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931.
J. L. Gascón M. Rodríguez J. A. Suárez Del Rey 《Journal of Radioanalytical and Nuclear Chemistry》1996,207(1):63-69
The determination of Am and Cm in typical waste streams from nuclear power plants using anion exchange chromatography has some drawbacks like the contamination by Pu and Po. This improved procedure solves these problems, and it has been applied with success to the analysis of Am and Cm in nuclear waste samples: ion exchange resins, ion exchange resins solidified with cement and evaporator concentrates. 相似文献
932.
M. Angel Mateos Rocío Gálvez F. Javier Manuel de Villena José M. Pingarrón 《Mikrochimica acta》1995,120(1-4):339-349
An electroanalytical study of the herbicide propazine's reduction process in micellar solutions and oil-in-water emulsions is reported. The anionic surfactant sodium pentanesulphonate was chosen as the most suitable. The differential pulse polarograms of micellar solutions had two reduction peaks below pH 2.0, whereas only one peak was obtained above pH 2.O. Ethyl acetate was chosen as the organic solvent to form propazine emulsions. Unlike in micellar solutions, the DPP polarograms of propazine emulsions showed only one peak even at pH < 2.0, suggesting that propazine hydrolysis was hindered in the emulsified medium. The limiting current is diffusion-controlled and the electrode process is irreversible. Propazine can be determined by differential pulse polarography over the 1.0 × 10–1 – 1.0 × 10–1moll–1 and 1.0 × 10–15 – 4.0 × 10–1 moll–1 concentration ranges and the limit of detection was 2.8 × 10–1 moll–1. Of the potential interferents simazine, methoprotryne and terbutryn (alls-triazines), thiram (a dithiocarbamate), dinoseb (nitrophenolic), and heptachlor (chlorinated cyclo-diene herbicide), only the first two were significant (10% error for equimolar concentrations). The method was applied to the determination of propazine in spiked drinking water. At a concentration level of 2.0 × 10–1 moll–1 a recovery of 94 ± 6% was obtained, after tenfold concentration on Sep-Pak. 相似文献
933.
We study the rate of uniform approximation by Nörlund means of the rectangular partial sums of double Fourier series of continuous functionsf(x, y), 2π-periodic in each variable. The results are given in terms of the modulus of symmetric smoothness defined by $$\begin{gathered} \omega _2 \left( {f,\delta _1 ,\delta _2 } \right) = \mathop {\sup }\limits_{x,y} \mathop {\sup }\limits_{\left| u \right| \leqslant \delta _1 ,\left| v \right| \leqslant \delta _2 } \left| {f\left( {x + u,y + v} \right)} \right. + f\left( {x + u,y - v} \right) + f\left( {x - u,y + v} \right) \hfill \\ + \left. {f\left( {x - u,y - v} \right) + 4f\left( {x,y} \right)} \right| for \delta _1 ,\delta _2 \geqslant 0. \hfill \\ \end{gathered} $$ As a special case we obtain the rate of uniform approximation to functionsf(x,y) in Lip({α, β}), the Lipschitz class, and inZ({α, β}), the Zygmund class of ordersα andβ, 0<α,β ≤ l, as well as the rate of uniform approximation to the conjugate functions \(\tilde f^{(1,0)} (x,y), \tilde f^{(0,1)} (x,y)\) and \(\tilde f^{(1,1)} (x,y)\) . 相似文献
934.
935.
936.
Abramowicz H Belusevic R Blondel A Blümer H Böckmann P Brummel HD Buchholz P Burkhardt H Debu P Duda J Dydak F Falkenburg B Fiedler M Geiges R Geweniger C Grant AL Guyot C Hagelberg R Hepp V Hughes EW Kampschulte B Keilwerth H Kleinknecht K Knobloch J Krasny M Królikowski J Kurz N Lipniacka A Merlo J Müller E Para A Perez P Perrier F Pollman D Ranjard F Renk B Schuller J Taureg H Tittel K Turlay R Vallage B Wachsmuth H Wotschack J 《Physical review letters》1986,57(3):298-301
937.
Ludwik Adamowicz Rodney J. Bartlett Józef S. Kwiatkowski Willis B. Person 《Theoretical chemistry accounts》1988,73(2-3):135-145
The diatomic systems, PO and PO– are studied, using numerical Hartree-Fock (NHF) and coupled-cluster calculations. The latter employs a hybrid NHF and Slater orbital basis set. Highly accurate CCSD methods predict bond lengths accurate to <0.004 Å and frequencies to 60 cm–1. In addition the electron affinity of PO is computed to be 0.89 eV compared to an experimental value of 1.09±0.01. Comparisons are made with SCF and MBPT(2) results for PO+ using conventional basis sets.Dedicated to Professor J. Koutecký on the occasion of his 65th birthdayGuggenheim Fellow 相似文献
938.
939.
A very special case of one of the theorems of the authors states as follows: Let 1a
1a
2... be an infinite sequence of integers for which all the sumsa
i
+a
j
, 1ij, are distinct. Then there are infinitely many integersk for which 2k can be represented in the forma
i
+a
j
but 2k+1 cannot be represented in this form. Several unsolved problems are stated.Dedicated to our friend Professor E. Hlawka on the occasion of his seventieth birthday 相似文献
940.
1<q<2 L:=
n=1
1/q
n=1/q–1. [0,1]
n()=1, A
n:=
i=1
n–1
i(x)/qi+1/n
x
n(x)=0, n>. , =
n=1
n(x)/qn. F: [0,L]R , F(x)=
n=1
n(x)an,
n=1
¦a
n¦<. [0,L]. q(1,2), . , q(1, 2), . . 相似文献