聚氨酯泡沫低温下平均线膨胀系数的测定

使用相对比较法对聚氨酯泡沫从液氮温度到室温的平均线膨胀系数进行了测试。采用的试验装置具有微机自动测温系统、抽真空系统以及电加热系统 ,保证了测试的准确性。结果表明 :聚氨酯泡沫具有非常低的平均线膨胀系数 ,在平行与垂直发泡方向的膨胀性能差异不大。最后对试验进行了误差分析 ,得到最大相对误差为 8%。     

低温液体管路输送中几个问题的分析

对低温液体传输过程中气体置换、预冷过程、竖直管道中间歇泉现象、盲支管填充时和阀门开启时的不稳定现象作了较详细分析,指出了其可能造成的危害,并提出了相应的解决方法。     

A TRILAYER DERMAL EQUIVALENT CONTAINING SILVER NANOPARTICLES WITH ENHANCED ANTIBACTERIAL PROPERTY

A dermal equivalent having a trilayered structure was designed by combining a silver nanoparticles incorporated chitosan film with a bilayer collagen-chitosan/silicon membrane dermal equivalent(BDE).The silver nanoparticles prepared at different conditions were characterized by UV-Vis and transmission electron microscopy(TEM).The macroscopic sharp and the microstructure of the trilayer dermal equivalent(TDE) were also studied.Then,the in vitro antibacterial property of TDE was evaluated by the antibacter...     

Vibrational CD spectroscopy as a powerful tool for stereochemical study of cyclophynes in solution

Stereochemical study of cyclophynes, which is otherwise rather difficult to perform, can be achieved by vibrational CD spectroscopy.     

Polyelectrolyte Coated PLGA Nanoparticles: Templation and Release Behavior

Poly[(D ,L ‐lactide)‐co‐glycolide] nanoparticles coated with polyethyleneimine on their surface were prepared by an emulsification‐solvent evaporation method and subsequently surface modified by LBL assembly. The assembly of poly(acrylic acid) and polyethyleneimine on a planar substrate and on the PLGA nanoparticles was monitored by QCM‐D, ζ‐potential, flow cytometry and TEM. Carboxylic and amino groups in the multilayers were crosslinked by carbodiimide condensation, which was also later used to graft poly(ethylene glycol) (PEG). Rhodamine 6G, 5(6)‐carboxyfluorescein and fluorescein were incorporated into the nanoparticles and their release profiles were recorded at 60 °C and at 37 °C for rhodamine 6G, for nanoparticles with a multilayer coating, and those that were crosslinked and grafted with PEG.

     

Large-Eddy Simulation of the Flow Over a Circular Cylinder at Reynolds Number 3900 Using the OpenFOAM Toolbox

The flow over a circular cylinder at Reynolds number 3900 and Mach number 0.2 was predicted numerically using the technique of large-eddy simulation. The computations were carried out with an O-type curvilinear grid of size of 300 × 300 × 64. The numerical simulations were performed using a second-order finite-volume method with central-difference schemes for the approximation of convective terms. A conventional Smagorinsky and a dynamic k-equation eddy viscosity sub-grid scale models were applied. The integration time interval for data sampling was extended up to 150 vortex shedding periods for the purpose of obtaining a fully converged mean flow field. The present numerical results were found to be in good agreement with existing experimental data and previously obtained large-eddy simulation results. This gives an indication on the adequacy and accuracy of the selected large-eddy simulation technique implemented in the OpenFOAM toolbox.     

火花通道长度对激光触发开关特性的影响

利用超高速相机,在曝光时间100 ns时,对不同能量下激光在氮气气体开关中形成的火花通道进行拍照,得到了不同焦距下激光波长266 nm时激光火花通道长度与激光能量的关系。开展了激光触发气体火花开关的实验研究,激光触发开关延时、抖动随激光能量的增加而减小。将火花通道长度与激光触发开关的特性进行了分析,气体开关的抖动随着激光火花通道长度的增加而减小,当火花通道沿电极间轴向长度达到开关电极间距40%时,开关的抖动为亚ns量级。     

苯基荧光酮-十六烷基三甲基溴化铵分光光度法测定芦荟中痕量锗

在混合掩蔽剂盐酸羟胺和抗坏血酸混合液存在下,锗与苯基荧光酮和十六烷基三甲基溴化铵生成三元橙红色络合物。锗浓度在1.0-1.5μg/25mL范围内符合比耳定律。此法用于测定芦荟中的痕量锗,获得较为满意的结果。     

Flip-chip-type high-Tc gradiometer for biomagnetic measurements in unshielded environment

A flip-chip-type gradiometer has been constructed with a 10 mm×5 mm planar DC-SQUID gradiometer fabricated on a SrTiO3 bicrystal substrate and a flux transformer made from a YBCO*/YBCO/CeO2/YSZ multilayer on a φ50.8 mm Si wafer. The coupling coefficient between the flux transformer and the planar gradiometer is 0.18. The transformer increases effectively the resolution of the gradiometer. A magnetic field gradient resolution of 73 fT·cm-1·Hz-1/2 in the white region and 596 fT·cm-1Hz-1/2 at 1 Hz has been obtained. High quality magnetocardiogram signals have been successfully measured by using this flip-chip-type gradiometer in an unshielded environment.     

锗元素测定方法综述

锗在国防工业、航空航天和通信等领域中的战略性,锗含量的测定对于保证材料质量和满足国际标准至关重要。本文综述了锗含量测定方法的多种技术,包括分光光度法、原子荧光光谱法、原子吸收光谱法、电感耦合等离子体原子发射光谱法、电感耦合等离子体质谱法以及滴定法。在每个检测方法的介绍中,详细探讨了方法的原理、前处理步骤以及应用范围,并分别总结了各个方法的优势和不足。最后,强调了锗含量测定方法的意义,特别是在满足出口监管和促进科学研究方面的作用。同时对锗元素的测定方法进行了展望,为未来的发展提供了参考方向。