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An HPLC method was established and validated for the determination of compound FLZ, a synthetic novel anti-Parkinson's disease candidate drug, in rat plasma. FLZ and the internal standard bicyclol were extracted from plasma by solid-phase extraction method and analyzed on a Restek C18 column (4.6 x 250 mm, 5 microm) with a mobile phase consisting of methanol and water (60:40, v/v) at a flow rate of 1.0 mL/min. The detection wavelength was set at 320 nm. The calibration curve was linear within the concentration range from 25 to 500 ng/mL (r2 > 0.999), the limit of quantitation was 25 ng/mL and the average recovery was 92.0% with the RSD less than 5.9%. The relative standard deviation for intra- and inter-day precision was less than 3.8 and 6.9%, respectively. The established HPLC method was validated to be a simple, rapid and reliable procedure and applied to study the preclinical pharmacokinetics of FLZ in rat plasma, and it was the first time that the pharmacokinetics of FLZ had been investigated. 相似文献
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将实物期权理论引入传统现金流量折现法的应用框架,在不确定性条件下运用实物期权定价法来评估企业价值,提出了简约的Schwartz-Moon(2001)实物期权定价模型,并在此基础上运用蒙特卡罗模拟方法来计算了百度公司的价值. 相似文献
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面对日趋完善的食品接触材料卫生标准体系,为掌握高锰酸钾消耗量测定的技术要求,做好相应合规性判定,充分发挥能力验证对检验检测机构技术能力监督和质量提升的作用,该文进行了食品接触用塑料材料及制品中高锰酸钾消耗量的测定能力验证。通过定制棕色塑料食品包装瓶作为相关能力验证样品,依据相关标准要求进行均匀性、稳定性评价,对回收结果采用稳健统计技术算法A确定指定值和能力评定标准差,并对可能产生不满意结果的影响因素进行了分析。192家参与该项能力验证的实验室中有179家结果为满意,满意率为93.2%;12家实验室结果为不满意,占6.3%;1家实验室结果为可疑,占0.5%。总体结果较好,个别实验室出现的不合格结果可通过本次能力验证分析查找原因,达到提高实验室相应检测能力的目的。 相似文献
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钌离子催化氧化法研究大港减压渣油组分化学结构 总被引:1,自引:0,他引:1
利用钌离子催化氧化方法对大港减压渣油芳香分、胶质和庚烷沥青质进行了选择性降解,通过GC、GC-MS等分析手段对降解反应产物中一元正构脂肪酸、α,ω-二元正构脂肪酸和苯二~六元羧酸的含量和分布分别进行了定量分析。结果表明,芳香分、胶质和庚烷沥青质中的芳香结构上都存在大量烷基取代基和桥接不同芳碳的聚亚甲基桥。烷基取代基碳数最大约为33,聚亚甲基桥最大碳数约为24,而且这两种结构单元的含量均随碳数的增加而减少,并呈现出了偶碳优势。庚烷沥青质C12以下侧链相对较多而C16+较少,与芳香分的分布相反;正构烷基侧链的浓度按庚烷沥青质、胶质和芳香分的顺序递减。降解产物中都检测到了苯二甲酸到苯六甲酸等一系列的苯多酸,表明三个组分中都存在稠环芳香结构。庚烷沥青质中缩合程度较高的迫位缩合结构含量最高,芳香分渺位缩合结构最多,胶质介于两者之间。 相似文献
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采用光纤缠绕方法,对国产大模场面积多模光纤激光器缠绕前后的输出性能进行了对比研究。将光纤激光器输出端在半径为65 mm的圆筒上缠绕两圈后,获得了单横模输出。光纤缠绕前后,激光器的光束质量因子由1.24减小为1.06,斜率效率由64.7%减小为54.3%。当泵浦功率为149 W时,缠绕前后的输出功率分别为94.7 W和79.4 W。虽然缠绕后功率有所减小,但激光亮度增加了15%。同时对实验所用光纤的缠绕损耗进行了理论计算,实验结果与理论计算值符合得较好。 相似文献
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INFLUENCE OF THE DIPOLE-DIPOLE INTERACTION BETWEEN ATOMS ON THE PHASE PROPERTIES OF LIGHT 总被引:2,自引:0,他引:2
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The time evolution and the statistic characteristic of the light phase in the Tavis-Cummings (T-C) model of two identical two-level atoms coupled to a strong coherent light field are studied by means of the Pegg-Barnett phase theory. It is proved that the dipole-dipole interaction between atoms will lead to the frequency shift of light, the weakening of the degree of atom-field coupling and the restraint of light phase diffusion. 相似文献
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