Antibacterial activity of agave fructans against salmonella typhimurium

Abstract

The objective of this study was to evaluate the antimicrobial effect of Agave fructans against the Salmonella Typhimurium in “in vitro” experiments. The result of the antimicrobial activity was 263.89?±?0, 414.95?±?12.83, 494.54?±?13.88, 522.29?±?0, 580.41?±?14.92?AU for 10, 20, 30, 40 and 50% of Agave fructans (AF) respectively. In addition, there is a significant effect on the growth of the bacteria with all the percentages of AF evaluated (p?<?0.001, R2?=?0.859) with respect to the control. The growth rate of Salmonella with 25% AF was statistically significant compared to the control (?0.7353?±?0.586, 0.0079?±?0.002?D.O./h, respectively; p?>?0.01). Agave fructans could be an alternative to prevent the infections caused by Salmonella.     

Group Rings Whose Symmetric Units are Solvable

Let K be an infinite field of characteristic different from 2, and G a group. Under suitable restrictions upon G, we classify the groups such that the symmetric units of KG satisfy the solvability identity (x ₁, x ₂,…, x _{2 ⁿ} ) ^o  = 1, for some n.     

Univalent Functions, <Emphasis Type="Italic">VMOA</Emphasis> and Related Spaces

This paper is concerned mainly with the logarithmic Bloch space ℬ_log which consists of those functions f which are analytic in the unit disc \mathbbD{\mathbb{D}} and satisfy sup_{|z| < 1}(1-|z|)log\frac11-|z||f^￠(z)| < ￥\sup_{\vert z\vert <1}(1-\vert z\vert )\log\frac{1}{1-\vert z\vert}\vert f^{\prime}(z)\vert <\infty , and the analytic Besov spaces B ^p , 1≤p<∞. They are all subspaces of the space VMOA. We study the relation between these spaces, paying special attention to the membership of univalent functions in them. We give explicit examples of:

Different Faces of the Shearlet Group

Recently, shearlet groups have received much attention in connection with shearlet transforms applied for orientation sensitive image analysis and restoration. The square integrable representations of the shearlet groups provide not only the basis for the shearlet transforms but also for a very natural definition of scales of smoothness spaces, called shearlet coorbit spaces. The aim of this paper is twofold: first we discover isomorphisms between shearlet groups and other well-known groups, namely extended Heisenberg groups and subgroups of the symplectic group. Interestingly, the connected shearlet group with positive dilations has an isomorphic copy in the symplectic group, while this is not true for the full shearlet group with all nonzero dilations. Indeed we prove the general result that there exist, up to adjoint action of the symplectic group, only one embedding of the extended Heisenberg algebra into the Lie algebra of the symplectic group. Having understood the various group isomorphisms it is natural to ask for the relations between coorbit spaces of isomorphic groups with equivalent representations. These connections are examined in the second part of the paper. We describe how isomorphic groups with equivalent representations lead to isomorphic coorbit spaces. In particular we apply this result to square integrable representations of the connected shearlet groups and metaplectic representations of subgroups of the symplectic group. This implies the definition of metaplectic coorbit spaces. Besides the usual full and connected shearlet groups we also deal with Toeplitz shearlet groups.     

Orlicz function spaces without complemented copies ofl p

This paper proves the existence of Orlicz function spaces Lφ (0, 1) containing no complemented subspaces isomorphic tol ^p for anyp ≠ 2. Some properties of minimal Orlicz function spaces Lφ (0, 1) are also given. Supported in part by CAICYT grant 0338-84.     

An unexpected Pummerer rearrangement in the synthetic route to ethyl (2′-hydroxy-4′,5′-methylenedioxyphenyl)acetate: An alternative approach to 2,3-dimethylthio benzofurans

The synthesis of ethyl (2′-hydroxy-4′,5′-methylendioxophenyl)acetate, a fragment of the antihyperglycemic natural coumarin subcoriacin, is reported. We found an expeditious route to the title compound in five steps. Final metal catalyzed acid ethanolysis of the vinylic 1,1-methylthio methylsulfoxide derivative afforded the required aryl acetic ester, but in the absence of metal catalyst, an unexpected Pummerer rearrangement produced the 2,3-dimethylthiofuran derivative as the major product. This last result provides an alternative entry to 2,3-dimethlythiobenzofurans.     

Compositional and electrical properties of Cr,Nb, Cr/Nb,CrNbN, and CrN/NbN multilayers grown using the d.c. magnetron sputtering technique

Cr, Nb, Cr/Nb, CrN_x, NbN_x, CrNbN, and (CrN/NbN)_n structures were produced on Si and glass substrates, using the d.c. magnetron sputtering technique. Compositional analysis, based on binding energies of Cr, Nb, and N, was carried out by means of X-ray photoelectron spectroscopy (XPS). Through Auger electron spectroscopy (AES), depth profiles were obtained, allowing to demonstrate the multilayers production. Surface morphological characteristics, as roughness and grain size, were evaluated by atomic force microscopy (AFM), revealing very smooth surfaces, that is a consequence of the deposition parameters used in the synthetization experiments. Finally, for different configurations, conductivity measurements were carried out, revealing the influence of nitrogen content and temperature on electron transport. It was found that substoichiometric nitrides (CrN_0.35 and NbN_0.12) exhibited the highest conductivity, because the nitrogen atoms act as donor of electrons.     

Studies of proteasome inhibition and apoptosis induction in triple‐negative breast cancer cells by novel amino acid–polypyridine–copper complex

An innovative ternary copper(II) complex, [Cu(Cl‐PIP)(Tyr)Cl]_n, has been synthesized and characterized using infrared spectroscopy, elemental analysis and single‐crystal X‐ray diffraction analysis. X‐ray crystallography indicates that the Cu atom is five‐coordinated in a square‐pyramidal configuration. The unit forms a one‐dimensional chain along the crystallographic c‐axis. The complex was screened for cytotoxicity against a panel of eight human cancer cell lines, namely MDA‐MB‐231, CAL‐51, K562, HeLa, SGC‐7901, A549, MCF‐7 and SMMC‐7721. The best anticancer activity was obtained with triple‐negative breast cancer CAL‐51 and MDA‐MB‐231 cell lines, with IC₅₀ values in the range 0.035–0.10 μM, and this was better than using carboplatin. The complex inhibits proteasomal chymotrypsin‐like activity, and docking studies reveal its interaction with 20S proteasome. In addition, the complex causes accumulation of ubiquitinated proteins, induces apoptosis and inhibits cell proliferation, indicating its great potential as a novel therapy for triple‐negative breast cancer.     

Trace level vanadium determination using thermal lens spectrophotometry

Trace level vanadium determination is reported using a dual beam thermal lens spectrometer. The thermal lens was generated using an argon ion beam laser (pump beam) which was focused into a sample cuvette. The thermal lens signal (TLs) was monitored with a He-Ne laser beam and a photodiode detector. Multichannel averager software was developed for processing the transient TLs. The optimal set up, ensuring maximum sensitivity and linear calibration graphs was obtained using experimental design techniques. Under optimized conditions, the detection limits for aqueous and ethanol-water (2+3 v/v) and (4+1 v/v) vanadium complex solutions were, respectively, 0.0071 mg/l, 0.0065 and 0.0039 mg/l.     

Liquid chromatographic separation of fluoroquinolone antibacterials used as veterinary drugs

Summary A liquid chromatographic method has been developed to separate a series of quinolones which are widely used as veterinary drugs: danofloxacin, difloxacin, enrofloxacin (and its metabolite ciprofloxacin), marbofloxacin, norfloxacin and sarafloxacin. Separation was performed by using an end-capped high-purity silica-based C₈ column and a mobile phase consisting of acetonitrile-aqueous oxalic acid buffer solution. In order to establish the optimal conditions for an isocratic separation, a three-factor Doehlert experimental design was applied. Gradient elution was applied which reduced analysis time. Figures of merit of the method proposed, with fluorimetric detection, were evaluated.