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991.
Ralph E. Taylor-Smith Richard A. Register 《Journal of Polymer Science.Polymer Physics》1994,32(12):2105-2114
The nature and extent of phase mixing in blends of hydroxyl-functionalized polystyrene and poly(ethyl acrylate) (PS/PEA), where the driving force for mixing is hydrogen bonding, are characterized by several techniques. Small-angle x-ray scattering (SAXS) shows a reduction in average domain size with increasing functionalization level, a result also evident from scanning electron microscopy (SEM). Together, the two techniques reveal a very broad distribution of domain sizes. At high functionalization levels, both SAXS and SEM indicate a high degree of “in-domain” mixing, with little or no pure PS or PEA remaining in the blends. Mathematical modeling of dynamic mechanical thermal analysis (DMTA) data is employed to quantify this progression. Initially, mixing is primarily interfacial, but as the functionalization level increases, the mixed interphase rapidly grows to occupy the entire material. In agreement with the SAXS and SEM results, DMTA modeling shows that further increases in the functionalization level suppress the amplitude of composition variations in the sample. The onset of extensive in-domain mixing coincides with the marked changes in stress-strain behavior observed previously in these materials. © 1994 John Wiley & Sons, Inc. 相似文献
992.
David A. Kort Wengan Wu Phillip E. Fanwick Richard A. Walton 《Transition Metal Chemistry》1995,20(6):625-629
993.
Richard Ormerod 《The Journal of the Operational Research Society》1996,47(9):1083-1097
The development of an information systems (IS) strategy for a mineral extraction and processing plant operated by Rio Tinto Zinc (RTZ) in South Africa is described. The participative approach used was developed from soft OR and systems thinking. The aim of the Richards Bay project was to test commercially whether the Participative Information Management Strategy (PIMS) methodology could be used as a standard method to be applied to the development of an information systems strategy at any mine site. The paper describes the implementation of the process and the problems encountered. More generally it discusses the diffusion of new ideas in an international company, illustrated by the use of the participative approach for other activities including systems development. Conclusions are drawn about the value of participative approaches based on soft OR in this context. 相似文献
994.
995.
Richard D. Sontheimer 《Photochemistry and photobiology》1996,63(5):583-594
996.
A new tricyclic C12 hydrocarbon, inflatene (1), possessing unexpected ichthyotoxic properties, has been isolated as the major metabolite of the stoloniferan var. . The structure of inflatene was secured by extensive FT-NMR studies with the natural product and several key derivatives. 相似文献
997.
Tetrakis(dimethylamino)ethene (TDAE) and trimethylamine react with anhydrous unsaturated fluorocarbons to produce, ‘in situ’, powerful fluoride- ion sources. These are used to initiate carbon- carbon bond forming reactions eg. oligomerisation and polyfluoroalkylation, and many of these reactions occur efficiently in the absence of a solvent. 相似文献
998.
999.
Richard B. Abbott 《Zeitschrift fur Physik C Particles and Fields》1984,26(3):393-399
Standard path-integral techniques such as instanton calculations give good answers for weak-coupling problems, but become unreliable for strong-coupling. Here we consider a method of replacing the original potential by a suitably chosen harmonic oscillator potential. Physically this is motivated by the fact that potential barriers below the level of the ground-state energy of a quantum-mechanical system have little effect. Numerically, results are good, both for quantum-mechanical problems and for massive φ4 field theory in 1+1 dimensions. 相似文献
1000.
This paper examines the relative efficiency of alternative methods of producing care for the developmentally disabled. A linear programming framework is used to construct a production frontier which allows measurement of relative efficiency among institutions in the sample. Tests are performed to detect influential observations in the data which might result from measurement error which could distort the efficiency measures. Different types of institutions are compared in terms of average efficiency. Policy implications of the analysis are discussed in the concluding section. 相似文献