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31.
Marwa A. A. Ragab Hadir M. Maher Salma Tarek Hoda Mahgoub 《Journal of separation science》2023,46(4):2200951
Gastrointestinal tract disorders constitute a heavy burden to healthcare providers. To eradicate Helicobacter pylori infection, different triple therapy protocols have been proposed. Among which are combinations of proton pump inhibitors (e.g., omeprazole), histamine-2 receptor antagonists (e.g., famotidine), along with antibiotics (e.g., amoxicillin). In this work, a sensitive and accurate high-performance thin-layer chromatographic method was developed for the simultaneous determination of amoxicillin, metronidazole, and famotidine in bulk powder and laboratory-prepared combined-tablet mixtures. Complete separation of the cited compounds was achieved using pre-coated silica gel plates with a mixture of methanol:chloroform:toluene:water:glacial acetic acid (5:2:1.5:0.5:0.1 v/v/v/v/v) as the mobile phase. The method was fully validated as per the international conference of harmonization guidelines. Good linearity, a correlation coefficient of 0.9991, was obtained in the concentration ranges 0.1–1.6 μg/band (amoxicillin), 0.1–0.9 μg/band (metronidazole), and 0.1–0.9 μg/band (famotidine). Since the method allowed the determination of the three compounds in combined tablets with a high degree of selectivity, accuracy, precision, with cost-effectiveness, it could be used for regular quality control. Moreover, the applicability of the proposed method was extended to the determination of the ternary mixture in simulated gastric juice. Method greenness was assessed using different green metrics. 相似文献
32.
Tarek Emam 《数学物理学报(B辑英文版)》2009,29(5):1128-1142
In this paper, we consider a method of centers for solving multi-objective programming problems, where the objective functions involved are concave functions and the set of feasible points is convex. The algorithm is defined so that the sub-problems that must be solved during its execution may be solved by finite-step procedures. Conditions are given under which the algorithm generates sequences of feasible points and constraint multiplier vectors that have accumulation points satisfying the KKT conditions. Finally, we establish convergence of the proposed method of centers algorithm for solving multiobjective programming problems. 相似文献
33.
SAANOUNI Tarek 《偏微分方程(英文版)》2011,(1):37-54
Let u ∈ C(1R, H1) be the solution to the initial value problem for a 2D semilinear Schr6dinger equation with exponential type nonlinearity, given in [1]. We prove that the Lr norms of u decay as t→±∞, provided that r〉2. 相似文献
34.
Tarek Sayed Ahmed 《Mathematical Logic Quarterly》2011,57(4):384-394
Using games, as introduced by Hirsch and Hodkinson in algebraic logic, we give a recursive axiomatization of the class RQPEA α of representable quasi‐polyadic equality algebras of any dimension α. Following Sain and Thompson in modifying Andréka’s methods of splitting, to adapt the quasi‐polyadic equality case, we show that if Σ is a set of equations axiomatizing RPEA n for $2< n <\omegaUsing games, as introduced by Hirsch and Hodkinson in algebraic logic, we give a recursive axiomatization of the class RQPEA α of representable quasi‐polyadic equality algebras of any dimension α. Following Sain and Thompson in modifying Andréka’s methods of splitting, to adapt the quasi‐polyadic equality case, we show that if Σ is a set of equations axiomatizing RPEA n for $2< n <\omega$ and $l< n,$ $k < n$, k′ < ω are natural numbers, then Σ contains infinitely equations in which ? occurs, one of + or · occurs, a diagonal or a permutation with index l occurs, more than k cylindrifications and more than k′ variables occur. © 2011 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim 相似文献
35.
36.
[reaction: see text] The conversion of 1-(2-methoxyethoxy)ethyl-protected beta-hydroxy ketones to syn-1,3-ethylidene acetals is effected by Et(3)SiH and SnCl(4). This reaction is proposed to proceed via a cyclic oxocarbenium ion intermediate and provides the products in yields that range from 69 to 94% and with diastereoselectivities that are >200:1. 相似文献
37.
Tarek A. Ramadan 《Optical and Quantum Electronics》2012,43(11-15):175-189
A search-and-track algorithm is proposed for controlling the number of guided modes of planar optical waveguides with arbitrary refractive index profiles. The algorithm starts with an initial guess point in the parameter space that supports a specific number of guided modes. Then, it searches for, and tracks, the boundaries of this space or another space supporting different number of modes. It does so by monitoring the sign of a unified cutoff dispersion function. The algorithm is applied to both symmetric and asymmetric silicon-based parabolic-index waveguides. It shows that unlike asymmetric waveguides, the single-mode condition of symmetric waveguides is controlled by TM-, as opposed to TE-, polarization. This abnormal polarization control is strongest for high index contrast waveguides of sub-micrometer core sizes. The results are verified by full-vectorial beam propagation method. 相似文献
38.
Tarek A.?SalamaEmail author Bernd?Lackner Heinz?Falk 《Monatshefte für Chemie / Chemical Monthly》2003,134(8):1113-1119
Summary. An efficient synthesis of tri-O-methylemodin aldehyde was achieved via bromination of tri-O-methylemodin utilizing N-bromosuccinimide yielding the monobromo and dibromo derivatives. Sommelet reaction of the monobromomethyl derivative as well as hydrolysis of the dibromomethyl analog with aqueous silver nitrate afforded the protected aldehyde in good yield. Accordingly, both bromo derivatives can be used even when they are obtained as a mixture of the bromination reaction, which could not be controlled easily to yield the bromo products selectively. From the aldehyde the tri-O-methylemodin nitrile was prepared in a one-pot reaction using hydroxylamine-O-sulfonic acid.Received February 18, 2003; accepted March 3, 2003
Published online June 2, 2003 相似文献
39.
Salama Tarek A. El-Ahl Abdel-Aziz S. Khalil Abdel-Galil M. Girges Margret M. Lackner Bernd Steindl Christian Elmorsy Saad S. 《Monatshefte für Chemie / Chemical Monthly》2003,134(9):1241-1252
Summary. Several new 1-aryl-, aralkyl-, and heteroaryl-5-(4-phenylbuta-1,3-dienyl)tetrazole derivatives and annulated tetrazole derivatives were efficiently and regiospecifically prepared in nearly quantitative yield via a facile one step reaction of dienones with a combination of tetrachlorosilane and sodium azide in acetonitrile under mild conditions. A complete structure assignment of three representative examples of the tetrazoles was achieved by advanced 2D NMR measurements including COSY, TOCSY, HSQC, HMBC, NOESY, and ROESY experiments.Received March 17, 2003; accepted March 18, 2003
Published online July 28, 2003 相似文献
40.
Mohamed Baqar Tarek Agag Hatsuo Ishida Syed Qutubuddin 《Journal of polymer science. Part A, Polymer chemistry》2012,50(11):2275-2285
A new class of high‐performance resins of combined molecular structure of both traditional phenolics and benzoxazines has been developed. The monomers termed as methylol‐functional benzoxazines were synthesized through Mannich condensation reaction of methylol‐functional phenols and aromatic amines, including methylenedianiline (4,4′‐diaminodiphenylmethane) and oxydianiline (4,4′‐diaminodiphenyl ether), in the presence of paraformaldehyde. For comparison, other series of benzoxazine monomers were prepared from phenol, corresponding aromatic amines, and paraformaldehyde. The as‐synthesized monomers are characterized by their high purity as judged from 1H NMR and Fourier transform infrared spectra. Differential scanning calorimetric thermograms of the novel monomers show two exothermic peaks associated with condensation reaction of methylol groups and ring‐opening polymerization of benzoxazines. The position of methylol group relative to benzoxazine structure plays a significant role in accelerating polymerization. Viscoelastic and thermogravimetric analyses of the crosslinked polymers reveal high Tg (274–343 °C) and excellent thermal stability when compared with the traditional polybenzoxazines. © 2012 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem, 2012 相似文献