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Glasses with the base compositions xNa2O · 15Al2O3 · (85 ? x)SiO2 (x = 8.5, 11 and 16) doped with 0.5 mol% SnO2 were investigated by both square-wave voltammetry and impedance spectroscopy in the temperature range from 1300 to 1600 °C. Each recorded square-wave voltammogram exhibits a well pronounced peak attributed to the Sn2+/Sn4+-redox pair. Impedance spectra were measured in a frequency range from 0.1 to 105 s?1 as a function of the superimposed dc-potential and were simulated using an equivalent circuit taking into account the resistivity of the melt, the electrochemical double layer, a resistor attributed to a kinetically hindered electron transfer and a Warburg parameter which accounts for the diffusion process of Sn4+ and Sn2+ to and from the electrode. Additionally, two impedance elements, a resistor and a capacitance both attributed to adsorption processes were necessary to fit the impedance spectra. 相似文献
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Anna Evans Anja Bieberle-Hütter Henning Galinski Jennifer L. M. Rupp Thomas Ryll Barbara Scherrer René T?lke Ludwig J. Gauckler 《Monatshefte für Chemie / Chemical Monthly》2009,16(3):975-983
Abstract
Micro-solid oxide fuel cells (micro-SOFC) are predicted to be of high energy density and are potential power sources for portable electronic devices. A micro-SOFC system consists of a fuel cell comprising a positive electrode-electrolyte-negative electrode (i.e. PEN) element, a gas-processing unit, and a thermal system where processing is based on micro-electro-mechanical-systems fabrication techniques. A possible system approach is presented. The critical properties of the thin film materials used in the PEN membrane are discussed, and the unsolved subtasks related to micro-SOFC membrane development are pointed out. Such a micro-SOFC system approach seems feasible and offers a promising alternative to state-of-the-art batteries in portable electronics. 相似文献1000.
A set of vertices in a graph is an independent dominating set of if is an independent set and every vertex not in is adjacent to a vertex in . The independent domination number, , of is the minimum cardinality of an independent dominating set. In this paper, we extend the work of Henning, Löwenstein, and Rautenbach (2014) who proved that if is a bipartite, cubic graph of order and of girth at least , then . We show that the bipartite condition can be relaxed, and prove that if is a cubic graph of order and of girth at least , then . 相似文献