丙烯酸类单体与倍半铝的络合常数及其与共轭双烯烃的交替共聚

用紫外光谱法测定了丙烯腈、丙烯酸甲酯、甲基丙烯酸甲脂和甲基丙烯酸丁酯与倍半铝 的络合常数(K),其值分别为123,82.6,50和17.51/mol,它们和单体的e值有关:K=2.57 exp(1.39e)。 丙烯酸类单体与共轭双烯在倍半铝存在下的交替共聚反应速度,随络合常数值及两种单体e值之差增大而增大,说明单体极性效应在这种给电子—受电子单体共聚中起重要作用。     

有亏格为1的Heegaard分解的三维流形中的环面纽结

将存在亏格为1的Heegaard分解T’1∪F T’2的三维流形记为M=L(p,q),其中p和q是互素整数,q/p为T’2的纬线在T’1上的斜率.若环面F上的简单闭曲线γ在M中非平凡,则称γ是M中的环面纽结.本文对在M中沿环面纽结作m/n-Dehn手术所得流形进行了分类,并给出了两个实心环体沿边界上平环作融合所得流形是L(p,q)中环面纽结补的特征描述.     

动态弹塑性断裂韧性测试方法的比较研究

利用示波冲击试验,对动态弹塑性断裂韧性测试的不同方法（单试样法和多试样法）进行了研究．结果表明,单试样法（柔度变化率）测定材料的动态断裂韧性是一种简单、准确、适合于工程应用的好方法     

Characterizations and thermal stability of soluble polyimide derived from novel unsymmetrical diamine monomers

Two kinds of novel aromatic, unsymmetrical diamines with ether-ketone group, 3-amino-4′-(4-amino-2-trifluoromethylphenoxy)-benzophenone and 3-amino-4′-(4-aminophenoxy)-benzophenone, was successfully synthesized by two different synthetical routes and polymerized with various aromatic tetracarboxylic acid dianhydrides, including 4,4′-oxydiphthalic anhydride, 3,3′,4,4′-benzophenone tetracarboxylic dianhydride, and 2,2′-bis(3,4-dicarboxyphenyl)-hexafluoropropane dianhydride, via a conventional two-step thermal or chemical imidization method to produce a series of fluorinated polyimides. The polyimides were characterized with solubility tests, viscosity measurements, mechanical properties tests, IR-FT, and thermogravimetric analysis. The polyimides had inherent viscosities of 0.54-0.77 dL/g and were easily dissolved in both polar, aprotic solvents and common, low-boiling-point solvents. The resulting strong and flexible polyimide films exhibited excellent thermal stability, with decomposition temperatures (at 10% weight loss) above 573 °C and glass-transition temperatures in the range of 222-251 °C. Moreover, the polymer films showed outstanding mechanical properties, with tensile strengths of 86.5-121.6 MPa, elongations at break of 9-16%, and initial moduli of 1.26-1.97 GPa. These outstanding combined features ensure that the polymers are desirable candidate materials for advanced applications.     

Synthesis and characterization of fluorinated polyimides derived from novel unsymmetrical diamines

Two kinds of aromatic, unsymmetrical diamines with ether-ketone group, 3-amino-4′-(4-amino-2-trifluoromethylphenoxy)-benzophenone and 4-amino-4′-(4-amino-2-trifluoromethylphenoxy)-benzophenone, were successfully synthesized with two different synthetic routes. Then, they were polymerized with 4,4′-oxydiphthalic anhydride, 3,3′,4,4′-benzophenone tetracarboxylic dianhydride, and 2,2′-bis(3,4-dicarboxyphenyl)-hexafluoropropane dianhydride to form a series of fluorinated polyimides via a conventional two-step thermal or chemical imidization method. The resulting polyimides were characterized by measuring their solubility, viscosity, mechanical properties, IR-FT, and thermal analysis. The results showed that the polyimides had inherent viscosities of 0.48-0.68 dl/g and were easily dissolved in bipolarity solvents and common, low-boiling point solvents. Meanwhile, the resulting strong and flexible polyimide films exhibited excellent thermal stability, e.g., decomposition temperatures (at 10% weight loss) are above 575 °C and glass-transition temperatures in the range of 218-242 °C. The polymer films also showed outstanding mechanical properties, such as tensile strengths of 86.5-132.8 MPa, elongations at break of 8-14%, and initial moduli of 1.32-1.97 GPa. These outstanding combined features ensure that the polymers are desirable candidate materials for advanced applications.     

Thin Position of Heegaard Splittings

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An Extension of The Handle Addition Theorem

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模拟法描绘静电场实验中导电液体的选择与研究

通过对氯化钠(蒸馏水+氯化钠)导电液体的使用和对实验数据的计算分析,发现选用浓度或电导率不同的导电液体,对实验结果有着明显的影响.文章为实验选用氯化钠导电液体提供了相对客观的参考标准,对减少导电液体(如自来水)的各种偶然因素对实验造成的诸多不确定影响有一定实用价值.     

Some Properties of an Annulus Sum of 3-manifolds

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