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131.
Gd-diethylenetriamine pentaacetic acid-bismethylamide, Gd(DTPA-BMA), is shown to be a reagent suitable for the identification of protein surfaces. Compared to the conventionally used spin-label TEMPOL, Gd(DTPA-BMA) is a stronger relaxation agent, requiring lesser concentrations to achieve the same paramagnetic relaxation enhancement of solvent-exposed protein protons. It is also less hydrophobic and therefore less prone to specific binding to proteins. Relaxation enhancements predicted by a second-sphere interaction model correlated with experimental data recorded with ubiquitin, while the correlation with corresponding data recorded with TEMPOL was poor. 相似文献
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136.
Rosarina Carpignano Piero Savarino Ermanno Barni Guido Viscardi Sergio Clementi Gianfranco Giulietti 《Analytica chimica acta》1986
Several physicochemical properties (13C-n.m.r., spectrophotometric, chromatographic, calorimetric) were measured for a series of 38 azo dyes in order to test the existence of relationships between one or more of these data sets and the fastness of the dyes on polyester fabric. The partial least-squares method was applied; it had previously proved useful in establishing structure/property relationships for the same dyes. It is shown that 13C-n.m.r. data can be used successfully to predict dye fastness to light. These data are quickly and cheaply obtained with small amounts of compound. 相似文献
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Guido Schneider 《Physica D: Nonlinear Phenomena》2000,140(3-4):283-293
Modulating pulse-solutions consist of a pulse-like envelope advancing in the laboratory frame and modulating an underlying spatially and temporarily oscillating wave train. Such solutions play a big role in nonlinear optics, where information is transported as pulse-like modulations of an underlying electromagnetic wave. For a phenomenological model we prove criteria for the existence and asymptotic stability of such solutions in terms of the coefficients of the associated equation for the envelope. 相似文献
139.
Maria F. Ebel Horst Ebel Guido Barnegg-Golwig Michael Mantler Robert Svagera 《Mikrochimica acta》1990,101(1-6):63-69
The paper gives an outline of the basic principle of our imaging technique for XPS. The advantage of the concept is its excellent applicability to quantitative pixel information. This idea is verified by two examples which are representative for routine problems in XPS. These are quantitative surface analysis and determination of overlayer thicknesses. A lateral resolution of at least 0.2 mm is achieved and thus a pixel size of 0.2 mm × 0.2 mm can be quantified automatically by means of numerical algorithms without need of reference samples.Dedicated to Professor Günther Tölg on the occasion of his 60th birthday 相似文献
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