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21.
The interface thermal contact resistance between the copper and stainless steel thin disk is investigated using the non-contact
photo-thermal technique. The diffusivity and the interface thermal contact resistance were estimated using the phase sensitivity
measurement over a temperature range from 20 to 300 K, at 1.20, 2.38 and 4.28 MPa contact pressure, respectively. Results
show that the interface thermal contact resistance decreases with the rise of the temperature and contact pressure. 相似文献
22.
考虑双层碳纳米管的层间范德华力,采用连续介质力学的波动理论,建立了双层碳纳米管中周向导波传播模型,研究周向导波的频散现象.通过与单层碳纳米管结果的比较表明,双层碳纳米管中周向导波的传播表现出更为明显的频散特性,出现更多的模态干涉现象,并发现在某些特殊频率处出现成对模态的消失与新启现象. 相似文献
23.
The successive projections algorithm (SPA) is widely used to select variables for multiple linear regression (MLR) modeling. However, SPA used only once may not obtain all the useful information of the full spectra, because the number of selected variables cannot exceed the number of calibration samples in the SPA algorithm. Therefore, the SPA-MLR method risks the loss of useful information. To make a full use of the useful information in the spectra, a new method named “consensus SPA-MLR” (C-SPA-MLR) is proposed herein. This method is the combination of consensus strategy and SPA-MLR method. In the C-SPA-MLR method, SPA-MLR is used to construct member models with different subsets of variables, which are selected from the remaining variables iteratively. A consensus prediction is obtained by combining the predictions of the member models. The proposed method is evaluated by analyzing the near infrared (NIR) spectra of corn and diesel. The results of C-SPA-MLR method showed a better prediction performance compared with the SPA-MLR and full-spectra PLS methods. Moreover, these results could serve as a reference for combination the consensus strategy and other variable selection methods when analyzing NIR spectra and other spectroscopic techniques. 相似文献
24.
An Efficient Synthesis of Pyrido[2,3‐d][6,5‐d]dipyrimidine and 5,5′‐Arylmethylenebis(2,6‐diaminopyrimidinone) Derivatives under Microwave Irradiation
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Zhilan Lin Huiling Hu Xinkui You Xueli Zhang Yuan Gao 《Journal of heterocyclic chemistry》2014,51(1):277-281
A series of pyrido[2,3‐d][6,5‐d]dipyrimidine and 5,5′‐arylmethylenebis(2,6‐diaminopyrimidinone) derivatives have been synthesized through a rapid reaction of aromatic aldehydes with aminopyrimidines in acetic acid under microwave irradiation. This method has the advantages of simple operation, high yields, short reaction time, and easy work‐up. 相似文献
25.
Suarez AI Jiang H Zhang XP de Bruin B 《Dalton transactions (Cambridge, England : 2003)》2011,40(21):5697-5705
The mechanism of cobalt(II) porphyrin-mediated aziridination of styrene with PhSO(2)N(3) was studied by means of DFT calculations. The computations clearly indicate the involvement of a cobalt 'nitrene radical' intermediate in the Co(II)(por)-catalyzed alkene aziridination. The addition of styrene to this species proceeds in a stepwise fashion via radical addition of the 'nitrene radical'C to the C=C double bond of styrene to form a γ-alkyl radical intermediate D. The thus formed tri-radical species D easily collapses in an almost barrierless ring closure reaction (TS3) to form the aziridine, thereby regenerating the cobalt(II) porphyrin catalyst. The radical addition of the 'nitrene radical'C to the olefin (TS2) proceeds with a comparable barrier as its formation (TS1), thus providing a good explanation for the first order kinetics in both substrates and the catalyst observed experimentally. Formation of C is clearly accelerated by stabilization of C and TS1 via hydrogen bonding between the S=O and N-H units. The computed radical-type mechanism agrees well with all available mechanistic and kinetic information. The computed free energy profile readily explains the superior performance of the Co(II)(porAmide) system with H-bond donor functionalities over the non-functionalized Co(TPP). 相似文献
26.
27.
本文证明了当2-(v,k,1)设计的自同构群G的基柱soc(G)=2F4(q2)时,Buekenhaut-Delandtsheer-Doyen猜想成立,即自同构群G的基柱为Ree群2F4(q2)的区本原2-(v,k,1)设计必为点本原的. 相似文献
28.
Let F be a family of holomorphic functions in a domain D, and let a(z), b(z) be two holomorphic functions in D such that a(z)?b(z), and a(z)?a′(z) or b(z)?b′(z). In this paper, we prove that: if, for each f∈F, f(z)−a(z) and f(z)−b(z) have no common zeros, f′(z)=a(z) whenever f(z)=a(z), and f′(z)=b(z) whenever f(z)=b(z) in D, then F is normal in D. This result improves and generalizes the classical Montel's normality criterion, and the related results of Pang, Fang and the first author. Some examples are given to show the sharpness of our result. 相似文献
29.
Uniform blow-up profiles and boundary layer for a parabolic system with localized nonlinear reaction terms 总被引:3,自引:0,他引:3
LI Huiling & WANG Mingxin Department of Mathematics Southeast University Nanjing China Department of Mathematics Xuzhou Normal University Xuzhou China 《中国科学A辑(英文版)》2005,48(2):185-197
This paper deals with the blow-up properties of the solution to a semilin-ear parabolic system with localized nonlinear reaction terms, subject to the null Dirichlet boundary condition. We first give sufficient conditions for that the classical solution blows up in the finite time, secondly give necessary conditions and a sufficient condition for that two components blow up simultaneously, and then obtain the uniform blow-up profiles in the interior. Finally we describe the asymptotic behavior of the blow-up solution in the boundary layer. 相似文献
30.