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The performance of a new separation technique for metal-speciation — capillary electrophoresis (CE) — is presented. Polyhydroxy compounds such as polyphenols and organic tanning agents can be determined in the g/L range. Certain complexes of these compounds with iron (III) ions may also be directly or indirectly verified. The work has shown that it is possible to determine certain complexes existing in beverages (tea and coffee) by decomplexation with chelating agents (CDTA). The ligands released can be separated by CE and identified by their migration time and UV/VIS absorption spectra. 相似文献
95.
It is shown that for certain classes of infinite block Toeplitz matricesT(a)=[a
j-k
]
0
the Moore-Penrose inverses of the finite sectionT
n
(a)=[a
j-k
]
0
n–1
converge to the Moore-Penrose inverse ofT(a). Furthermore the convergence for modified finite section methods and the finite section method for Wiener-Hopf integral and related operators are studied. 相似文献
96.
Guido Schneider 《Communications in Mathematical Physics》1994,164(1):157-179
The so-called Ginzburg-Landau formalism applies for parabolic systems which are defined on cylindrical domains, which are, close to the threshold of instability, and for which the unstable Fourier modes belong to non-zero wave numbers. This formalism allows to describe an attracting set of solutions by a modulation equation, here the Ginzburg-Landau equation. If the coefficient in front of the cubic term of the formally derived Ginzburg-Landau equation has negative real part the method allows to show global existence in time in the original system of all solutions belonging to small initial conditions, inL
. Another aim of this paper is to construct a pseudo-orbit of Ginzburg-Landau approximations which is close to a solution of the original system up tot=. We consider here as an example the socalled Kuramoto-Shivashinsky equation to explain the methods, but it applies also to a wide class of other problems, like e.g. hydrodynamical problems or reaction-diffusion equations, too. 相似文献
97.
Georg Keller 《Communications in Mathematical Physics》1994,161(2):311-322
It is shown how the differential flow equation (or, equivalently, the continous renormalization group) method can be employed to give an astonishingly easy proof of the local Borel summability of the renormalized perturbative Euclidean massive
4
4
.Supported by NSF grant # DMS-9100383 相似文献
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R. F. Kiefl J. Sonier D. A. Bonn J. H. Brewer J. F. Carolan K. H. Chow P. Dosanjh W. N. Hardy Ruixing Liang W. A. MacFarlane P. Mendels G. D. Morris T. M. Riseman J. W. Schneider 《Hyperfine Interactions》1994,86(1):537-542
We report precision transverse fieldSR measurements of the internal field distribution in the vortex state of crystalline YBa2Cu3O6.95. A novel low background apparatus was used to study a mosaic sample of three high quality single crystals (Tc=93.3K). The observed frequency spectra in magnetic fields of 5kG and 15 kG applied along the c-axis have the characteristic features expected for a regular vortex lattice with some additional broadening. From a preliminary analysis we find that [(0)/(T)]2 has a linear temperature coefficient forT<30 K. Such a term is inconsistent with simple s-wave pairing in the superconducting state. These results support recent microwave measurements of(T) on similar crystals in zero applied field but differ significantly from previousSR reports on sintered powders and crystals with lower Tc.This research was supported by the Natural Sciences and Engineering Research Council of Canada. 相似文献