基于动态Allan方差的光纤陀螺随机误差分析及算法改进EI北大核心CSCD

为了全面了解光纤陀螺(FOG)各项随机误差随时间的变化特性,利用动态Allan方差(DAVAR)方法对光纤陀螺输出信号进行了分析研究。结果表明,与经典Allan方差对光纤陀螺随机误差的分析相比较,DAVAR不仅能准确地评估光纤陀螺各项误差,而且能够直观地反映光纤陀螺各项误差随时间变化的稳定性;由于DAVAR需要估计出陀螺信号各个时间点的Allan方差,因此其具有随着分析数据量增大、运算耗时急剧增加的缺点。为此提出了一种基于选择相关时间序列t的改进型快速DAVAR的计算方法。实验证明,在不影响DAVAR运算结果的前提下,改进型快速DAVAR算法在大数据量分析时有效提高了运算效率。     

流动注射-化学发光法用于药物分析研究进展

简述了近年来国内外流动注射-化学发光法在药物分析领域中的主要运用。主要介绍了鲁米诺-H2O2体系、鲁米诺-铁氰化钾体系、鲁米诺-高碘酸盐体系、鲁米诺-KMnO4体系、鲁米诺-Ag(Ⅲ)配合物体系以及其他体系在药物分析中的运用。     

Measurements of electron-phonon coupling factor and interfacial thermal resistance of metallic nano-films using a transient thermoreflectance technique

Using a transient thermoreflectance (TTR) technique,several Au films with different thicknesses on glass and SiC substrates are measured for thermal characterization of metallic nano-films,including the electron-phonon coupling factor G,interfacial thermal resistance R,and thermal conductivity K s of the substrate. The rear heating-front detecting (RF) method is used to ensure the femtosecond temporal resolution. An intense laser beam is focused on the rear surface to heat the film,and another weak laser beam is focused on the very spot of the front surface to detect the change in the electron temperature. By varying the optical path delay between the two beams,a complete electron temperature profile can be scanned. Different from the normally used single-layer model,the double-layer model involving interfacial thermal resistance is studied here. The electron temperature cooling profile can be affected by the electron energy transfer into the substrate or the electron-phonon interactions in the metallic films. For multiple-target optimization,the genetic algorithm (GA) is used to obtain both G and R. The experimental result gives a deep understanding of the mechanism of ultra-fast heat transfer in metals.     

飞秒激光热反射实验系统测量金属薄膜中的超快速热传递过程

飞秒激光热反射技术已经成为研究不同材料中超快速热传导过程的有效实验方法.实验中采用前表面加热、后表面探测的方法对不同厚度的Au薄膜进行了测量,通过比较表面电子温度可以得到超快速激光加热条件下Au薄膜材料中电子温度振荡的传递速度.结果表明瞬态条件下非平衡态电子是热量的主要载体,根据实验测量值拟合得到的能量传递速度接近于非...     

吸附物种在金纳米电极上的表面扩散

应用激光加热拉伸方法制备金纳米电极,研究了非金属物种氧和碘在金纳米电极表面的吸附以及金属铅和铜在金纳米电极表面的欠电势沉积行为,观察到吸附物种在金纳米电极上显著的表面扩散现象.     

普鲁士蓝纳米修饰电极的制备及表征

采用激光加热拉伸的方法制备铂纳米电极,并通过交流电刻蚀的方法制备纳米孔电极,在这两种电极上可通过电化学方法原位合成单颗普鲁士蓝微晶. 结果表明,普鲁士蓝微晶在纳米微孔电极上的机械附着强度增强. 这种方法可用于制备纳米修饰电极或研究功能微晶体材料的电化学性质.     

激光光热反射光谱检测装置的研制

研制出一种采用直接测量激光反射光信号的激光光热反射光谱检测装置。讨论了该装置的硬件结构和程序模块,并应用于分子印迹实验。该装置具有操作简单、精度高、稳定性好和抗干扰能力强等优点。     

第一性原理计算:MgCNi_3镁位空穴(Na)掺杂的声子谱研究

应用全势线性响应线性糕模轨道(FP-LR-LMTO)方法对MgcM3镁位进行钠掺杂的虚原子近似,计算晶格振动的动力学矩阵,得到Mg1-xNaxCNi3(x=0,0.06)的声子谱.计算结果表明MgCNi3声子谱中最低声学支沿F-M方向有接近一半距离的不稳定声子模存在,不稳定声子模都包括存原胞内x-y平面上两个相邻Ni原子沿着与C-Ni键垂直的方向上,向着镍八面体间隙区的垂直运动x为0.06的掺杂,使得布里渊区沿三个主要高对称性方向(Г-x、Г-M、Г-R)虚频范围扩大,容易使MgCNi3结构不稳定而产生结构相变.     

INHIBITION OF STREPTOMYCIN-DEPENDENT MUTATION IN Escherichia coli ON THE LYTIC GROWTH OF BACTERIOPHAGE LAMBDA

Spontaneous streptomycin-dependent mutants (Str~DA) were isolared from Escherichia coli C600. OnC600 Str~D, the lytic growth of phage λ Nam and λcI857 was inhibited. After E. coli lysogenic strain1.1485 (λcI857) mutated to Str~DA, induction of λ was decreased greatly. On Str~DA of E. coli strainsC600 and 1.1485 (λcI857), the plating efficiencies and burst sizes of phage T4 and T7 remained nor-mal. Since Str~DA is a mutation in the structural gene for ribosomal protein S12, the results obtained inthe present study suggest that ribosomes of the Str~DA mutants inhibit the Iytic growth of λ phage. The possibility that Str~DA ribosomes inhibit the expression of λ N gene is discussed based on thecomparison of the genetic background of λcI857 and λNam.     

癸胺盐酸盐晶体相变的拉曼光谱研究

在290—340K温度范围内,考察了标题化合物分子链的C—H和C—C伸缩振动等主要拉曼散射谱带频率和强度随温度的变化。结果表明,癸胺盐酸盐晶体在313K和321K发生两次结构相变。在低于313K时,分子链以完全有序的全反式构象存在;在313K以上时,分子链出现了旁式构象。高于321K时,随着旁式链构象的骤增,分子链的侧向填充有序度明显降低,链的“流动性”明显增强。