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11.
Hà Huy Tài 《manuscripta mathematica》2002,107(4):479-501
Suppose ? is a set of arbitrary number of smooth points in ℙ2
its defining ideal. In this paper, we study the Rees algebras of the ideals generated by I
t
, t ≥α. When the points of ? are general, we give a set of defining equations for the Rees algebra . When the points of ? are arbitrary, we show that for all t≫ 0, the Rees algebra is Cohen-Macaulay and its defining ideal is generated by quadratics. A cohomological characterization for arithmetic Cohen-Macaulayness
of subvarieties of a product space is also given.
Received 4 April 2001 相似文献
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General and selective isolation procedure for high-performance liquid chromatographic determination of anabolic steroids in tissues 总被引:5,自引:0,他引:5
A multi-residue method has been developed for the determination of anabolic steroids in animal tissue. The analytes are extracted from tissue with methanol and the extract is subjected to two solid-phase extractions, one using a non-specific adsorbing material, such as graphitized carbon black (Carbopack B), and the other Amberlite CG-400 I in the OH form. This procedure allowed the neutral anabolics (testosterone, trenbolone and progesterone) to be isolated and separated from the acidic type (phenolic group), such as diethylstilbestrol, oestradiol, zeranol/zearalenone and their respective metabolites. The determination was effected using high-performance liquid chromatography with different detectors (ultraviolet, fluorimetric and electrochemical). Several analytical parameters were studied: chromatographic conditions, recoveries, evaporation step, solvent flow-rate, cartridges reusability, interference of plastic cartridges. For all the anabolics investigated the recoveries were greater than 83.6%. 相似文献
14.
This paper presents a method to estimate reflected and transmitted wave amplitude spectra in a bounded domain such as a wave tank, when available data signals must be shortened due to interferences and wall effects. This paper extends the well known Goda and Suzuki two-probe method to three probes. The paper also suggests solutions to compute reliable transmission and reflection coefficients in spite of problems linked to higher harmonics and to the interference between different wave trains propagating in the tank. To cite this article: G. Duclos, A.H. Clément, C. R. Mecanique 331 (2003). 相似文献
15.
A. Badalà R. Barbera G. Lo Re A. Palmeri G. S. Pappalardo A. Pulvirenti F. Riggi 《Acta Physica Hungarica A》2006,25(2-4):337-346
Results are shown from a Monte Carlo simulation study of the capabilities of the Inner Tracking System of the ALICE experiment, used in standalone mode, for HBT analysis of Pb?Pb collisions at LHC energies (5.5 ATeV). Different values of the coherence factor and the Gaussian source radius have been studied. For this purpose, a specific ITS stand-alone tracking algorithm, based on the Denby-Peterson neural algorithm, has been developed. 相似文献
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G. Giraudi Claudio Baggiani Antonella Cosmaro Emilio Santià Adriano Vanni 《Analytical and bioanalytical chemistry》1998,360(2):235-240
A very selective polyclonal antiserum against 1,1,1-trichloro-2,2-bis-(4-chlorophenyl)-ethane (p,p′-DDT) was obtained by a careful choice of the haptenic structure (2,2-bis(4-chlorophenyl)-ethanol hemisuccinate). This hapten was conjugated to BSA to prepare the immunogen. The effects of different types of solid phases on the equilibrium reaction between the hapten on solid phase and the polyclonal antiserum were evaluated to obtain a fine tuning of the antiserum performances in terms of specificity for p,p′-DDT and sensitivity to low levels of this pesticide. The calibration curves obtained show that it is possible to set up a sensitive assay for p,p′-DDT, employing a p,p′-dichlorodiphenylacetic acid-based solid phase, with a detection limit of 0.12 ng/mL and a working range of about 0.21–40 ng/mL. Selectivity towards several p,p′-DDT-related substances was good (o,p-DDT 17%, p,p′-DDD 1.2% o,p-DDD 6.3%, p,p′-DDE 6.7%). 相似文献
18.
Sannomiya M Rodrigues CM Coelho RG dos Santos LC Hiruma-Lima CA Souza Brito AR Vilegas W 《Journal of chromatography. A》2004,1035(1):47-51
The methanolic extract of the leaves of the medicinal plant Byrsonima crassa (Malpighiaceae) contain flavonoids with antioxidant activity. They were separated in a preparative scale using high-speed counter-current chromatography. The optimum solvent system used was composed of a mixture of ethyl acetate-n-propanol-water (140:8:80 (v/v/v)) and led to a successful separation between monoglucosilated flavonoids (quercetin-3-O-alpha-L-arabinoside, quercetin-3-O-beta-D-galactoside) and the biflavonoid amentoflavone in only 3.5 h. The purities of quercetin-3-O-alpha-L-arabinoside (95 mg), quercetin-3-O-beta-D-galactoside (16 mg) and the biflavonoid amentoflavone (114 mg) were all isolated at purity over 95%. Identification was performed by 1H NMR, 13C NMR and UV analyses. 相似文献
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Résumé La méthyl-9-trihydroxy-2,3,7-fluorone-6 permet de déceler les ions de l'antimoine, en présence de tous autres cations et anions. Les conditions deph (ph = 4) sont à observer rigoureusement.Ce nouveau réactif est avantageusement utilisé dans la méthode d'analyse à la touche ou par empreinte.Les limites de sensibilité sont: en godet 0,2; sur papier gélatine 0,5; sur papier filtre 0,8.
Summary Methyl-9-trihydroxy-2,3,7-fluorone-6 is a reagent which allows to detect antimony ion in the presence of all the other cations and anions. Aph value of 4 must be strictly maintained.This new reagent can be advantageously applied for spot test and offprint analysis.Limits of identification: On the spot test plate 0,2; On gelatine paper 0,5; On filter paper 0,8.
Zusammenfassung Das Methyl-9-trioxy-2,3,7-fluoron-6 gestattet den Nachweis des Antimonions in Gegenwart aller anderen Kationen und Anionen. Dieph-Bedingungen (ph = 4) sind streng einzuhalten.Dieses neue Reagens läßt sich mit Vorteil zur Tüpfel- oder Abdruckanalyse verwenden.Erfassungsgrenzen: auf der Tüpfelplatte 0,2; auf Gelatinepapier 0,5; auf Filtrierpapier 0,8.相似文献