多氯甲基芳烃的合成与表征

以甲苯、乙苯、异丙苯、间二甲苯和均三甲苯为原料,在由路易斯酸、有机酸和无机酸所组成的新型复合催化剂协同催化下,经多氯甲基化反应制备了2,4,6-三(氯甲基)甲苯、2,4,6-三(氯甲基)乙苯、2,4,6-三(氯甲基)异丙苯、2,4,6-三(氯甲基)间二甲苯和2,4,6-三(氯甲基)均三甲苯.利用IR、1H NMR、13C NMR等手段对所合成产物的结构进行了表征,在优化反应条件下,5种产物的收率分别可达 24.5％、31.7％、15.3％、78.1％和89.6％.     

Improved interframe registration based nonuniformity correction for focal plane arrays

In this paper, an improved interframe registration based nonuniformity correction algorithm for focal plane arrays is proposed. The method simultaneously estimates detector parameters and carries out the nonuniformity correction by minimizing the mean square error between the two properly registered image frames. A new masked phase correlation algorithm is introduced to obtain reliable shift estimates in the presence of fixed pattern noise. The use of an outliers exclusion scheme, together with a variable step size strategy, could not only promote the correction precision considerably, but also eliminate ghosting artifacts effectively. The performance of the proposed algorithm is evaluated with clean infrared image sequences with simulated nonuniformity and real pattern noise. We also apply the method to a real-time imaging system to show how effective it is in reducing noise and the ghosting artifacts.     

有限气相反应速率条件下MFF模型应用方法的研究

本文使用CO相对燃烧速率的概念和通用的有效影响参数转化方程,将带有气相反应速率无穷快假设的移动火焰锋面(MFF)模型成功地扩展应用到有限气相反应速率条件的计算中。对于多组不同有限气相反应速率、以及不同粒径的碳粒燃烧计算,MFF模型扩展应用的预报结果都与严格连续膜模型符合较好,碳粒着火温度的预报也更为准确。     

First experimental research of the bunch compressor at CAEP

Magnetic bunch compressor is one of the key technologies on the path to next generation accelerator driven facilities. In this paper we report the design principles and the first experimental research of the bunch compressor developed at Chinese Academy of Engineering Physics （CAEP）. The length of the bunch after compressor is found to be about 0.7 ps （rms） and the peak current exceeds 500 A when operated in the optimized condition. The sensitivity of the bunch length on the phase of the acceleration field and magnetic field of the bunch compressor was also measured and analyzed.     

Low dimensional chaos in the AT and GC skew profiles of DNA sequences

This paper investigates the existence of low-dimensional deterministic chaos in the AT and GC skew profiles of DNA sequences. It has taken DNA sequences from eight organisms as samples. The skew profiles are analysed using continuous wavelet transform and then nonlinear time series methods. The invariant measures of correlation dimension and the largest Lyapunov exponent are calculated. It is demonstrated that the AT and GC skew profiles of these DNA sequences all exhibit low dimensional chaotic behaviour. It suggests that chaotic properties may be ubiquitous in the DNA sequences of all organisms.     

超声波法提取迎春花总黄酮含量的工艺研究

研究了超声波法对迎春花中总黄酮的提取条件。其最优提取条件为:料液比1∶40,超声波温度20℃,作用时间20min。在此条件下,用NaNO2-Al(NO3)3-NaOH显色法测定的总黄酮为18.22%,RSD=1.48%(n=5)。     

自然科学与人文社会科学的异同——科学与人文漫话之四

分析了自然科学与人文社会科学的异同,人文科学与社会科学的联系及区别,并初步讨论了自然科学与人文社会科学的统一问题．     

一种基于信息理论的高动态范围图像评价方法

高动态范围图像(high dynamic range image)指的是扩大了景物可分辨的光照范围的图像。在HDRI成像中动态范围是难以量化测量的,必须将对动态范围的计算转化为其它易于计算的像质评价函数。HDRI图像的像质评价和普通图像的像质评价存在着较大不同。比较了几种像质评价的方法后,提出了利用图像的熵作为标准进行高动态范围成像评价的方法。利用一种自然图像的概率模型对图像的熵与成像动态范围之间的关系进行了数值模拟,得到了具有普遍意义上的理想成像动态范围的计算公式,公式指出了对自然景物完善成像所需的最大动态范围;给出了图像熵与动态范围之间的关系。利用这种关系可以经由计算图像的熵来对系统的动态范围特性做出评价。这种评价方法在指导高动态范围成像系统的设计,以及高动态范围成像系统的测试中将发挥重要的作用。     

Forward and inverse problem for cardiac magnetic field and electric potential using two boundary element methods

This paper discusses the forward and inverse problem for cardiac magnetic fields and electric potentials.A torso-heart model established by boundary element method(BEM) is used for studying the distributions of cardiac magnetic fields and electric potentials.Because node-to-node and triangle-to-triangle BEM can lead to discrepant field distributions,their properties and influences are compared.Then based on constructed torso-heart model and supposed current source functional model-current dipole array,the magnetic and electric imaging by optimal constrained linear inverse method are applied at the same time.Through figure and reconstructing parameter comparison,though the magnetic current dipole array imaging possesses better reconstructing effect,however node-to-node BEM and triangleto-triangle BEM make little difference to magnetic and electric imaging.     

高温超导滤波器两种刻蚀方法的研究

在高温超导滤波器的制备过程中,针对所使用的高温超导薄膜的特点,采用了两种刻蚀方法——湿化学刻蚀法和离子束刻蚀法,设计对比了两种刻蚀的制作流程及其优缺点,并用两种方法分别制备了高温超导滤波器,对微波特性做了对比分析。得出离子束刻蚀对超导薄膜的性能影响要小一些,用此方法制备的高温超导滤波器具有更好的微波特性。