激光拉曼光谱结合紫外光谱检测茶水中的咖啡因

利用激光拉曼光谱法结合紫外光谱法对直接一次浸泡茶水(碧螺春、龙井和普洱)中的咖啡因进行了定性和定量检测,分析了其咖啡因含量。该方法便捷易行,具有较高的灵敏度,为茶水中咖啡因的直接检测提供了一条有效的途径。     

氩、氢混合等离子体处理对GaAs表面性质及发光特性的影响

介绍了一种氩、氢混合等离子体清洗GaAs基片的实验工艺,深入研究了氩、氢等离子体清洗GaAs表面污染物和氧化层,并活化表面性能的基本原理,同时讨论了气体流量、溅射功率和清洗时间等不同溅射参数对等离子体清洗效果的影响。结果表明,在氩气和氢气流量分别为10 cm³/min和30 cm³/min,溅射功率为20 W,清洗时间为15 min的条件下,GaAs样品的光致发光强度提高达139.12%,样品表面的As-O键和Ga-O键基本消失。     

基于集成综合评价法和聚类分析法的综合评价方法

针对传统的主成分分析法在数据无量纲化中"中心标准化"的缺点,提出了改进的主成分分析方法,并建立了一种基于集成综合评价法和聚类分析法的新的综合评价方法,通过黑龙江省各城市综合竞争力的统计分析结果说明该方法能有效的得出合理结果.     

基于金纳米簇探针的荧光猝灭检测铁离子

以D-色氨酸为保护剂和还原剂, 采用水热法快速制备了具有强荧光的金纳米簇(D-Trp@AuNCs); 以其作为荧光探针, 建立了基于荧光猝灭的选择性高灵敏检测Fe³⁺的传感方法. 利用透射电子显微镜(TEM)、 紫外-可见光谱(UV-Vis)和红外光谱(IR)等手段对制备的金纳米簇进行了表征, 并利用荧光光谱研究了D-Trp@AuNCs的荧光性能. 结果表明, D-Trp@AuNCs具有较好的生物相容性, 其最大激发波长为370 nm, 最大发射波长为460 nm; 向金纳米簇溶液中加入Fe³⁺后, D-Trp@AuNCs的荧光发生明显猝灭, 其猝灭程度与Fe³⁺的浓度在0.3~500.0 μmol/L范围内呈现良好的线性关系, 检出限为33.1 nmol/L(S/N=3). 将该荧光探针用于实际水样中Fe³⁺的检测, 回收率为86.6%~106.5%.     

解耦双回路气化系统中生物质催化水蒸气气化制富氢气体

为强化生物质气化过程中焦油转化和氢气富集,提出了一种新型解耦双回路气化系统(DDLG) 。该气化系统将气化过程解耦为燃料气化、焦油重整和半焦燃烧三个子过程,分别发生于三个独立的反应器,即气化反应器、重整反应器和燃烧反应器。其中,气化反应器和重整反应器并行布置,分别与燃烧反应器相连,形成两个平行的且可独立控制的双循环回路。以松木屑为原料及兼作为原位焦油重整催化剂的煅烧橄榄石为循环固体热载体,考察了反应条件对 DDLG 中松木屑气化性能的影响。结果表明,重整反应器从气化反应器中解耦,并辅以橄榄石催化剂,可实现焦油高效转化脱除。如气化反应器700℃、重整反应器 850℃和水蒸气与原料中碳的质量比(S/C) 1.2 反应条件下,产品气中焦油含量降低至13.9g /m~3,气体产率和H_2分别达到1.0m~3 /kg,和38.8%。     

基于AdapChem方法的甲烷预混和非预混燃烧数值计算

采用自适应化学理论AdapChem的方法对两种CH4/空气部分预混、非预混火焰的燃烧过程开展了数值模拟工作.计算得到了两种燃烧工况下,几种重要的主量成分、非主量成分的浓度值;同时对反应放热和HCO之间的潜在关系进行了分析.通过对两种工况下模拟结果的比较,AdapChem方法合理预报了甲烷预混和非预混燃烧过程的各种物理化学特性,并达到了节约计算时间的目的.     

Restudy on Dark Matter Time-Evolution in the Littlest Higgs Model with T-Parity

Following previous study, in the littlest Higgs model （LHM）, the heavy photon is supposed to be a possiL dark matter candidate and its relic abundance of the heavy photon is estimated in terms of the Boltzman- Lee-Weinba time-evolution equation. The effect of the T-parity violation is also considered. Our calculations show that when Higmass MH taken to be 300 GeV and do not considering T-parity violation, only two narrow ranges 133 〈 MAH 〈 135 Ge and 167 〈 MAH〈 169 GeV are tolerable with the current astrophysical observation and if 135 〈 MAH 〈 167 GeV there must at least exist another species of heavy particle contributing to the cold dark matter. As long as the T-pari; can be violated, the heavy photon can decay into regular standard model particles and would affect the dark matt abundance in the universe, we discuss the constraint on the T-parity violation parameter based on the present dat Direct detection prospects are also discussed in some detail.     

Calculation of High Frequency Complex Permeability of Carbonyl Iron Flakes in a Nomagnetic Matrix

The carbonyl iron flakes are fabricated by high-energy ball milling. The effective permeability is measured and calculated for the composite consisting of flakes embedded in a nonmagnetic matrix. The magnetic flakes with a shape anisotropy and random spatial distribution of normal direction are considered to calculate the complex permeability of magnetic flake materials. Its analytical model is derived from the Landau-Lifshitz-Gilbert equation and Bruggeman ＇s effective medium theory. The calculated results agree well with the experiment.     

Demonstration of a 4H SiC Betavoltaic Nuclear Battery Based on Schottky Barrier Diode

A 4H SiC betavoltaic nuclear battery is demonstrated. A Schottky barrier diode is utilized for carrier separation. Under illumination of Ni-63 source with an apparent activity of 4mCi/cm^2, an open circuit voltage of 0.49 V and a short circuit current density of 29.44nA/cm^2 are measured. A power conversion efficiency of 1.2% is obtained. The performance of the device is limited by low shunt resistance, backscattering and attenuation of electron energy in air and Schottky electrode. It is expected to be significantly improved by optimizing the design and processing technology of the device.     

兰州重离子加速器冷却储存环

 兰州重离子加速器冷却储存环HIRFL-CSR,是一个多用途、多功能的双冷却储存环同步加速器系统,由主环CSRm和实验环CSRe构成,并以兰州重离子级联回旋加速器HIRFL作注入器。CSR利用高频变谐波的方法,将重离子束的能量从7～25 MeV/u同步加速到２00～1 000 MeV/u,同时利用重离子储存环中空心电子束冷却技术将束流品质提高１个数量级,并通过储存环的快引出及慢引出,提供多种类的重离子束以及放射性次级束(RIBs),以开展范围更广精度更高的物理实验。该装置于2007年投入运行,已取得了重要的运行结果,如实现了剥离注入与多圈注入、空心电子束对重离子束的冷却与累积、变谐波宽能区同步加速、等时性环型谱仪、RIBs的产生收集与ToF高分辨质量测量以及高能重离子束的变能慢引出等。