火焰原子吸收分光光度法测定五氧化二钒中铁及氧化钾、氧化钠含量

五氧化二钒样品用盐酸分解,在稀盐酸介质中,用原子吸收分光光度计分别于248.3,766.5,589.0 nm波长处,使用空气–乙炔火焰,测量五氧化二钒中铁及氧化钾、氧化钠含量。在最佳实验条件下,铁、氧化钾、氧化钠的质量浓度分别在0.05~0.20,0.05~0.80,0.20~1.0 mg/L范围内与吸光度线性关系良好,相关系数分别为0.998 6,0.994 3,0.994 2。方法检出限铁为6.7μg/L,氧化钾为1.0μg/L,氧化钠为1.4μg/L,加标回收率为95.9%~103.0%。铁、氧化钾、氧化钠测定结果的相对标准偏差分别为3.2%,4.2%,2.9%(n=6)。该方法适合五氧化二钒中铁及氧化钾、氧化钠的测定。     

Linear maps on operator algebras that preserve elements annihilated by a polynomial

In this paper some purely algebraic results are given concerning linear maps on algebras which preserve elements annihilated by a polynomial of degree greater than 1 and with no repeated roots and applied to linear maps on operator algebras such as standard operator algebras, von Neumann algebras and Banach algebras. Several results are obtained that characterize such linear maps in terms of homomorphisms, anti-homomorphisms, or, at least, Jordan homomorphisms.

     

K-POTENT PRESERVING LINEAR MAPS

Let B(X) be the Banach algebra of all bounded linear operators on a complex Banach space X. Let k ≥ 2 be an integer and φ a weakly continuous linear surjective map from B(X) into itself. It is shown that φ is k-potent preserving if and only if it is k-th-power preserving, and in turn, if and only if it is either an automorphism or an antiautomorphism on B(X) multiplied by a complex number λ satisfying λk-1= 1. Let A be a von Neumann algebra and B be a Banach algebra, it is also shown that a bounded surjective linear map from A onto B is k-potent preserving if and only if it is a Jordan homomorphism multiplied by an invertible element with (k - l)-th power I.     

Saddle point and exact penalty representation for generalized proximal Lagrangians

In this paper, we introduce a generalized proximal Lagrangian function for the constrained nonlinear programming problem and discuss existence of its saddle points. In particular, the local saddle point is obtained by using the second-order sufficient conditions, and the global saddle point is given without requiring compactness of constraint set and uniqueness of the optimal solution. Finally, we establish equivalent relationship between global saddle points and exact penalty representations.     

用于短波段发光二极管的二维光子晶体禁带研究

运用平面波展开法(PWE),针对光子晶体在短波长段发光二极管(LED)领域上的应用,主要选择高频禁带模式,研究了4种具有较大应用潜力的二维光子晶体结构,包括正方空气柱结构、三角空气柱结构、正方介质柱结构和三角介质柱结构。在不同晶格常数、占空比(AFF)、柱半径和晶格常数比下,分析了TE模式和TM模式光子禁带的变化。数据分析表明,光子禁带中心波长随AFF增加而变小。相比于其他结构,正方介质柱结构更适于短波段光子晶体LED来提高其出光效率,三角介质柱结构和三角空气柱结构适合用于构造短波段偏振光LED。     

含幂等元的环上的Jordan导子的刻画-在零点Jordan可导的可加映射

设A为包含非平凡幂等元且有单位的环(或代数),δ:A→A是可加(或线性)映射.称δ在零点Jordan可导,若δ(A)B+Aδ(B)+δ(B)A+Bδ(A)=0对任意满足AB+BA=0的A,B∈A成立.在一定条件下,证明了δ在零点Jordan可导当且仪当存在可加Jordan导子τ,使得δ(A)=τ(A)+δ(I)A对任意的A∈A成立.利用此结论,完全刻画了因子von Neumann代数上在零点Jordan可导的可加映射.此外,还刻画了一般von Neumann代数和C*代数上在零点Jordan可导的有界线性映射.     

聚氧化烯烃脂肪酸乙醇酰胺磺基琥珀酸单酯二钠的表面活性

聚氧化烯烃脂肪酸乙醇酰胺磺基琥珀酸单酯二钠的表面活性吴金川＊庄燕何志敏屠雨恩（天津大学化学工程研究所天津３０００７２）关键词聚氧化烯烃脂肪酸乙醇酰胺磺基琥珀酸单酯二钠，表面活性，临界胶束浓度，润湿力，起泡力，乳液稳定性１９９７－０２－２８收稿，１９９...