Isolation and Structure Elucidation of Nortriterpenoids from Schisandra rubriflora

Seven new highly oxygenated nortriterpenoids, rubriflorins D–J ( 1 – 7 ), were isolated from the leaves and stems of Schisandra rubriflora, and their structures were elucidated on the basis of extensive analysis of spectroscopic data. These new compounds feature the opening of ring A compared with related known nortriterpenoids isolated from the genus Schisandra and showed weak activity against HIV‐1.     

Stability of Methods for Matrix Inversion

Inversion of a triangular matrix can be accomplished in severalways. The standard methods are characterized by the loop ordering,whether matrix-vector multiplication, solution of a triangularsystem, or a rank-1 update is done inside the outer loop, andwhether the method is blocked or unblocked. The numerical stabilityproperties of these methods are investigated. It is shown thatunblocked methods satisfy pleasing bounds on the left or rightresidual. However, for one of the block methods it is necessaryto convert a matrix multiplication into the solution of a multipleright-hand side triangular system in order to have an acceptableresidual bound. The inversion of a full matrix given a factorizationPA=LU is also considered, including the special cases of symmetricindefinite and symmetric positive definite matrices. Three popularmethods are shown to possess satisfactory residual bounds, subjectto a certain requirement on the implementation, and an attractivenew method is described. This work was motivated by the questionof what inversion methods should be used in LAPACK.     

关于拟AP内射模的一些研究

Let R be a ring. R is called right AP-injective if, for any a ∈ R, there exists a left ideal of R such that lr(a) = Ra (?) Xa. We extend this notion to modules. A right .R-module M with 5 = End(MR) is called quasi AP-injective if, for any s ∈ S, there exists a left ideal Xs of S such that ls(Ker(s)) = Ss (?) Xs. In this paper, we give some characterizations and properties of quasi AP-injective modules which generalize results of Page and Zhou.     

Design and Fabrication of 1.06 μm Resonant-Cavity Enhanced Reflective Modulator with GaInAs/GaAs Quantum Wells

A resonant-cavity enhanced reflective optical modulator is designed and fabricated, with three groups of three highly strained InGaAs/GaAs quantum wells in the cavity, for low voltage and high contrast ratio operation. The quantum wells are positioned in antinodes of the optical standing wave. The modulator is grown in a single growth step in an molecular beam epitaxy system, using GaAs/AlAs distributed Bragg reflectors as both the top and bottom mirrors. Results show that the reflection device has a modulation extinction of 3 dB at -4.5 V bias.     

Synthesis of TiO2–SiO2/polymer core–shell microspheres with a microphase‐inversion method

A novel microphase‐inversion method was proposed for the preparation of TiO₂–SiO₂/poly(methyl methacrylate) core–shell nanocomposite particles. The inorganic–polymer nanocomposites were first synthesized via a free‐radical copolymerization in a tetrahydrofuran solution, and the poor solvent was added slowly to induce the microphase separation of the nanocomposite and result in the formation of nanoparticles. The average particle sizes of the microspheres ranged from 70 to 1000 nm, depending on the reaction conditions. Transmission electron microscopy and scanning electron microscopy indicated a core–shell morphology for the obtained microspheres. Thermogravimetric analysis and X‐ray photoelectron spectroscopy measurements confirmed that the surface of the nanocomposite microspheres was polymer‐rich, and this was consistent with the core–shell morphology. The influence of the synthetic conditions, such as the inorganic composition and the content of the crosslinking monomer, on the particle properties was studied in detail. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 3911–3920, 2006     

基于CT算法的束团横向相空间测量

精确测量束团的发射度和横向相空间, 在高亮度电子束的产生和应用中具有重要意义. 传统测量方法在测量发射度时需要对束团在相空间内分布进行初始假设, 且只能给出相椭圆的twiss参数;基于CT(computerized tomography)算法的束团横向相空间测量方法无需先验假设, 能给出粒子在相空间内的真实分布, 测量结果更为精确. 介绍了基于CT算法的束团横向相空间测量的原理和初步实验结果, 并与四极透镜扫描法测量的结果进行了比较.     

Positive Steady States of a Prey-predator Model with Diffusion and Non-monotone Conversion Rate

In this paper, we study the positive steady states of a prey-predator model with diffusion throughout and a non-monotone conversion rate under the homogeneous Dirichlet boundary condition. We obtain some results of the existence and non-existence of positive steady states. The stability and uniqueness of positive steady states are also discussed.     

三种瓜环与4,4′-联吡啶及N,N′-二甲基4,4′-联吡啶盐酸盐相互作用的研究

以七元瓜环(Q[7])和新型椭圆型改性瓜环———对称四甲基取代六元瓜环(TM eQ[6])为主体,4,4′-联吡啶的盐酸盐(44)以及N,N′-二甲基4,4′-联吡啶的盐酸盐(dm44)为客体的主客体相互作用进行了考察.实验结果表明,Q[7]与客体44及dm44作用体系中,客体为了更有效地被主体Q[7]包结,在Q[7]内腔中呈倾斜状分布的几率最高.用核磁共振、循环伏安以及紫外吸收光谱对实验结果进行了印证和补充,验证了TM eQ[6]与客体44及dm44可发生较强的相互作用,形成一维的自组装超分子结构.核磁共振以及循环伏安方法的实验结果表明,没有观察到Q[6]与客体44及dm44的明显作用,而紫外吸收光谱方法证实,Q[6]与客体44确实存在一定的相互作用,比较主客体的结构特征,该作用体系也可能存在自组装的一维超分子结构等多种作用形式.     

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HT-7中性束诊断电源系统的计算机控制系统由PLC、工控机、逻辑控制和定时单元等组成。对起弧、束流引出等实验进行了研究。在多种参数下,通过调节弧压、进气量等观察了其对弧流的影响。初步实验结果表明,在高压35kV、弧流80A的情况下,束电流可以达到3.6A,引出的中性束流功率可以稳定地达到50kW以上。     

Phase-Locked Fibre Array for Coherent Combination and Atmosphere Aberration Compensation

We report a fibre amplifier array that not only achieves coherent beam combination by compensation of phase noises of fibre amplifier, but also accomplishes correction of atmosphere aberration. It is of master-oscillatormultiple-amplifier （MOPA） configuration, which can be phase-locked by the multidither principle or heterodyne detection principle. First laboratory experiments of atmosphere aberration compensation of a three-element fibre amplifier array are reported. The atmosphere aberration is created by a phase screen in the experiment. The phase changes of the beam, which are introduced by the fibre amplifier and the phase screen, are both detected by the heterodyne detection method. Phase modulators are controlled to compensate for the phase in the three paths. No matter whether there is a phase screen producing atmosphere aberration or not, the dim dynamic interference fringes in the far field turn to a clear and stable pattern, and the peak intensity is maximized. It is indicated that the fibre amplifier array is phase-locked, and coherent combination of the three beams is achieved. It can be used not only to obtain high power fibre laser array but also in laser space communication.