briefly reviewed.This work was supported in part by the Grant Agency of the Czech Republic under contract No. 202/93/1023. 相似文献