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91.
By controlling the reflux time and the quantity of the shell materials, different sizes of thioglycollic acid (TGA) modified
CdTe/CdSe core/shell quantum dots were synthesized in aqueous solution. This type of QDs was used for sensitive and selective
determination of ascorbic acid in commercial tablets. Under optimal conditions, a good linearity was observed between the
relative fluorescence (FL) intensity and the concentration of ascorbic acid in the range of 4.0 to 64.0 μg/mL with a correlation
coefficient of 0.9968. The limit of detection was 2.4 μg/mL. This method was applied to the determination of the ascorbic
acid in Vitamin C tablets and Vitamin C Yinqiao pills, and satisfactory results were obtained. 相似文献
92.
A stability analysis for the resistive wall mode is studied in the presence of trapped energetic particles (EPs). When the EPs' beta exceeds a critical value, a fishbonelike bursting mode (FLM) with an external kink eigenstructure can exist. This offers the first analytic interpretation of the experimental observations [Phys. Rev. Lett. 103, 045001 (2009)]. The mode-particle resonances for the FLM and the q=1 fishbone occur in different regimes of the precession frequency of EPs. In certain ranges of the plasma rotation speed and the EPs' beta, a mode conversion can occur between the resistive wall mode and FLM. 相似文献
93.
94.
基于抽取和连续投影算法的可见近红外光谱变量筛选 总被引:1,自引:0,他引:1
大多数短波CCD硅检测器为2 048或3 648像元,相邻波长间隔小,预处理算法对其适用性差.本文在600.09~980.47 nm光谱范围内,采用等间隔抽取方法重构光谱矩阵.经不同光谱预处理后,分别采用遗传算法(GA)和连续投影算法(SPA),筛选偏最小二乘法(PLS)建模变量.采用留一法交叉验证评价模型的预测能力,... 相似文献
95.
铕与4-(4-吡啶甲酰基)苯甲酸配合物的合成与荧光性能研究 总被引:2,自引:0,他引:2
以Eu3+为中心离子,4-(4-吡啶甲酰基)苯甲酸(HPFBA)、1,10-菲罗啉(Phen)和三苯基氧膦(TPPO)为配体,合成了新型配合物Eu(PFBA)3(H2O)4,Eu(PFBA)3Phen(H2O)3和Eu(PFBA)3TPPO(H2O)3(PFBA=4-(4-吡啶甲酰基)苯甲酸根).红外光谱表明,形成配合... 相似文献
96.
A simple sensor system for high spatial resolution distributed strain field measurement is proposed and demonstrated experimentally. The fiber loop ringdown technique combined with a linear chirped fiber Bragg grating is used to realize the high spatial resolution. A proof-of-concept distributed strain sensor with 2?mm spatial resolution is realized. The sensor network is also explored and researched experimentally. The proposed technique suggests a broad range of applications for real-time distributed physical parameter sensing, such as strain or temperature. 相似文献
97.
以建筑工程为研究对象,选取13项影响建筑工程质量因素的指标,运用解释结构模型(ISM)系统分析各因素之间的内在联系,并在此基础上建立4级多层次递阶结构模型,进一步精确描述各因素间的直接关系,从而直观地反映各因素间的层级关系及相互影响,并找到了影响建筑工程质量的根本原因,进而为改善我国建筑工程质量提供一定的参考依据. 相似文献
98.
Gnetifolin L and O, Two Dimeric Stilbenes from Gnetum Montanum 总被引:1,自引:0,他引:1
GnetuI)1monlanlImgr0wsinthes0uthernpart0fChinaandhasbeenusedf0rthetreatment0fbronchitisandarthritisinf0lkmedicinel.Previously,aninvestigationofthisspeciesledt0theis0lationofs0meaIkal0idsanddibenzyletherderivatives2.lnourstudies,tenc0mp0nentsincludingresveratr0l,is0rhapontigenin,daucoster0l,O-sitosterol,stearicacid,gnetif0linE,gnet0l,is0rhapontigenin-3-O-6-gluc0pyra(-)8-viniferinandgnetifolinCwere0btainedfromthisplant'.Inthefurtherstudy,f0urnewdimericstilbenesnamedgnetif0IinMandN',gnetifoli… 相似文献
99.
Qingkai Han·Lina Hao·Hao Zhang·Bangchun Wen School of Mechanical Engineering Automation Northeastern University Shenyang China 《Acta Mechanica Sinica》2010,(3)
This paper addresses a master-slave synchronization strategy for complex dynamic systems based on feedback control.This strategy is applied to 3-DOF planar manipulators in order to obtain synchronization in such complicated as chaotic motions of end-effectors.A chaotic curve is selected from Duffing equation as the trajectory of master end-effector and a piecewise approximation method is proposed to accurately represent this chaotic trajectory of end-effectors.The dynamical equations of master-slave mani... 相似文献
100.
Chen Guo Hao Wen Huizhou Liu 《中国颗粒学报》2005,3(6):310-316
In this paper we review our work on self-assembly of the system, poly(ethylene oxide)-poly(propylene oxide)-poly(elhylene oxide) (PEO-PPO-PEO) block copolymers, which is a kind of macromolecular complex fluids. The control of self-assembly could be obtained by adding inorganic salts or aliphatic alcohols. By self-assembly of amphiphilic block copelymers a microemulsion phase is formed which could be applied in micelle extraction, such as hollow-fiber membrane micelle extraction, magnetic micelle extraction and immobilized micelle extraction. 相似文献