Hilbert空间上线性算子的Drazin可逆性

主要研究了Hilbert空间上两个Drazin可逆算子和的Drazin可逆性.同时,对上三角算子矩阵的Drazin可逆性也给出了详细的讨论.     

一个非协调膜元的高精度分析

本文讨论一个四自由度三角形非协调膜元的整体超收敛性，外推和亏量校正。     

HL—1装置中心热区电子热传导初步分析

在电流及温度分布满足“不变性”原理的基础上,本文分析了等离子体中心热区的能量平衡,求出了电子热传导系数,根据实验数据拟合出HL-1装置电子热传导系数的定标关系为X_e=6.8(n_(eq1))~(-1.2)。此关系与其他托卡马克装置的结果类似。     

高考预效度的混合估计

用传统的预测效度估计法估计高考预测效度，其估计值往往偏低。为此，本文应用回归分析中混合估计理论提出了高考预测效度的混合估计。这种估计是预测效度的无偏估计，并解决了预测效度估计值偏低的问题。     

房水中烯醇化酶总活性的联酶荧光法测定

采用酶联反应荧光法测定样品中烯醇化酶的总活性。方法最低检出限为０２ＩＵ／Ｌ，在０２０～３５ＩＵ／Ｌ范围标准曲线呈线性，γ＞０９９７，回收率达９０％，相对标准偏差＜１０％。对临床确诊的视网膜母细胞瘤进行了初步探讨，检验结果的特异性较高。     

超声波在多糖降解及提取中的应用

本文支综合介绍了超声波在多糖降解和提取中应用的研究进展．着重对超声波在淀粉，壳多糖，细菌多糖的降解和真菌多糖的提取中的应用作了较详细的阐述．     

CONVERGENCE ON RANDOMLY TRIMMED SUMS WITH A DEPENDENT SAMPLE

§１．ＩｎｔｒｏｄｕｃｔｉｏｎａｎｄＲｅｓｕｌｔｓＬｅｔ｛Ｘｎ，ｎ１｝ｂｅａｓｅｑｕｅｎｃｅｏｆｒａｎｄｏｍｖａｒｉａｂｌｅｓｗｉｔｈａｃｏｍｍｏｎｄｉｓｔｒｉｂｕｔｉｏｎｆｕｎｃｔｉｏｎＦ（ｘ）ａｎｄｌｅｔＸｎ１Ｘｎ２…Ｘｎｎｂｅｔｈｅｏｒ...     

Coboundaries of irreducible markov operators onC(K)

LetK be a compact Hausdorff space, and letT be an irreducible Markov operator onC(K). We show that ifgεC(K) satisfies sup _N ‖Σ _j ^=0N T ^j g‖<∞, then (and only then) there existsfεC(K) with (I − T)f=g. Generalizing the result to irreducible Markov operator representations of certain semi-groups, we obtain that bounded cocycles are (continuous) coboundaries. For minimal semi-group actions inC(K), no restriction on the semi-group is needed.     

金催化化学发光新体系——苯并吡喃化学发光分析法测定金矿中的痕量金

本文提出了一种测定矿样中痕量金的化学发光分析法,氯化6,7-二羟基-2,4-二甲基苯并吡喃-H_2O_2化学发光体系,方法的检出限为7ppb。工作曲线线性范围是10～1000ppbAu,测定的相对标准偏差小于7％。应用本法测定矿样中的金,结果良好。     

Sensitive monitoring of humic acid in various aquatic environments with acidic cerium chemiluminescence detection.

In this research, a simple, sensitive chemiluminescence (CL) method for the determination of humic acid (HA) in water samples was first developed based on the redox reaction between humic acid and cerium(IV) in the acidic condition. Different with the former redox CL reaction which occurred in alkaline solution, no enhancers were needed and neither precipitation nor a second contamination would occur in the present CL system. Comparing with other spectrometric methods, we find that the proposed analysis system had better applicability and accuracy. Under the optimal experiment conditions, the CL peak height was linear with the concentration of HA in the range of 0.03 to 10.0 microg mL(-1). The detection limit is 0.01 microg mL(-1) (S/N = 3), and the relative standard deviation was 2.3% for 0.5 microg mL(-1) HA solution with eleven repeated measurements. The present CL method was successfully applied to the determination of HA in tap water, spring water and river water samples with good recovery from 90.0 to 110.0%. A possible CL mechanism was proposed based on the results of UV and fluorescence spectrometry and the CL spectrum of HA. It was speculated that the semi-quinone radicals in the excited state were the emitters.