The polynomial stress function solution for the rectangular strip bending

In this paper, we propose some formulas for seeking a part of the particular solutions of the heavy harmonics and Tricomi equations and obtain the precise polynomial solutions of the finite-item number for rectangular strip bending problem when the intensity of the distributed load varies with the fourth power of longitudinal coordinate.     

薄层荧光检测中激发波长的选择

具有荧光的化合物经薄层展开后,用荧光法扫描测定具有简便灵敏的优点,而且线性范围宽,并可免除因显色操作带来的误差。正确选择激发波长是测定时的一个重要步骤,在采用高压汞灯光源时,习惯上常采用254和365nm作激发光。但是,具有荧光的化合物在不同激发波长下其荧光强度差别极大。例如,中草药白花前胡中所含的白花前胡丙素,当激发光采用210nm时的测定灵敏度比365nm时高44倍。荧光光谱     

自动进样器故障一例

氨基酸自动分析仪因分析周期长,常采用自动进样装置,在维护不当情况下发生脏堵故障,即进样系统的管道或单向阀内有很多黑色胶状脏物。出现此种故障时,仪器一切正常,唯分析结果错误,如不及时发现,会造成分析失误,操作人员应警惕此种故障的出现。     

固体酸催化合成富马酸二甲酯的研究

富马酸二甲酯是80年代国内外研究开发的新型防腐防霉剂^[1],具有毒性低,耐热性能好,能在pH=3~8范围内使用等特点,广泛用于食品、饲料、粮食、化妆品、纺织品、制药等行业。因其用量小,毒性低,在国外已广泛被使用,特别是在饲料方面。目前,生产上合成富马酸二甲酯多以硫酸和盐酸或磷酸和盐酸的混合酸为催化剂,在马来酸(或顺酐)和甲醇反应体系中进行异构酯化而制得。然而用硫酸盐酸混合酸做催化剂对设备严重腐浊,污染环境,后处理麻烦,且易发生副反应。本文采用固体酸催化剂 HZSM-5分子筛,用顺酐与甲醇反应,一步催化合成富马酸二甲酯,并对其反应机制作了推理。     

Laminar boundary layer between two planes perpendicular to each other

In this paper, we obtain a third-order approximate solution for the laminar boundary layer between two planes perpendicular to each other.In boundary layer equations, the viscous and the inertial terms have the same quantity step. In this paper, at first, supposing that the inertial terms are bigger than the viscous terms, we solve the boundary layer equations, and then we suppose that the viscous terms are bigger than the inertial terms. At last, we take the mean value as the valid solution of the boundary layer equations.The first- and the second-order approximate solutions obtained in this paper coincide with the results in ref. [1], while the third-order solution obtained in this paper is better than that in ref. [1].     

The approximate solution of the self-similar problem for radial flow of non-newtonian fluids through porous media

In this paper, we study the approximate solution of the self-simikar problem for radial flow of non-Newtonian fluids through porous media. Assuming that the fluids obey the exponential function law, we obtain an exact solution for the exponent n=0 and compare it with the approximate solution in ref. [1]. For n>1 and n<1, we obtain respectively approximate solutions. Some exampls are presented.     

ANALYTICAL SOLUTION FOR THE SELFSIMILAR PROBLEMS OF VISCOUS FLUID FLOW

This paper presents a step-by-step approximating method to obtain the analyticalsolutions of the differential equations for the self-similar problems of viscous fluid flow(1.1-1.4).Prosnak(1969)obtained solutions of these equations by using a small paremetermethod,but he reduced the governing equations to the linear differential equations withconstant coefficients.     

小范围屈服时的应力强度因子

对于实际金属材料,裂纹前端总是存在一个或大或小的塑性区.对于小范围屈服,线弹性断裂力学分析仍适用,但必须对塑性区的影响作修正.传统的修正方法(以下简称lrwin法)[1,2],是引入有效裂纹长度的概念,即认为由于塑性区的存在,实际裂纹长度必有所增加,如取裂纹长度等于有效裂纹长度2(a+r_y),其中2a为裂纹的原长,2r_y为裂纹的增长量,则可不必考虑塑性区的存在,仍按线弹性断裂力学处理.本文则认为:由于塑性区的存在,实际的裂纹长度和外加应力均会增大.即是说,应力强度因子中的两个参量a及σ₁(外加应力)值均将改变.文中指出,按本文方法确定的应力强度因子式(3.2),较通用公式(3.4)更接近于Duffy[4]的符合实验结果的经验公式(3.6).     

对流热交换的一维非等温流动

文献[1]研究了在有稳定换热过程的管道流动中.当粘性系数μ是温度的指数函数时,在甚么条件下发生一维非等温流动.对于平面渠道及圆管的流动,还研究了速度及温度场.本文对同样问题补充提出了二种新的解法.文献[1]的方法可看成是本文方法的一个自然的分支.两个新解法中的一个只能求解文献[1]的同样问题,其计算过程的复杂程度也和文献[1]不相上下;但是另一个却能超出文献[1]的研究范围,即对管道的横截面的周界不是等曲率曲线的情形亦可求解.