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91.
Haihong Fang Binyuan Hu Lingshen Wang Rongli Lu Cui Yang 《Frontiers of Chemistry in China》2008,3(2):193-197
Nanometer MgO was prepared via a sol-gel auto-combustion technique using magnesium nitrate as raw material and citric acid
as chelating agent. IR spectra of the dried gel were used to investigate the structure of the precursors. By studying the
different TG curves of magnesium citrate gel prepared by different methods, we found that a combustion process occurred and
the nitrate ions acted as an oxidant in the combustion process. TEM photographs of synthesized powders from the sol-gel auto-combustion
showed that the crystallites were uniform in size. In addition, the XRD pattern of this sample showed that the particle size
was 8.9 nm. The BET curves, in turn, showed that the specific surface of the sample was 26.34 m2/g. The mechanism of the frothing process in restraining agglomeration is discussed.
__________
Translated from Journal of East China Normal University (Natural Science), 2007, (2): 52–57 [译自: 华东师范大学学报(自然科学版)] 相似文献
92.
Frictionless indentation responses of transversely isotropic piezoelectric film/rigid substrate systems under circular cylindrical indenter (i.e., punch), conical indenter (i.e., cone), and spherical indenter (i.e., sphere) are investigated. Both insulating and conducting indenters are considered. The technique of Hankel transformation is employed to derive the corresponding dual integral equations for the mixed boundary value indentation problems. For the two limiting cases of infinitely thick and infinitely thin piezoelectric films, closed-form solutions are obtained. For piezoelectric films of finite thickness, a numerical method is constructed to solve the dual integral equations and semi-empirical models having only two unknown parameters are proposed for the responses of indentation force, electric charge and electric potential, and contact radius. With the two parameters inferred from the numerical results, the semi-empirical formulae are found to provide good estimates of the indentation responses for the two limiting cases of infinitely thick and thin piezoelectric films, as well as those in between. The inferred parameters in the proposed semi-empirical formulae for normalized indentation force and electric charge are checked against four different piezoelectric materials and are found to be insensitive to the selection of piezoelectric materials. It is believed that the proposed semi-empirical indentation formulae are useful in developing experimental indentation techniques to extract the material properties of piezoelectric films. 相似文献
93.
94.
X. S. Wu Xuehai Wu Yunping Li Zhangde Lu Liangen Gong Ping Zhou Qing Zhang 《Fiber and Integrated Optics》1993,12(1):97-103
Miniature, etching ridge InGaAsP/InP Phase Modulator with highly efficient phase shifting efficiency of 60°/V.mm and 43°/V.mm for TE and TM modes, respectively, and 3 dB bandwidth of 650 MHz at 1.52 μm are reported. It is well suited for integrated opto-electronics. Some functions depending on bandwidth of the devices are discussed. 相似文献
95.
北京同步辐射装置3B1B生物光谱实验站 总被引:1,自引:0,他引:1
本文介绍北京同步辐射装置(BSRF)3B1B光束线、生物光谱实验站和圆二色谱仪的基本情况。报道北京正负电子对撞机(BEPC)同步辐射专用光期间,我们在站测量了11种手征性生物和药物样品的圆二色(CD)谱,首次在国内利用同步辐射光获取了D-苯丙氨酸等样品的CD谱和D-及L-亮氨酸对称的CD曲线。 相似文献
96.
Jiang-Hua Lu 《Communications in Mathematical Physics》1993,157(2):389-404
We introduce the notion of moment maps for quantum groups acting on their module algebras. When the module algebras are quantizations of Poisson manifolds, we prove that the construction at the quantum level is a quantization of that at the semi-classical level. We also prove that the corresponding smashed product algebras are quantizations of the semi-direct product Poisson structures.Research partially supported by NSF grant DMS-89-07710 相似文献
97.
Lu KangAlison R. Keimowitz Michaeleen R. MunrowStewart E. Novick 《Journal of Molecular Spectroscopy》2002,213(2):122-129
The rotational spectra of the argon acetone weakly bound complex was studied by pulsed jet Fabry-Perot Fourier transform microwave spectroscopy. Over 500 transitions of the complex were measured between 5.5 and 26 GHz from J=2-1 to J=12-11. The two methyl groups undergo hindered internal rotation resulting in four or five internal rotation states. The microwave transitions are within these states, resulting in a splitting of each rotational transition into four and sometimes five distinct transitions. The three-fold barrier to internal rotation is determined to be 260 cm−1, 2% less than the 266 cm−1 barrier in acetone itself. The structure of the complex has the argon atom above the heavy atom plane of the acetone, 3.52 Å from the CO bond and approximately in the Cs plane, which is perpendicular to the CCC plane of acetone. 相似文献
98.
99.
Binglin Lu 《Journal of statistical physics》1987,49(3-4):669-684
The coagulation equation with kernelK
ij
=A+B(i+j)+C
ij and arbitrary initial conditions is studied analytically and a simple expression for the solution is found. For monodisperse initial conditions, we recover the known size distribution expressed in terms of a degeneracy factorN
k, which is determined by a recursion relation. For polydisperse initial conditions, a similar solution form is found, which includes a degeneracy factorN
kl, also determined by a recursion relation. The physical meaning ofN
kl and the recursion relation is given. A method to get explicit expressions forN
k andN
kl is illustrated. Finally, the pre-gel solution is given explicitly and a general method to get the post-gel solution is proposed. 相似文献
100.
D. W. Taylor V. Villas-Boas Q. Lu M. F. Rossignol F. P. Missell D. Givord S. Hirosawa 《Journal of magnetism and magnetic materials》1994,130(1-3):225-236
We studied the coercivity in magnets of composition R17Fe83−χBχ (R = Nd, Pr and χ = 8, 30), using measurements of the coercive field Hc, its angular dependence, and the magnetic viscosity coefficient Sv, for temperatures between 4.2 and 500 K. The results are discussed in relation to a model which does not specifically consider the detailed mechanisms involved in magnetization reversal, but which provides information about the magnetic properties in the activation volume v where magnetization reversal is initiated. It is concluded that the ordering temperature in v tends to be slightly smaller than in the bulk and that the room temperature anisotropy in v is not strongly reduced with respect to the bulk value. Finally, a direct evaluation of the dipolar interactions is in good agreement with results obtained from Hc(T). 相似文献