Production of Atosiban’s Key Intermediate Pentapeptide: Synthetic Approaches to the Development of a Peptide Synthesis with Less Racemization and Simplifier Purification Process

The key intermediate NH₂-Ile-Thr(Bzl)-Asn-Cys(Bzl)-Pro-COOH of Atosiban was prepared from N-Boc-S-Bzl-cysteine by the stepwise lengthening of the chain according to the repetitive N,O-bis(trimethylsilyl)acetamide/N-hydroxysuccinimide ester (BSA/NHS) strategy. This synthetic route required no chromatography purification and can be readily performed, yielding a highly pure pentapeptide compound.     

GDP vs. LDP: A Survey from the Perspective of Information-Theoretic Channel

The existing work has conducted in-depth research and analysis on global differential privacy (GDP) and local differential privacy (LDP) based on information theory. However, the data privacy preserving community does not systematically review and analyze GDP and LDP based on the information-theoretic channel model. To this end, we systematically reviewed GDP and LDP from the perspective of the information-theoretic channel in this survey. First, we presented the privacy threat model under information-theoretic channel. Second, we described and compared the information-theoretic channel models of GDP and LDP. Third, we summarized and analyzed definitions, privacy-utility metrics, properties, and mechanisms of GDP and LDP under their channel models. Finally, we discussed the open problems of GDP and LDP based on different types of information-theoretic channel models according to the above systematic review. Our main contribution provides a systematic survey of channel models, definitions, privacy-utility metrics, properties, and mechanisms for GDP and LDP from the perspective of information-theoretic channel and surveys the differential privacy synthetic data generation application using generative adversarial network and federated learning, respectively. Our work is helpful for systematically understanding the privacy threat model, definitions, privacy-utility metrics, properties, and mechanisms of GDP and LDP from the perspective of information-theoretic channel and promotes in-depth research and analysis of GDP and LDP based on different types of information-theoretic channel models.     

氮掺杂改性二氧化钛光催化剂的研究进展

综述了近年来国内外利用氮掺杂改性二氧化钛的光催化剂性能、提高可见光的利用效率的最新研究进展;分析和讨论了氮掺杂二氧化钛的制备方法、理论计算和结构模型、掺杂机理等;总结了氮掺杂改性二氧化钛存在的问题,同时讨论了今后的研究方向.     

ICP-AES测定Ni-Cr合金在人工唾液中析出的Ni离子

在模拟口腔环境下用人工唾液浸泡Ni-Cr桥,150h后采用ICP-AES测定Ni-Cr桥在人工唾液中的Ni离子析出量.镍在0.01-7.5μg/mL内有良好的线性关系,相关系数为0.9998;方法检出限为0.0059μg/mL;标准加入法测定镍的回收率为92.3%-99.8%.     

热图法测量激光强度时空分布的重构理论研究

为了把量热法应用于远场激光强度时空分布测量,研究了基于热像仪靶面温度测量反演入射激光强度时空分布的重构理论。针对背光面两种不同边界条件(对流-辐射热流边界和恒定温度边界)推导出了由靶面温度分布反演激光束时空分布的重构表达式。获得的分析表达式对广泛的材料具有适用性。通过引入广义参量F0=α/L2,分别就F0》1和F0《1情况给出了重构近似表达式,并对满足F0》1条件的回推算法进行了数值模拟验证。数值结果表明,两种背光面边界条件下回推得到的激光束时空分布与原始激光束达到了很好的一致,但存在一与靶材傅里叶数相关的最小起始回推时间τ0。成果可用于强激光远场参量测量设备的研制。     

低曝光量下投影算法的稳健性研究

研究了在低曝光量情况下灰度投影算法的稳健性,为提出的稳定成像系统的设计与实现提供可行性论证。通过合成视频实验探讨、实际视频实验论证相结合的研究方法,探讨曝光量不足对灰度投影算法性能的影响。实验结果表明,灰度投影算法在欠曝5档和存在一定随机噪声的情况下,仍能保持良好的运动矢量估计性能,从而说明了投影算法在一定的曝光量范围内仍能准确地得到运动矢量估计,是一种运算量小、实时性好且稳健性较强的电子稳像算法。投影算法在低曝光量情况下良好的稳像稳健特性,使其能在低亮度及高实时性要求等环境下应用于航拍、卫星遥感等稳定成像或高清晰成像场合。     

用蒙特卡罗光子追迹方法分析闪光灯的结构设计

闪光灯反光罩结构设计的目标是使得所拍摄视场内的光能量分布尽量均衡。不同于基于几何光学理论的闪光灯计算和设计方法,采用了蒙特卡罗光子追迹法来分析闪光灯的结构设计。通过对照相机闪光灯几何结构的分析,引入余弦随机变量等方法,建立了闪光灯系统中光源、反光罩、菲涅耳透镜等部件的数学模型。先用蒙特卡罗光子追迹法模拟了单光子在闪光灯中飞行的各种可能状态,再通过产生大量光子仿真真实的情况。并对一个具体的闪光灯结构进行了计算,计算得到了光强和光子方向矢量在水平、垂直两个方向的投影角之间的分布曲线图。仿真结果符合设计要求并与实测曲线很接近,从而验证了蒙特卡罗光子追迹法在闪光灯结构设计中的可行性。     

一种多视点视频自动颜色校正系统

针对多视点视频系统中视点间图像颜色不一致的问题,提出了一种多视点视频自动颜色校正系统。通过求取目标图像和源图像间的颜色校正矩阵,判断其是否满足全局校正的要求;对不满足要求的图像,通过图像分割和K-L变换(Karhunen-Loeve transform),建立起目标图像和源图像中各分割区域间的局部映射关系,并通过感兴趣区域匹配,来实现对源图像的校正,最后通过视频跟踪技术实现对视频图像的校正。以标准的多视点测试图像集为例,通过将新方法与直方图匹配、全局一维线性校正算法等进行比较,表明新方法能消除匹配失真的影响,且具有较好的颜色校正效果。研究结果表明该系统可以很好地揭示图像间的颜色变化关系,并且具有很好的内容自适应性,是一种有效的多视点视频图像系统颜色校正方法。     

光纤型宽带可调连续波差频产生中红外激光器

报道一种新型光纤化宽带可调连续波中红外激光器系统,该激光系统采用准相位匹配(QPM)的差频产生(DFG)技术,非线性晶体为多周期的周期性极化掺镁铌酸锂晶体(PPMgLN),掺镱光纤激光器(YDFL)用作抽运光源,可调激光器经掺铒光纤放大器(EDFA)功率提升后作为信号光源。利用建立的准相位匹配-差频产生系统,获得了连续波中红外差频光输出;实验发现,温度导致相位失谐的半峰全宽(FWHM)为4.5℃;通过优化选择晶体周期,并结合调节信号光波长和控制温度,该准相位匹配-差频产生系统可在3.1~3.6μm内连续调谐。     

A PENNY-SHAPED CRACK IN A MAGNETOELECTROELASTIC LAYER UNDER RADIAL SHEAR IMPACT LOADING

This paper analyzes the dynamic magnetoelectroelastic behavior induced by a penny- shaped crack in a magnetoelectroelastic layer.The crack surfaces are subjected to only radial shear impact loading.The Laplace and Hankel transform techniques are employed to reduce the prob- lem to solving a Fredholm integral equation.The dynamic stress intensity factor is obtained and numerically calculated for different layer heights.And the corresponding static solution is given by simple analysis.It is seen that the dynamic stress intensity factor for cracks in a magnetoelec- troelastic layer has the same expression as that in a purely elastic material.And the influences of layer height on both the dynamic and static stress intensity factors are insignificant as h/a>2.