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Ritesh Raju Oleksandr Gromyko Viktor Fedorenko Andriy Luzhetskyy Rolf Müller 《Tetrahedron letters》2012,53(24):3009-3011
A Streptomyces sp. Lv3-13, isolated from the rhizosphere soil of the plant Mespilus germanica, has yielded three new pimprinine derivatives, named pimprinols A–C (1–3) and the unknown (2-aminophenyl)(2-ethyloxazol-5-yl) methanone (4) along with the known compounds 2-ethyl oxazole pimprinine and 2-propyl oxazole pimprinine. The structures of the compounds were elucidated based on spectroscopic methods including UV, HR-ESIMS and 1D, 2D NMR data. Compounds 1–4 were screened for antimicrobial and cytotoxic activities. 相似文献
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E. Fischbach G. L. Klimchitskaya D. E. Krause V. M. Mostepanenko 《The European Physical Journal C - Particles and Fields》2010,68(1-2):223-226
We discuss the constraints on the parameters of a Yukawa interaction obtained from the indirect measurements of the Casimir pressure between parallel plates using the sphere–plate configuration. Recently, it was claimed in the literature that the application of the proximity force approximation (PFA) to the calculation of a Yukawa interaction in the sphere–plate configuration could lead to a large error of order 100% in the constraints obtained. Here we re-calculate the constraints both exactly and using the PFA, and arrive at identical results. We elucidate the reasons why an incorrect conclusion was obtained suggesting that the PFA is inapplicable to calculate the Yukawa force. 相似文献
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Rolf Huisgen 《Angewandte Chemie (International ed. in English)》2011,50(41):9535-9536
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In this editorial, we set out the aims in the call to publish papers on informal statistical inference, randomness, modelling and risk. We discuss how the papers published in this issue have responded to those aims. In particular, we note how the nine papers contribute to some of the major debates in mathematics and statistics education, often taking contrasting positions. Such debates range across: (1) whether knowledge is fractured or takes the form of mental models; (2) heuristic or intuitive thinking versus operational thinking as for example in dual process theory; (3) the role of different epistemic resources, such as perceptions, modelling, imagery, in the development of probabilistic reasoning; (4) how design and situation impact upon probabilistic learning. 相似文献
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A short and versatile synthesis of substituted quinolines is provided. Alkylation of sodium tolylsulfinate with bromomethyl- or chloromethyl ketones generates beta-keto sulfones. Knoevenagel condensation of the beta-keto sulfones with an aldehyde provides alpha-tolylsulfonyl-alpha,beta-unsaturated ketones. Michael addition of the dianion of N-Boc-anilines in the presence of CuCN and LiCl with the unsaturated ketone generates a 1,4-adduct, which after deprotection of the Boc group and thermal elimination of the tolyl sulfone provides the quinoline. 相似文献
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