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141.
钾离子选择电极的研究一直是一个非常活跃的题目,具有令人瞩目的发展。本文就其研制、测试法与应用方面的新进展进行评述。 相似文献
142.
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144.
本文在变量选择问题的基础上,提出了一种新的图示模型──减变残差图。并给出它的两种推广形式:均值平移异常值检验图和部分影响诊断图。通过它们不但可以容易地考察一个变量在模型中的作用和检验异常值,而且可以诊断样本点对模型和变量的影响大小。 相似文献
145.
A new porphyrin, peroxyacetic acid uroporphyrin I, has been isolated from the urine of patients with congenital erythropoietic porphyria by reversed phase high performance liquid chromatography. The porphyrin was characterized by high resolution mass spectrometry and by typical chemical reactions of a peroxyacid. 相似文献
146.
This paper tries to introduce the reader to the method of using photochemical re-action to copy holographic optical elements(HOEs)in relief.The holographic blazing gratingso copied is groove depth adjustable phase modulability enlarged through copying and 3.3times the diffraction efficiency(DE)of the original grating.It is expected that the newmethod will lead to the mass production of the light-weight HOEs at low cost. 相似文献
147.
ThefascinatingsbocturesandpropertiesoffullereneshaveoPeneduPanewfieldofchendstry.Inparticular,F.Wudletal.l'2haveshownthatwatersofubleC6ocomPoundsinhibittheHITVen-zymesprotease(HIVP)andreversetranscriPtase(HIVRT).IthasbeenafocusofstUdytoinvestigatethebiologicalactivitiesofthesenovelsubstances.Fortheirpossiblemedicaluses,tolinkC6omoleculetonaturalProductssuchassugars,pephdes,amioacides,andsoonisanimPortantmethodinthisfield.Vasella3reportedthefirstglucosidederivativeofC6o'InthispaPer,w… 相似文献
148.
We reported controllable synthesis of ZnS nanocrystal-polymer transparent hybrids by using polymethylmethacrylate (PMMA) as
a polymer matrix. In a typical run, the appropriate amounts of zinc chloride (ZnCl2) and sodium sulfide (Na2S) in the presence of 2-mercaptoethanol (ME) as the organic ligand were well dispersed in H2O/dimethylformamide solution without any aggregation. In addition, the Mn-doped ZnS nanocrystals (NCs) were synthesized with
similar method. Then, ZnS-PMMA hybrids were obtained via free radical polymerization in situ by using ZnS NCs functionalized
with methacryloxypropyltrimethoxysilane (MPS). FT-IR characterization indicates the formation of robust bonding between ZnS
NCs and the organic ligand. The TEM images show that ZnS NCs are well dispersed in PMMA matrix, and particle size of as-prepared
ZnS NCs is about 2.6 nm, in agreement with the computing results of Brus’s model and Debye–Scherrer formula. The photoluminescence
measurements present that ZnS NCs, Mn-doped ZnS NCs, and ZnS/PMMA hybrid show good optical properties. 相似文献
149.
Yaping Guo 《European Polymer Journal》2007,43(6):2292-2297
Polyaniline (PANI) nanofibers with interconnected network-like structures were electropolymerized on stainless steel substrates by galvanostatic electrolysis. The samples were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV-visible spectroscopy (UV-vis) and Fourier transform infrared spectroscopy (FTIR). The results show that PANI and gels (mixtures of oligomer, dopant and aniline) form simultaneously during the electrochemical deposition. The gels play an important role in the formation of PANI nanofibers. The PANI formed in the early stage of polymerization is subject to secondary growth along one dimension, since the nucleation sites are suppressed by the wrapped gels. The dendritic degree of PANI nanofibers is related to dopants, and the order is as follows: PANI-H3PO4 > PANI-H2SO4 > PANI-HNO3. No nanofibers are obtained using CH3COOH as dopants due to the high solubility of PANI-CH3COOH. 相似文献
150.
An interval-parameter fuzzy linear programming method (IFMOLP) is proposed in this study for multiple objective decision-making
under uncertainty. As a hybrid of interval-parameter and fuzzy methodologies, the IFMOLP incorporates interval-parameter linear
programming and fuzzy multiobjective programming approaches to form an integrated optimization system. The method inherits
advantages of interval-parameter programming, and allows uncertainties and decision-makers’ aspirations to be effectively
communicated into its programming processes and resulting solutions. Membership functions for both objectives and constraints
are formulated to reflect uncertainties in different system components and their interrelationships. An interactive solution
procedure has been developed based on solution approaches of the interval-parameter and fuzzy programming techniques, plus
necessary measures for handling the multiobjective feature. A didactic example is provided in the paper to illustrate the
detailed solution process. Possibilities of further improvements by seeking Pareto optimum and incorporating flexible preference
within constraints are also discussed. 相似文献