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排序方式: 共有126条查询结果,搜索用时 15 毫秒
41.
Jiang Yanxiao Ma Pinyi Piao Huilan Qin Zucheng Tao Shuo Sun Ying Wang Xinghua Song Daqian 《Mikrochimica acta》2019,186(11):1-10
Microchimica Acta - A nanostructure was prepared from titania nanoparticles and copper oxide (TiO2NP@CuO) and used to modify a carbon paste electrode (CPE). The modified CPE is shown to enable... 相似文献
42.
Direct coupling of haloquinolines and sulfonyl chlorides leading to sulfonylated quinolines in water
Pengli Bao Leilei Wang Qishun Liu Daoshan Yang Hua Wang Xiaohui Zhao Huilan Yue Wei Wei 《Tetrahedron letters》2019,60(3):214-218
A simple and efficient method has been developed for construction of sulfonylated quinolines via coupling of haloquinolines and sulfonyl chlorides in water. The present methodology provides an attractive approach to various sulfonylated quinolines in moderate to good yields with favorable functional group tolerance, which has the advantages of operation simplicity, readily available starting materials, excellent regioselectivity, scale-up synthesis, and organic solvent-free conditions. 相似文献
43.
A new coenzyme B12 (AdoCbl) analogue, 3'-deoxy-2',3'-didehydrothymidylcobalamin (2',3'-anThyCbl) was prepared by the reaction of 5'-iodo-3'-deoxy-2',3'-dihydrothmidine with reduced B12a, and characterized by UV-Vis, CD, ESI-MS and NMR spectroscopies. Its axial base (dbzm) coordination equilibria with pH's and temperatures were investigated and showed similar features to those of coenzyme B12. Photolytic dynamics studies under homolytic and heterolytic conditions demonstrated that the Co-C bond of the analogue is slightly more photolabile relative to coenzyme B12. 相似文献
44.
Bergeron and Li have introduced a set of axioms which guarantee that the Grothendieck groups of a tower of algebras $\bigoplus_{n\ge0}A_n$ can be a pair of graded dual Hopf algebras. Hivert and Nzeutchap, and independently Lam and Shimozono constructed dual graded graphs from primitive elements in Hopf algebras. In this paper we apply the composition of these constructions to towers of algebras. We show that if a tower $\bigoplus_{n\ge0}A_n$ gives rise to a pair of graded dual Hopf algebras, then $\dim(A_n)=r^nn!$ where $r = \dim(A_1)$ . In the case of r?=?1 we give a conjectural classification. We then investigate a quantum version of the main theorem. We conclude with some open problems and a categorification of these constructions. 相似文献
45.
We propose a diode end-pumped passively mode-locked Nd: Gd0.42 Y0.58 VO4 (Nd: GdYVO4) laser at 1064nm using a GaAs absorber grown at low temperature as the output coupler.Stable continuous-wave (CW) mode locking with a 5.1-ps pulse duration at a repetition rate of 113MHz is obtained.The maximum average output power is 2.29W at the incident pump power of 12W with the slope efficiency of about 24.8%. 相似文献
46.
In this paper, a linear and adaptive feedback pinning strategy is used to study the lag synchronization of complex dynamical networks with known state time-delay and unknown channel time-delay. Firstly, based on the Lyapunov stability theory, a novel Lyapunov functional, which involves the estimated error \(\hat{e}_{i}(t)\) rather than the general synchronization error \(e_{i}(t)\), is constructed. Secondly, in view of the unknown information of the channel time-delay, two available pinning controllers are designed such that the considered networks achieve lag synchronization. Furthermore, by a proper adaptation mechanism, we estimate the unknown channel time-delay successfully under the case that the initial value of the estimated channel time-delay is larger than true channel time-delay, i.e., \(\hat{\tau }(0)>\tau \) and the another case \(\hat{\tau }(0)<\tau \). Finally, the effectiveness and correctness of the lag synchronization criteria are verified through two simulation experiments. 相似文献
47.
Baohua Zheng Yunhan Yu Meiling Wang Jianwu Wang Huilan Xu 《Journal of separation science》2022,45(2):432-440
High-performance liquid chromatography-tandem mass spectrometry coupled with the quick, easy, cheap, effective, rugged and safe method was established for the qualitative and quantitative detections of 20 mycotoxins in milk. The linear range of this method was 0.01–10 μg/L and the correlation coefficients were all greater than or equal to 0.9933. At three levels of addition, the spiked recoveries ranged from 80.00 to 112.50%, relative standard deviations were 2.67–14.97%, limits of quantitation were 0.02–4.00 μg/kg, and limits of detection were 0.007–1.300 μg/kg. This developed procedure for the identification and quantitation of mycotoxins provided prospective support for quality regulation. 相似文献
48.
Yunhan Yu Mengya Kuang Baohua Zheng Meiling Wang Zhenqiang Liu Huilan Xu Jianwu Wang 《Journal of separation science》2022,45(9):1538-1549
Herein, an improved method for detecting the endocrine-disrupting chemicals in milk is presented, which is based on high performance liquid chromatography tandem mass spectrometry, coupled with a quick, effective, and safe method. The linearity of the proposed method was in the range of 0.05–100 μg/L, and all correlation coefficients were ≥0.9973. At three concentration levels, the spiked recoveries ranged from 77.7 to 107.5%, relative standard deviations ranged from 0.2 to 14.6%, limits of quantitation ranged from 0.1 to 40 μg/kg, limits of detection ranged from 0.03 to 13.3 μg/kg. The proposed method for the identification and quantitation of 26 endocrine disruptors present in milk is not only easy, fast, and cost-efficient but also provides a reference for the detection of various endocrine disruptors in milk and other dairy products. 相似文献
49.
C5烃中双环戊二烯过氧化物的分光光度测定 总被引:1,自引:0,他引:1
本报道了C5烃中双环戊二烯过氧化物(PDCPD)快速准确的分析方法。在HOC2H4OCH3-H2O介质中,PDCPD与KI反应生成I3^-而I3^-与PDCPD的量成正比,在λmax=352nm处可进行PDCPD的光度测定,测定下限为3.2×10^-5mol/L,SD=0.34,RSD=1.40%。 相似文献
50.