导数分光光度法直接测定环境水中的十二烷基苯磺酸钠

用四阶导数分光光度法,无需经显色与萃取便可直接测定环境水中十二烷基苯磺酸钠的含量。本法抗干扰能力较强,检出限为0.7mg/l(即2×10~(-6)M),回收率为96～103%。     

高频视角下中国股市动态VaR预测模型研究

如何充分挖掘交易数据中有价值的信息对金融风险管理极其重要,现有研究中基于低频波动模型的风险测度方法几乎已经做到了极致,而能达到的预测效果却并不稳健,对高频波动模型的研究相对比较匮乏。那么高频模型能否从高频数据中挖掘出更有价值的信息以便用于风险管理之中呢？本研究通过建立12个低频和9个高频波动模型对上证综指进行样本外动态VaR的滚动预测发现,高频模型相对于低频模型具有更好的稳定性,并且在多数情况下高频模型优于低频模型;多头与空头的风险预测效果具有显著差异,多头风险在高风险情况下高频模型表现出色,低风险情况下并不理想,空头风险则在所有情况下都表现较好。     

Room-Temperature Ferromagnetism in Zn1-xMnxO Thin Films Deposited by Pulsed Laser Deposition

Zn1-xMnxO （x = O.Olq3.1） thin films with a Curie temperature above 300K are deposited on Al2O3 （0001） substrates by pulsed laser deposition. X-ray diffraction （XRD）, ultraviolet （UV）-visible transmission and Raman spectroscopy are employed to characterize the microstructural properties of these films. Room temperature ferromagnetism is observed by superconducting quantum interference device （SQUID）. The results indicate that Mn doping introduces the incorporation of Mn^2＋ ions into the ZnO host matrix and the insertion of Mn^2＋ ions increases the lattice defects, which is correlated with the ferromagnetism of the obtained films. The doping concentration is also proven to be a crucial factor for obtaining highly ferromagnetic Zn1-xMnxO films.     

PCLT/P(VDF-TrFE)纳米复合多层热释电探测器的灵敏度

以0-3 PCLT/P (VDF-TrFE)纳米复合材料为热释电膜,制备了具有多层结构的热释电探测器,测量了热释电电流灵敏度.通过引进矩阵方法从理论上计算了这个多层热释电探测器的电流灵敏度并讨论了各层厚度对其影响.计算值与实验测量值相比较,两者在10¹～10³ Hz的频率范围内符合得很好.     

用有限差分法解简单超静定变截面梁(Ⅱ)

<正> 研究简单超静定梁的强度与刚度问题,关键在于确定多余支反力.当用有限差分法计算多余支反力时,一般文献中介绍,需要解联立方程组,当梁分成较多等分区段时,就显得比较麻烦.本文导出了直接计算多余支反力的公式,大大简化了计算.1.有支承的悬臂梁图1(a)为这种梁.分两种情况进行研究.(1)取支座 n 为多余约束时[图1(b)].设多余支反力为 R_n,相当静定系统为悬臂梁。将     

物理知识在汽车上的应用

生活、学习、工作处处离不开物理知识,随着社会的发展,有车族不断壮大,汽车上的物理知识非常多,这里介绍几项,供大家参考。一、“防抱死”讲安全防抱死系统是现代中高档轿车必不可少的装备,很多汽车广告都会把防抱死刹车系统(ABS)作为“卖点”,其实,ABS是antilock braking syst     

用离子束增强沉积从V2O5粉末制备高热电阻温度系数VO_2薄膜

采用了一种用离子束增强沉积从V2O5粉末直接制备VO2薄膜的新方法,将纯度为997%的V2O5粉末压成溅射靶,在用Ar离子束溅射的同时,用氩氢混合束对沉积膜作高剂量离子注入,使沉积膜中V2O5的V—O键断裂,进而被注入的氢还原,退火后获得热电阻温度系数(TCR)高达4%的VO2薄膜.高剂量的氩氢混合束注入对薄膜引入应力,使薄膜的转换温度降低、电阻温度曲线斜率变大,是薄膜TCR增大的原因 关键词： 离子束增强沉积 VO2薄膜 热电阻温度系数     

硫酸钾水溶液亚稳区性质的研究（Ⅲ）：成核诱导期

按照过饱和溶液产生的方式,研究其亚稳态行为可分为两种类型:一是研究亚稳区宽度随过饱和度(或过冷度)的变化;二是测量恒定过饱和度下的诱导期。前者在前文中已进行了分析讨论。本文旨在测定K_2SO_4水溶液诱导期的基础上,进行理论分析和成核特征值的计算,并将两种方法加以比较。     

Ho and Ti co-doped BiFe03 multiferroic ceramics with enhanced magnetization and ultrahigh electrical resistivity

Bio.9HOo.lFeo.9503 and Bio.9HOo.lFeo.9Tio.0503 ceramics were prepared and compared to reveal the effects of Ho and Ti codoping in BiFeO3. X-ray diffraction indicated that both ceramics had a high rhombohedral perovskite phase content, and microstructural analyses showed that the grains of the Bio.9HOo.lFeo.9Tio.0503 ceramics were much smaller than those of Bio.9HOo.lFeo.9503. An electrical resistivity of more than 1 × 1014.cm at room temperature, and a magnetic hysteresis loop with a remnant magnetization 2Mr of 0.485 emu/g were obtained for Bi0.9HO0.1Fe0.9Ti0.0503; both were much higher than those of Bio.9Hoo.1Feo.9503. Changes in the defect subsystem of BiFeO3 induced by Fe-deficiency and （Ho,Ti） codoping are proposed as being responsible for the improvement in the properties.