荧光猝灭法测定壳聚糖凝胶膜中壳聚糖的含量

壳聚糖(CTS)在PBS缓冲溶液中对异硫氰酸荧光素(FITC)具有明显的荧光猝灭作用,且发现荧光猝灭程度与壳聚糖的量在一定范围内呈线性关系,吐温-20(T20)对此反应有明显的增敏效果,据此建立了通过荧光猝灭测定壳聚糖含量的方法.实验结果表明:在pH6.4的PBS缓冲溶液及T20含量为0.00200％的体系中,壳聚糖浓度在0.0400-1.00mg/L范围内的回归方程为:△F=13603C-4.5948,r=0.9992.对0.0400mg/L的壳聚糖平行测定9次,检出限为0.0350mg/L,RSD为2.70％.本方法具有简便易行、干扰小的特点,可用于壳聚糖医用制剂的含量检测和相关研究.     

双折叠模型对相互作用势实部的计算

用双折叠模型计算了核核碰撞的相互作用势, 其中核子-核子相互作用势采用M3Y-Reid和M3Y-Paris形式, 交换部分考虑了有限力程的密度依赖的核子-核子相互作用, 程序用于重离子散射光学势实部的计算. 回顾了折叠模型的普遍特征和讨论了理论计算过程, 对各种类型的核子-核子相互作用下计算的相互作用势进行比较, 发现双折叠模型对大部分系统相互作用势的实部取得了满意的结果. 因此这个工作为重离子相互作用势的折叠计算提供了很好的方法.     

卡塞格林系统调焦时成像晃动的研究

卡塞格林系统观测不同距离目标时需要用螺纹微调旋转次镜的方法来改变焦距以获得清晰的像,但次镜随螺纹旋转会导致系统成像的周期性晃动,这在许多高精度光学仪器中是不允许的。针对该问题,分析了系统成像周期性晃动的影响因素并给出具体的运算公式。通过具体事例结合工厂加工水平,分析出该加工精度下的最大可能偏差,若其不在仪器误差允许范围内,就需采用无旋转的次镜微调机构。结果说明,用旋转次镜的微调机构产生的晃动半径有0.65 mm,而用无旋转的次镜微调机构产生的晃动半径只有 0.13 mm,系统精度得到较大提高。     

采用Helmholtz共鸣器与悬臂梁压电换能器的声能采集器研究

针对环境中广泛存在的声能,提出了一种采用Helmholtz共鸣器和悬臂梁压电换能器的声能采集器。Helmholtz共鸣器对入射声压进行放大,放大后的声压引起共鸣器弹性薄壁振动,薄壁的振动传递到压电换能器产生电能输出。建立了带弹性壁的立方形共鸣器的等效集中参数理论模型,并与压电换能器的机电特性结合,分析了声能采集器的声-机-电转换原理,研究了声压、声波频率和负载阻抗对输出功率的影响,研究结果为此类声能采集器的优化设计及工程应用提供了一种可行的方法。实验中,声源通过声波导管输出声能,当共鸣器管口处的声压级为94 dB时,系统实测最大输出功率达240μW。该采集器不仅可作为声能自供能采集器,还可在较远距离为低能耗电子装置进行有源声供能。      

生物陶瓷铣削加工辅助支撑优化设计方法研究

基于氧化锆生物陶瓷正交铣削试验数据,采用多元线性回归方程建立铣削力经验预测模型,为辅助支撑结构优化设计有限元模拟提供铣削力加载参考;结合生物陶瓷力学特性,通过有限元分析探索铣削力不同加载位置对辅助支撑应力应变的影响规律,校核支撑强度,为模型导入CAM系统后辅助支撑的设计提供优化及设计准则.理论分析和生物陶瓷修复体实际加工情况表明,该设计方法进行生物陶瓷铣削加工辅助支撑设计具有有效性和可行性,为提高生物陶瓷铣削效率提供了一种思路和方法.     

High-power ultraviolet 278-nm laser from fourth-harmonic generation of an Nd:YAG amplifier in CsB_3O_5 crystal

We report on the experimental investigation and theoretical analysis of a nanosecond pulse high power ultraviolet(UV) 278 nm laser by fourth-harmonic generation(FHG) of a 1112-nm Nd:YAG amplifier in LiB_3O_5(LBO) and CsB_3O_5(CBO) crystals. The UV laser delivers a maximum average power of 10.3 W at 278 nm with peak power of 36.8 k W under input pump power of 41 W at 556 nm. This is, to the best of our knowledge, the highest output power at the specific UV wavelength of 278 nm. We also performed the theoretical investigation on the FHG with a model in the Gaussian approximation of both spatial and temporal profiles, especially accounting for the two-photon absorption effect in CBO crystal for the first time. The average output power, pulse width, and beam spatial distribution of the UV laser were simulated. The theoretical calculations are in close agreement with the experimental results.     

近垒重离子熔合反应中的中子转移效应(英文)

近势垒及其以下能区重离子熔合反应中的中子转移耦合道效应是一个复杂且有争议的问题。简要介绍了近年来在中国原子能科学研究院的HI-13串列加速器上,基于静电偏转板装置完成的32S+90,94,96Zr,18O+74Ge和18O+58Ni等几个典型体系的熔合反应研究情况,并结合耦合道理论对实验数据进行了分析。选取反应体系时同时关注了正Q值的中子拾取和削裂道。另外,基于完全耦合道理论计算,提出了一种能够定量提取熔合反应中中子转移效应的自洽方法。这些研究进一步证实了垒下重离子熔合反应中的中子转移效应,同时指出了其复杂性。需要进一步的实验和理论研究来澄清相关核反应机制。The effect of neutron transfers on near-and sub-Coulomb-barrier fusion of heavy-ions is still a complicated and controversial problem. This paper reviews the recent experimental results of the fusion excitation functions of several typical systems, which have been measured by using an electrostatic deflector setup at the HI-13 tandem accelerator of CIAE. Both the neutron pickup and stripping effects were studied. Moreover, a self-consistent method to reliably isolate the transfer effect quantitatively based on the coupledchannels calculation is proposed. These studies give a further support for the neutron transfer effect on sub-barrier fusion of heavy-ions and its complexity. Further experimental and theoretical studies are needed for clarifying the relevant reaction mechanisms.     

High power high beam quality diode-pumped 1319-nm Nd:YAG oscillator-amplifier laser system

This paper demonstrated a high power and high beam quality diode-pumped 1319-nm Nd:YAG master oscillator-power amplifier laser system. A thermally near-unstable resonator with four-rod birefringence compensation flat--flat cavity was adopted as the master oscillator. A solid etalon was inserted in the unidirectional ring resonator to compress the laser linewidth. Under a repetition rate of 500~Hz and pulse width of 160~\mus, the master oscillator delivers an average output power of 16.8~W at 1319~nm with linear polarisation, beam quality factor M^{2} = 1.16 and linewidth of 3.2~GHz. A double-pass power amplifier with two amplifier stages was employed for higher power scaling and the output power was amplified to be 25.9~W with M^{2} = 1.43.     

Systematic extraction of the strong absorption distance and Coulomb barrier from elastic scattering

The reduced strong absorption distance d_S and Coulomb barrier height V_B are extracted from the quarter-point recipe from a series of experimental elastic scattering angle distributions. The nuclei with different binding energies are systematically studied as the projectile, including the tightly bound, weakly bound, and halo nuclei. It is found that the mean d_S for halo nuclei is significantly larger than that of tightly and weakly bound nuclei. The complex behav...     

无限压电体内共线周期裂纹间的相互作用

研究了无限压电体内共线周期裂纹间的相互作用的问题,并且考虑了裂纹尖端的饱和条带作用．应用Stroh理论和保角变换方法,得到了共线裂纹的一般周期解A·D2对应力强度因子和饱和条带尺寸进行了理论推导,详细分析了它们与周期长和半裂纹长的比值h/l之间的关系．数值结果表明:1) 当h/l大于4.0时,裂纹之间的相互作用对应力强度因子影响较小,无限压电体内周期裂纹和单裂纹的值几乎相等．这表明当h大于4.0l时,建立裂纹扩展判据时可以近似忽略裂纹之间的相互作用;2) 周期裂纹的饱和条带尺寸趋近于单裂纹值的速度,取决于无穷远处的电载荷,通常无穷远处的电载荷越大,趋近速度越慢．