全文获取类型
收费全文 | 11905篇 |
免费 | 1782篇 |
国内免费 | 1619篇 |
专业分类
化学 | 9194篇 |
晶体学 | 168篇 |
力学 | 586篇 |
综合类 | 179篇 |
数学 | 1342篇 |
物理学 | 3837篇 |
出版年
2024年 | 24篇 |
2023年 | 182篇 |
2022年 | 391篇 |
2021年 | 354篇 |
2020年 | 453篇 |
2019年 | 455篇 |
2018年 | 369篇 |
2017年 | 329篇 |
2016年 | 599篇 |
2015年 | 548篇 |
2014年 | 695篇 |
2013年 | 840篇 |
2012年 | 974篇 |
2011年 | 1025篇 |
2010年 | 815篇 |
2009年 | 764篇 |
2008年 | 847篇 |
2007年 | 815篇 |
2006年 | 761篇 |
2005年 | 582篇 |
2004年 | 524篇 |
2003年 | 411篇 |
2002年 | 470篇 |
2001年 | 374篇 |
2000年 | 250篇 |
1999年 | 236篇 |
1998年 | 168篇 |
1997年 | 150篇 |
1996年 | 150篇 |
1995年 | 94篇 |
1994年 | 102篇 |
1993年 | 82篇 |
1992年 | 61篇 |
1991年 | 74篇 |
1990年 | 72篇 |
1989年 | 49篇 |
1988年 | 27篇 |
1987年 | 27篇 |
1986年 | 25篇 |
1985年 | 33篇 |
1984年 | 13篇 |
1983年 | 19篇 |
1982年 | 10篇 |
1981年 | 10篇 |
1980年 | 8篇 |
1978年 | 6篇 |
1974年 | 3篇 |
1973年 | 3篇 |
1969年 | 3篇 |
1928年 | 3篇 |
排序方式: 共有10000条查询结果,搜索用时 15 毫秒
21.
The effect of γ-ray irradiation on the magnetic properties of NdFeB and Fe–Cr–Co permanent magnets has been investigated. The magnetic flux loss of two kinds of magnets before and after irradiation was measured. Results show that the effect of γ-ray irradiation on the magnetic properties of sintered NdFeB is not so obvious as that on Fe–Cr–Co magnet. Irradiation-induced damage from γ-ray for the Fe–Cr–Co magnets was characterized for the first time. The decline of permanent magnetic properties of Fe–Cr–Co magnet induced by γ-ray irradiation is reversible except for the maximum energy product (BH)max. The difference of coercivity mechanism between these two kinds of permanent magnets is responsible for the different dependence of magnetic properties loss induced by γ-ray irradiation. 相似文献
22.
巯基乙酸锑配合物的合成与X射线粉末衍射数据指标化 总被引:2,自引:0,他引:2
一些锑和铋的配合物可以应用于医药研究[1,2 ] ,已合成了许多锑的有机配体配合物[3~ 7] ,但其中大多数没有生物活性。因此 ,研究锑或铋离子的配合物不仅对主族元素化学、生物无机化学而且对医药都有着非常重要的意义。我们用三氯化锑与巯基乙酸液相反应法合成的二巯基乙酸锑 (Ⅲ)配合物 ,其组成为HSb(SCH2 COO) 2 ,用X射线粉末多晶衍射数据指标化来研究配合物晶体结构[8] 。1 实验部分1 1 仪器与试剂EA - 1 1 0 6型元素分析仪 (意大利卡拉欧巴公司制造 ) ,D Max -YB型多晶X射线粉末衍射仪(日本理学 ,CuKα射线 ,… 相似文献
23.
新药交沙霉素能否制成片剂,取决于能否找到最佳的片剂处方.本文运用正交试验法成功地解决了这一问题. 相似文献
24.
Xuefeng Yue Xinliang Lu Yongyuan Song Zongshu Shao Daliang Sun Quanzhong Jiang Huanchu Chen 《Applied physics. B, Lasers and optics》1991,53(5-6):319-322
The use of Cu-doped (K0.5Na0.5)0.2(Sr0.61Ba0.39)0.9Nb2O6 as self-pumped phase conjugators using internal reflection is reported. Reflectivities as high as 63% at 5145.5 nm and 60% at 632.8 nm were realized. It was found that the photorefractive response changes significantly at different doping concentration. The responses of the crystals to the laser wavelength, incident angle and dopant concentration are studied. 相似文献
25.
Mooson Kwauk 《中国颗粒学报》2004,(1)
IntroductionInmaterialscience,differentmicrostructuresofthesamematerialsmayinducediversebehaviorsanddifferentcharacteristics.Westwood(1988)showed,asanexample,thatthetreatmentofaluminumsurfacewithcommercialphosphoricacidproducedmechanicallyinterlockedoxide搘hiskers?approximately10nmindiameterand400nminlength,whichmechanicallyinterlocked.Thismicro-structurecankeepsuchaconglomeratebondedoverconsiderablerangesofstressandtemperature.Inahumidatmosphere,especiallythatcontainingchlorine,however,suchox… 相似文献
26.
Al-Cu-Fe thin films were prepared by laser induced arc (laser-arc) method from a single source—Al63Cu25Fe12 alloy, which was proved to consist of quasicrystalline phase together with approximant phase. The composition of the deposited films meets the requirement for formation of icosahedral symmetry phase. Quasicrystalline phase was obtained after annealing the amorphous as-deposit film samples. The optical properties of the samples were investigated. Thin film samples of Al, Cu and Fe deposited under the same condition were employed for comparison. The results showed specific reflective properties of Al-Cu-Fe quasicrystal thin film in some wavelength range. The optical conductivity of the films exhibited a negative peak, centered about 440 nm in range of 190 to 800 nm. The Al-Cu-Fe quasicrystal thin films could absorb almost all the ray in the wavelength range from 420nm to 450 nm. The ratio of absorption was greater than 99%. 相似文献
27.
Ying‐Ling Liu Chuan‐Shao Wu Yie‐Shun Chiu Wen‐Hsuan Ho 《Journal of polymer science. Part A, Polymer chemistry》2003,41(15):2354-2367
A novel epoxy system was developed through the in situ curing of bisphenol A type epoxy and 4,4′‐diaminodiphenylmethane with the sol–gel reaction of a phosphorus‐containing trimethoxysilane (DOPO–GPTMS), which was prepared from the reaction of 9,10‐dihydro‐9‐oxa‐10‐phosphaphenanthrene‐10‐oxide (DOPO) with 3‐glycidoxypropyltrimethoxysilane (GPTMS). The preparation of DOPO–GPTMS was confirmed with Fourier transform infrared, 1H and 31P NMR, and elemental analysis. The resulting organic–inorganic hybrid epoxy resins exhibited a high glass‐transition temperature (167 °C), good thermal stability over 320 °C, and a high limited oxygen index of 28.5. The synergism of phosphorus and silicon on flame retardance was observed. Moreover, the kinetics of the thermal oxidative degradation of the hybrid epoxy resins were studied. © 2003 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 2354–2367, 2003 相似文献
28.
研究了 2 0 0 0年 MCM— B题 ,将问题推广到有三层干扰的复杂情况 ,给出并严格证明了 ( k,1,1)问题的最优解 相似文献
29.
This paper investigates regression quantiles (RQ) for unstable autoregressive models. The uniform Bahadur representation of the RQ process is obtained. The joint asymptotic distribution of the RQ process is derived in a unified manner for all types of characteristic roots on or outside the unit circle. It involves stochastic integrals in terms of a sequence of independent and identically distributed multivariate Brownian motions with correlated components. The related L-estimator is also discussed. The asymptotic distributions of the RQ and the L-estimator corresponding to the nonstationary componentwise arguments can be transformed into a function of a normal random variable and a sequence of i.i.d. univariate Brownian motions. This is different from the analysis based on the LSE in the literature. As an auxiliary theorem, a weak convergence of a randomly weighted residual empirical process to the stochastic integral of a Kiefer process is established. The results obtained in this paper provide an asymptotic theory for nonstationary time series processes, which can be used to construct robust unit root tests. 相似文献
30.
热喷涂技术的现状和发展 总被引:4,自引:0,他引:4
介绍了热喷涂工艺的特点,喷涂方法的种类及其技术以及热喷涂技术的应用概况,并对热喷涂技术的发展方向给予了展望。 相似文献