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41.
Markus Bacher Karl Baumann Hermann Knapp Andrea Steck Sigrid Teibl 《Magnetic resonance in chemistry : MRC》2009,47(1):71-83
The complete 1H and 13C NMR data of 27 pravastatin derivatives are presented. Assignment was achieved by use of 1D and 2D NMR experiments (selective 1D NOE, COSY, NOESY, HSQC, HMBC). Copyright © 2008 John Wiley & Sons, Ltd. 相似文献
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We consider an integrated production and distribution scheduling problem in a make-to-order business scenario. A product with a short lifespan (e.g., perishable or seasonal) is produced at a single production facility with a limited production rate. This means that the product expires in a constant time after its production is finished. Orders are received from a set of geographically dispersed customers, where a demand for the product and a time window for the delivery is associated with each customer for the planning period. A single vehicle with non-negligible traveling times between the locations is responsible for the deliveries. Due to the limited production and distribution resources, possibly not all customers may be supplied within their time windows or the lifespan. The problem consists in finding a selection of customers to be supplied such that the total satisfied demand is maximized. We extend the work by Armstrong et al. (Annals of Operations Research 159(1):395–414, 2008) on the problem for fixed delivery sequences by pointing out an error in their branch and bound algorithm and presenting a corrected variant. Furthermore, we introduce model extensions for handling delays of the production start as well as for variable production and distribution sequences. Efficient heuristic solution algorithms and computational results for randomly generated instances are presented. 相似文献
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In the present work, we discuss the benefits, limitations and restrictions for the high order phase fitted variational integrators, derived specifically for the numerical integration of systems with oscillatory solutions. To do that, we study linear stability properties of these methods using the eigenvalues of the amplification matrix. The obtained stability region verifies their good behavior, when used for the numerical solution of highly oscillatory problems. (© 2014 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
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Let S be a bounded, Riemann measurable set in Rd, and Λ be a lattice. By a theorem of Fuglede, if S tiles Rd with translation set Λ, then S has an orthogonal basis of exponentials. We show that, under the more general condition that S multi-tiles Rd with translation set Λ, S has a Riesz basis of exponentials. The proof is based on Meyer?s quasicrystals. 相似文献
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Sigrid Baumgarten Ron C. Gaba Richard B. van Breemen 《Biomedical chromatography : BMC》2012,26(12):1529-1533
Because liver cancer is rarely suitable for surgery, transcatheter arterial chemoembolization (TACE) is used for palliative therapy. In this procedure, an emulsion of doxorubicin in iodized oil is injected directly into liver tumors through a catheter positioned within the artery supplying blood flow to the tumor. At present, there is limited understanding of factors affecting the delivery and dispersion of doxorubicin within treated tumors during TACE. This study addresses the development and application of an ultrahigh‐pressure liquid chromatography–tandem mass spectrometry (UHPLC‐MS‐MS) method for rapid confirmation of drug delivery after TACE in a rabbit VX2 liver cancer model. Doxorubicin levels in liver tumors were measured using UHPLC‐MS‐MS and compared with computed tomography measured levels of iodized oil, a metric used clinically to indicate drug delivery. We found that tissue drug levels determined using UHPLC‐MS‐MS did not correlate with the regional iodized oil concentration (vehicle) within tumors following TACE, suggesting that chemotherapeutic drugs like doxorubicin spread throughout tumors, and that lack of iodized oil staining in portions of a tumor does not necessarily indicate inadequate therapy during TACE. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
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Sigrid Blömeke Lynn Paine Richard T. Houang Feng-Jui Hsieh William H. Schmidt M. Teresa Tatto Kiril Bankov Tenoch Cedilllo Leland Cogan Shin Il Han Marcella Santillan John Schwille 《ZDM》2008,40(5):749-762
The study "Mathematics Teaching in the 21st Century (MT21)" focuses beyond others on the measurement of teachers’ general pedagogical knowledge (GPK). GPK is regarded as a latent construct embedded in a larger theory of teachers’ professional competence. It is laid out how GPK was defined and operationalized. As part of an international comparison GPK was measured with several complex vignettes. In the present paper, the results of future mathematics teachers’ knowledge from four countries (Germany, South Korea, Taiwan, and the US) with very different teacher-education systems are presented. Significant and relevant differences between the four countries as well as between future teachers at the beginning and at the end of teacher education were found. The results are discussed with reference to cultural discourses about teacher education. 相似文献