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H2S is considered as the main gas pollutant from livestock farm and activated carbon (AC) is widely used as adsorbent for H2S. This paper focuses on the influence of modification conditions and operation conditions on the H2S adsorption performance on AC samples. The H2S adsorption performance on modified AC (MAC) samples by single and combinatory method has been investigated. It is concluded that the MAC by combinatory method of high-pressure hydrothermal method followed by alkaline solution impregnation method could promote the H2S adsorption performance remarkably. The H2S adsorption performance differs with different operation conditions. Meanwhile the samples of fresh AC and exhausted AC have been characterized using BET, FTIR, TPD and Boehm titration method. The experimental results are confirmed that the characteristics of AC have significant influence on the adsorption ability for H2S. 相似文献
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In vivo pharmacokinetics of and tissue distribution study of physalin B after intravenous administration in rats by liquid chromatography with tandem mass spectrometry
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A rapid and sensitive liquid chromatography tandem mass spectrometry quantitative analysis method was established for the pharmacokinetics and tissue distribution study of physalin B in rat. Physalin B and physalin H (internal standard, IS) were separated on an Agilent Eclips XDB C8 column. MS detection was performed on a triple quadrupole tandem mass spectrometer in the multiple reaction monitoring mode with a positive eletrospray ionization source. The assay was validated in the concentration ranges of 22.6–22600 ng/mL for heart and lung and 4.52–4520 ng/mL for other tissues. The intra‐ and inter‐day precisions (RSD) were ≤9.23 and ≤12.51%, respectively, with accuracy (%) in the range of 88.07–113.2%. A pharmacokinetic study showed that physalin B has a long dwell time with a half‐life of 321.2 ± 29.5 min and clearance of 175.4 ± 25.7 mL/min/kg after intravenous administration. Additionally, physalin B showed a wide tissue distribution with a special higher penetration in lung. The data presented in this study could provide useful information for the further study of physalin B. Copyright © 2016 John Wiley & Sons, Ltd. 相似文献
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Wei-Cheng Ding Liang He Hong-Quan Huang Wei-Fu Xu Shu-bin Li Tian He 《Journal of Radioanalytical and Nuclear Chemistry》2017,314(3):1635-1641
Determination of radon concentrations in soil usually requires the accumulation of many measurements over a large area. In this study, an alpha cup technique that provides a cumulative result for adsorption of radon progeny over time was investigated. In addition, the performance of measurements were evaluated. To avoid the impacts of temperature and humidity, a new arithmetic correction was explored. Finally, we also investigated the effect of burial time of the alpha cup on soil radon measurements. Experiments showed that the alpha cup technique can satisfy the demands of soil radon measurements in efficiency, accuracy, reliability, and stability. 相似文献
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Chaotic ant swarm optimization (CASO) is a powerful chaos search algorithm for optimization problems, but it is often easy to be premature convergence. To overcome the weakness, this paper presents a CASO with passive congregation (CASOPC). Passive congregation is one type of biological information sharing mechanisms that allow animals to aggregate into groups and help to enhance the exploitation of animals. By introducing passive congregation strategy into the CASO, a modified evolution equation based on the CASO is proposed in the CASOPC. The modified evolution equation cannot only employ the parallel search of all ants and the well exploration ability of the CASO, but also stress and control the exploitation by passive congregation coefficient c in the stage of evolution. Due to linearly increasing c in the CASOPC, the exploration and exploitation ability of ants are well balanced so that premature convergence can be avoided and good performance can be achieved. In order to estimate the capability of the CASOPC, it is tested with a set of 5 benchmark functions with 30 dimensions and compared to the CASO. Experimental results indicate that the CASOPC improves the search performance on the benchmark functions significantly. 相似文献