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111.
112.
熔体旋淬MI(NiCoMnAl)5贮氢合金的组织结构与电化学特性 总被引:6,自引:1,他引:5
对比研究了熔体旋淬和常规熔铸Ml(NiCoMnAl) 相似文献
113.
邻甲苯基异腈酸酯与3,6-二甲基-1,6-二氢-S-四嗪在催化剂4-二甲胺基吡啶存在下反应,生成标题化合物( C20H22N6O2, Mr = 378.43 )。经X-射线单晶结构分析表明此晶体属单斜晶系,P21/c空间群,a = 11.151(4),b = 15.318(2),c = 11.352(2)?,β=103.85(2)°,V = 1882.7? 3,Z = 4,μ= 0.093mm-1,Dc = 1.413g/cm3,F(000) = 800。结果表明,该化合物的两个酰胺基处于S-四嗪环的1,4位,而四嗪环本身呈船式构象。 相似文献
114.
The synthesis of filled skutterudite compounds (Ce or Y)_y(Fe)_x(Co)_(4x)(Sb)_(12), through a solidstate reaction using chloride of Ce or Y,high purity powder of Co, Fe, and Sb as starting materials,was investigated. (Ce or Y)_y(Fe)_x(Co)_(4x)(Sb)_(12) (x=0--1.0, y=0--0.15) compounds were obtained at850--1 123 K. The results of Rietveld analysis demonstrate that (Ce or Y)_y(Fe)_x(Co)_(4x)(Sb)_12synthesized by a solid state reaction possesses a filled skutterudite structure. The filling fraction ofCe or Y obtained by Rietveld analysis agrees well with the composition obtained by chemicalanalysis. The lattice constant of (Ce)_y(Fe)_x(Co)_(4x)(Sb)_(12) increases with increasing substitution of Fe at Cosites, and with an increasing Ce filling fraction in the Sb-dodecahedron voids. The lattice thermalconductivity of (Ce or Y)_y(Fe)_x(Co)_(4x)(Sb)_(12) decreases significantly with an increasing Ce or Y fillingfraction in the voids and with substitution of Fe at Co sites. 相似文献
115.
Considering the properties of slow change and quasi-periodicity of
magnetocardiography (MCG) signal, we use an integrated technique of adaptive
and low-pass filtering in dealing with two-channel MCG data measured by high
$T_{\rm c}$ SQUIDs. The adaptive filter in the time domain is based on a noise feedback
normalized least-mean-square (NLMS) algorithm, and the low-pass filter with
a cutoff at 100Hz in the frequency domain characterized by Gaussian functions is
combined with a notch at the power line frequency. In this way, both
relevant and irrelevant noises in original MCG data are largely eliminated.
The method may also be useful for other slowly varying quasi-periodical
signals. 相似文献
116.
Z-pinch experiments with two arrays consisting, respectively, of 32
4-μm- and 6-μm-diameter tungsten wires have been carried out on
QiangGuang-1 facility with a current rising up to 1.5MA in 80ns. At early
time of implosion, x-ray framing images show that the initial emission comes
from the central part of arrays, and double clear emission rings, drifting
to the anode and the cathode at 5×106cm/s and 2.4×107cm/s respectively, are often produced near the electrodes. Later,
in a 4-μm-diameter tungsten wire array, filamentation caused by ohmic
heating is prominent, and more than ten filaments have been observed. A
radial inward shift of arrays starts at about 30\,ns earlier than the
occurrence of the x-ray peak power for both kinds of arrays, and the
shrinkage rate of emission region is as high as 1.7×107cm/s in
a 4-μm-diameter tungsten wire array, which is two times higher than
that in a 6-μm one. Emission from precursor plasmas is observed in
implosion of 6-μm-diameter tungsten wire arrays, but not in implosion
of a 4-μm-diameter tungsten wire array. Whereas, in a 4-μm-diameter tungsten wire array, the soft x-ray emission shows the growth of
m=1 instability in the plasma column, which is caused by current. The
reasons for the discrepancy between implosions of 4-μm- and 6-μm-diameter tungsten wire arrays are explained. 相似文献
117.
This paper reports that DLC (diamond like carbon)/Ti and DLC films were prepared by
using pulsed laser arc deposition. R-ray diffraction, Auger electron spectroscopy,
Raman spectroscopy, atomic force microscopy, nanoindenter, spectroscopic
ellipsometer, surface profiler and micro-tribometer were employed to study the
structure and tribological properties of DLC/Ti and DLC films. The results show that
DLC/Ti film, with $I(D)/I(G)$ 0.28 and corresponding to 76{\%} sp$^{3}$ content
calculated by Raman spectroscopy, uniform chemical composition along depth
direction, 98 at{\%} content of carbon, hardness 8.2 GPa and Young's modulus 110.5
GPa, compressive stress 6.579 GPa, thickness 46~nm, coefficient of friction 0.08,
and critical load 95mN, exhibits excellent mechanical and tribological properties. 相似文献
118.
脉冲激光沉积BNT和KNN系陶瓷薄膜的比较研究 总被引:2,自引:0,他引:2
利用脉冲激光沉积技术(PLD),在不同的制备工艺条件下,分别在Pt/Ti/SiO2/Si基片上制备了Bi0.5Na0.5TiO3(BNT)系列的Bi0.5(Na0.7K0.2Li0.1)0.5TiO3(BNKLT)和K0.5Na0.5NbO3(KNN)系列的Li0.04(Na0.5K0.5)0.96(Nb0.775Ta0.225)O3(KNNLT)无铅压电陶瓷薄膜,并利用X射线衍射仪(XRD)、扫描电镜(SEM)和原子力显微镜(AFM)对薄膜的晶体结构及表面形貌进行了比较研究.研究结果表明:薄膜的衬底温度、沉积室的氧气压力和薄膜的热处理温度对BNT和KNN薄膜结构和形貌都有较大影响,且影响程度不同;在最佳制备工艺参数下,利用PLD制备的BNT和KNN无铅压电陶瓷薄膜都具有精细的表面结构. 相似文献
119.
黄花倒水莲皂甙Reinioside C在大鼠体内代谢产物的鉴定 总被引:3,自引:0,他引:3
为了探讨五环三萜皂甙ReiniosideC在大鼠体内代谢产物的结构,单剂量口服ReiniosideC,5h后放血处死,用制备型高效液相色谱方法对血液和各脏器进行提取分离,从大肠内容物和粪中,分离得到了7种代谢产物.用FAB-MS,1H NMR和13C NMR方法鉴定了它们的结构. 相似文献
120.
Enhanced pulse compression induced by the interaction between the third—order dispersion and the cross—phase modulation in birefringent fibres 总被引:1,自引:0,他引:1 下载免费PDF全文
In this paper,we report on the enhanced pulse compression due to the interaction between the positive third-order dispersion (TOD) and the nonlinear effect (cross-phase modulation effect) in birefringent fibres.Polarization soliton compression along the slow axis can be enhanced in a birefringent fibre with positive third-order dispersion,while the polarization soliton compression along the fast axis can be enhanced in the fibre with negative third-order dispersion.Moreover,there is an optimal third-order dispersion parameter for obtaining the optimal pulse compression.Redshifted initial chirp is helpful to the pulse compression,while blueshifted chirp is detrimental to the pulse compression.There is also an optimal chirp parameter to reach maximum pulse compression.The optimal pulse compression for TOD parameters under different N-order solitons is also found. 相似文献