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921.
Simultaneous determination of betamethasone and dexamethasone residues in bovine liver by liquid chromatography/tandem mass spectrometry 总被引:1,自引:0,他引:1
Van Den Hauwe O Perez JC Claereboudt J Van Peteghem C 《Rapid communications in mass spectrometry : RCM》2001,15(11):857-861
In this study a new method for the simultaneous confirmation of betamethasone and dexamethasone residues in bovine liver is presented. A Quattro LCZ triple quadrupole mass spectrometer, equipped with an atmospheric pressure ionization (API) source, was coupled to a high performance liquid chromatograph (HPLC) system. Spiked liver samples were first extracted with acetonitrile, and the extracts were purified on C-18 columns. LC separations were performed on a Hypercarb column, with acetonitrile/water (90:10, v/v, +0.3% formic acid) as the mobile phase. Retention times for dexa- and betamethasone were 6.60 and 8.50 min, respectively. Fluorometholone had a retention time of 6.70 min and was used as the internal standard. The detection of the analytes was performed in the multiple reaction monitoring (MRM) mode. The assay was linear over the range of 0.5 to 8 microg/kg for both analytes. The estimated determination limits were 0.2 microg/kg for both beta- and dexamethasone and the quantification limits were 0.4 microg/kg for dexamethasone and 0.3 microg/kg for betamethasone. Analysis precision at 1, 2 and 4 microg/kg was lower than 6.1% (relative standard deviation, RSD) and accuracy was at least 97.5%. Recoveries at 1, 2 and 4 microg/kg ranged between 56 and 69%. 相似文献
922.
A. N. Andreyev D. Ackermann F. P. Heßberger S. Hofmann M. Huyse I. Kojouharov B. Kindler B. Lommel G. Münzenberg R. D. Page K. Van de Vel P. Van Duppen K. Heyde 《The European Physical Journal A - Hadrons and Nuclei》2003,18(1):55-64
Alpha-decay of the new nuclide 184Bi has been studied in the complete-fusion reaction 93Nb(94Mo, 3n)184Bi at the velocity filter SHIP. The evaporation residues were separated in-flight and subsequently identified on the basis of recoil-
, recoil-
-
analysis and excitation functions measurements. Two
-decaying isomeric states in 184Bi with half-life values of 13(2) ms and 6.6(1.5) ms were identified. The
-branching ratio of 180Tl was deduced for the first time as
. Improved data on the fine-structure
-decay of 186Bi were obtained in the 93Nb(95Mo, 2n)186Bi reaction. A similarity of the decay energies and half-life values of 184,186Bi is pointed out and a possible explanation for this effect is suggested.Received: 14 March 2003, Revised: 29 April 2003, Published online: 2 September 2003PACS:
23.60.+e
decay - 27.70.+q
- 27.80.+w
K. Heyde: Present address: EP-ISOLDE, CERN, CH-1211, Geneva 23, Switzerland. 相似文献
923.
E. Galichet F. Gulminelli D. C. R. Guinet M. F. Rivet J. F. Lecolley R. Bougault G. Auger B. Borderie B. Bouriquet A. Buta J. L. Charvet A. Chbihi J. Colin D. Cussol R. Dayras D. Durand J. D. Frankland B. Guiot S. Hudan P. Lautesse F. Lavaud N. Le Neindre O. Lopez L. Manduci J. Marie L. Nalpas J. Normand M. Pârlog P. Paw lowski E. Plagnol E. Rosato J. C. Steckmeyer B. Tamain A. Van Lauwe E. Vient C. Volant J. P. Wieleczko INDRA Collaboration 《The European Physical Journal A - Hadrons and Nuclei》2003,18(1):75-86
The transport properties of the 36Ar +58Ni system at
measured with the INDRA array, are studied within the BNV kinetic equation. A general protocol of comparison between the N-body experimental fragment information and the one-body distribution function is developed using global variables, with a special focus on charge density. This procedure avoids any definition of sources and any use of an afterburner in the simulation. We shall discuss the feasibility of such an approach and the distortions induced by the finite detection efficiency and the completeness requirements of the data selection. The sensitivity of the different global observables to the macroscopic parameters of the effective nuclear interaction will be studied in detail.Received: 21 January 2003, Published online: 5 August 2003PACS:
25.70.-z Low and intermediate energy heavy-ion reactions - 24.10.-i Nuclear reaction models and methodsN. Le Neindre: Permanent address: Institut de Physique Nuclaire, IN2P3-CNRS, F-91406 Orsay cedex, France. 相似文献
924.
J.W.?Van OrdenEmail author S.?Jeschonnek 《The European Physical Journal A - Hadrons and Nuclei》2003,17(3):391-395
The phenomena of scaling and Bloom-Gilman duality are examined in the context of simple nonrelativistic and relativistic quantum-mechanical models. These models are shown to scale and to show the qualitative features of Bloom-Gilman duality. This suggests that these phenomena do not necessarily require the properties of QCD.Received: 1 November 2002, Published online: 15 July 2003PACS:
12.40.Nn Regge theory, duality, absorptive/optical models - 12.39.Ki Relativistic quark model - 13.60.Hb Total and inclusive cross-sections (including deep-inelastic processes) 相似文献
925.
Many graphs arising in various information networks exhibit the "power law" behavior -the number of vertices of degree k is proportional to k-# for some positive #. We show that if # > 2.5, the largest eigenvalue of a random power law graph is almost surely(1+ o(1))?m (1+ o(1))\sqrt{m} where m is the maximum degree. Moreover, the klargest eigenvalues of a random power law graph with exponent # have power law distribution with exponent 2# if the maximum degree is sufficiently large, where k is a function depending on #, mand d, the average degree. When 2<#< 2.5, the largest eigenvalue is heavily concentrated at cm3-# for some constant c depending on # and the average degree. This result follows from a more general theorem which shows that the largest eigenvalue of a random graph with a given expected degree sequence is determined by m, the maximum degree, and [(d)\tilde] \tilde{d} , the weighted average of the squares of the expected degrees. We show that the k-th largest eigenvalue is almost surely (1+ o(1))?{mk} (1+ o(1))\sqrt{m_k} where mk is the k-th largest expected degree provided mk is large enough. These results have implications on the usage of spectral techniques in many areas related to pattern detection and information retrieval. 相似文献
926.
B Baesens T Van Gestel S Viaene M Stepanova J Suykens J Vanthienen 《The Journal of the Operational Research Society》2003,54(6):627-635
In this paper, we study the performance of various state-of-the-art classification algorithms applied to eight real-life credit scoring data sets. Some of the data sets originate from major Benelux and UK financial institutions. Different types of classifiers are evaluated and compared. Besides the well-known classification algorithms (eg logistic regression, discriminant analysis, k-nearest neighbour, neural networks and decision trees), this study also investigates the suitability and performance of some recently proposed, advanced kernel-based classification algorithms such as support vector machines and least-squares support vector machines (LS-SVMs). The performance is assessed using the classification accuracy and the area under the receiver operating characteristic curve. Statistically significant performance differences are identified using the appropriate test statistics. It is found that both the LS-SVM and neural network classifiers yield a very good performance, but also simple classifiers such as logistic regression and linear discriminant analysis perform very well for credit scoring. 相似文献
927.
Consider a regular diffusion process X with finite speed measure m. Denote the normalized speed measure by μ. We prove that the uniform law of large numbers
holds if the class
has an envelope function that is μ-integrable, or if
is bounded in L
p(μ) for some p>1. In contrast with uniform laws of large numbers for i.i.d. random variables, we do not need conditions on the ‘size’ of
the class
in terms of bracketing or covering numbers. The result is a consequence of a number of asymptotic properties of diffusion
local time that we derive. We apply our abstract results to improve consistency results for the local time estimator (LTE)
and to prove consistency for a class of simple M-estimators.
This revised version was published online in June 2006 with corrections to the Cover Date. 相似文献
928.
T. Loarer J. Gunn J. L. Lachambre E. Gravier C. Boucher K. H. Finken M. Lehnen G. Mank S. Jachmich H. Van Goubergen G. Van Oost 《Czechoslovak Journal of Physics》2001,51(10):1021-1031
Particle collection by the ALT-II belt limiter in the TEXTOR-94 tokamak is exclusively limited to the parallel outflux because the scoop walls that are oriented parallel to the field lines obstruct the poloidal E×B mass flow. With normal B
tor direction (E×B towards the scoops), a threefold decrease of plenum pressure is measured during negative biasing, while with reversed B
tor (E×B away from the scoops), a 60% pressure increase is observed. This behaviour is exactly opposite to that observed in X-point divertors. A simple fluid model explains this apparent contradiction, and gives good quantitative agreement with measurements of the parallel Mach number in the SOL. The essential physics is governed by the Bohm-Chodura criterion. 相似文献
929.
Guido Van Oost James P. Gunn Alexander Melnikov Jan Stöckel Michael Tendler 《Czechoslovak Journal of Physics》2001,51(10):957-975
Radial electric fields (E
r) and their role in the establishment of edge transport barriers and improved confinement have been studied in the tokamaks TEXTOR-94 and CASTOR, where E
r is externally applied to the plasma in a controlled way using a biased electrode, as well as in the tokamak T-10 where an edge transport barrier (H-mode) is obtained during electron-cyclotron resonance heating (ECRH) of the plasma.The physics of radial currents was studied and the radial conductivity in the edge of TEXTOR-94 (R = 1.75 m, a = 0.46 m) was found to be dominated by recycling (ion-neutral collisions) at the last closed flux surface (LCFS) and by parallel viscosity inside the LCFS. From a performance point of view (edge engineering), such electrode biasing was shown to induce a particle transport barrier, a reduction of particle transport, and a concomitant increase in energy confinement. An H-mode-like behaviour can be induced both with positive and negative electric fields. Positive as well as negative electric fields were shown to strongly affect the exhaust of hydrogen, helium, and impurities, not only in the H-mode-like regime.The impact of sheared radial electric fields on turbulent structures and flows at the plasma edge is investigated on the CASTOR tokamak (R = 0.4 m, a = 0.085 m). A non-intrusive biasing scheme that we call "separatrix biasing" is applied whereby the electrode is located in the scrape-off layer (SOL) with its tip just touching the LCFS. There is evidence of strongly sheared radial electric field and E×B flow, resulting in the formation of a transport barrier at the separatrix. Advanced probe diagnosis of the edge region has shown that the E×B shear rate that arises during separatrix biasing is larger than for standard edge plasma biasing. The plasma flows, especially the poloidal E×B drift velocity, are strongly modified in the sheared region, reaching Mach numbers as high as half the sound speed. The corresponding shear rates ( 5×106 s-1) derived from both the flow and electric field profiles are in excellent agreement and are at least an order of magnitude higher than the growth rate of unstable turbulent modes as estimated from fluctuation measurements.During ECRH in the tokamak T-10 (R = 1.5 m, a = 0.3 m), a regime of improved confinement is obtained with features resembling those in the H-mode in other tokamaks. Using a heavy ion beam probe, a narrow potential well is observed near the limiter together with the typical features of the L-H transition. The time evolution of the plasma profiles during L-H and H-L transitions is clearly correlated with that of the density profile and the formation of a transport barrier near the limiter. The edge electric field is initially positive after the onset of ECRH. It changes its sign during the L-H transition and grows till a steady condition is reached. Similar to the biasing experiments in TEXTOR-94 and CASTOR, the experimentally observed transport barrier is a barrier for particles. 相似文献
930.
Fred Van Oystaeyen Yinhuo Zhang 《Proceedings of the American Mathematical Society》2001,129(2):371-380
We calculate the Brauer group of the four dimensional Hopf algebra introduced by M. E. Sweedler. This Brauer group is defined with respect to a (quasi-) triangular structure on , given by an element . In this paper is a field . The additive group of is embedded in the Brauer group and it fits in the exact and split sequence of groups: where is the well-known Brauer-Wall group of . The techniques involved are close to the Clifford algebra theory for quaternion or generalized quaternion algebras.