多孔氧化铝模板催化制备定向碳纳米管阵列

Well-aligned open-ended multi-walled carbon nanotube (MWCNT) arrays were prepared via chemical vapor deposition (CVD) method in porous anodic aluminum oxide (AAO) templates without depositing any transition metals as catalyst. Effects of the CVD temperature and heat treatment were studied in detail.Well-aligned open-ended MWCNT arrays were obtained at the CVD temperature above 600 ℃; when CVD temperature is reduced to around 550 ℃, CNTs, CNFs and other structures existed at the same time; no CNTs or carbon nanofibres (CNFs) could be found as the CVD temperature is below 500 ℃, and only amorphous carbon in the porous AAO template was found. Experimental results showed that the AAO template is catalytic during the CVD process, and it has the following two effects: to catalyze thermal decomposition of acetylene and to catalyze conversion of carbon decomposed from acetylene into CNTs or CNFs. Heat treatment could improve the graphitization degree, but it might also introduce new defects.     

高性能、可弯曲碳纳米管纤维负载镍磷合金电催化析氢电极的研究

利用电化学沉积法在碳纳米管纤维(CNTFs)上沉积了镍磷合金,对比了不同循环圈数、不同镍磷比例下制备的碳纳米管纤维负载镍磷合金(Ni-P/CNTFs)电极在中性电解质溶液中的电催化析氢性能,发现当电沉积液中镍磷比为2:1时,沉积50圈时制备出的样品具有最佳的电催化析氢性能,产生10 mA·cm-2电流密度仅需138 mV过电势,塔菲尔(Tafel)斜率为83 mV·dec-1,同时具有良好的稳定性.并且在保持催化性能不变的前提下,样品可以进行弯曲,扩展了应用领域.     

Introducing Bt Gene Into Maize With Ovary Injection

It is reported here that Bt toxin gene has been successfully transferred into maize inbred line by ovary injection for the first time both at home and abroad. One transgenic plant (To) has been confirmed by Southern blotting and PCR test, and 71 progenies (T1) from T0 have been obtained through self-pollination. Of these 71 progenies, seven plants demonstrated positive results in the PCR test; four were used to feed Asian corn borer, and certain effect of insect-resistance was observed. The experiments on the ovary injection in Hainan Province have also been repeated, thus providing new chance to the application of genetic engineering to the maize improvement.     

纳米材料电化学与生物传感器——有机微污染物检测新途径

本文介绍了近年来纳米材料电化学与生物传感器在有机微污染物检测中的研究现状,分析了这些传感器中纳米材料修饰电极的特点,重点阐述了纳米材料在有机微污染物检测中的重要作用,列举了一些纳米材料电化学与生物传感器在有机微污染物检测中的应用。最后对纳米材料电化学与生物传感器用于有机微污染物的检测研究进行了简要评述和展望。     

BEPCⅡ低温控制系统研制

北京正负电子对撞机重大改造工程(BEPCⅡ)首次应用低温超导技术建造低温系统.低温控制系统通过控制前端低温系统的压力、液位、流量和功率等过程变量,分别产生饱和液氦、两相氦和过冷的单相液氦,使用这三种不同形式的氦流来冷却超导设备.低温控制系统采用EPICS+PLC双层架构体系,实现对前端低温超导设备的全自动控制.EPICS主要完成低温系统的过程控制、逻辑控制和PID闭环控制;PLC负责前端关键设备的联锁控制,用于保护低温超导设备的安全.     

完全r部图Kr（t）的{=C3，C2k}-强制分解（k≥4）的渐近存在性

研究基于顶点集V=Ui=1^rVi（其中｜Vi｜=t，i=1，2，……，r）的完全r部图Kr（t）的3圈和2k圈{C3，C2k}-强制分解（k≥4）的存在性问题．通过构造并运用Kr（t）的两种分解法，证明了Kr（t）的〈C3，C2k}-强制分解（k≥4）的渐近存在性，即对于任意给定的正整数k≥4，存在常数r0（k）=5k＋2，使得当r≥r0（k）时，Kr（t）的{C3，C2k}-强制分解存在的必要条件也是充分的．     

Si(111)分子束外延生长时RHEED强度振荡的观察

本文报道用反射式高能电子衍射的强度振荡测量来观察Si(111)衬底上分子束外延的生长行为,观察到了双原子层的振荡模式。振荡的衰减和恢复特性不同于Si(100)衬底上的生长行为,而同GaAs分子束外延时的特性非常相似。 关键词：     

同位素示踪法研究王冠—PVC膜钾离子选择性电极的响应机理

离子选择性电极的响应机理的报道较多,目前仍在进一步探讨中,但是采用示踪法者甚少。该法虽然难度较大。却具有直观和灵敏度高等优点。Thoma等采用~(42)K~+和~(36)Cl~-示踪法,对钾电极的离子传递机理进行了电渗析和扩散研究,结果表明钾离子和氯离子皆进入膜相中。Craggs、Jaber、Doyle、Moody和Thomas等经长时间的示踪试验,研究了~(45)Ca、~(36)Cl~-、~(89)Sr、~(133)Ba在由钙电极膜和钡电极膜分别组成的电池中的迁移和扩散特性,指出钡     

再议我国当代珠心算教育起源与发展的几个问题

珠心算是珠算的重要组成部分,研讨清楚珠心算起源、传承与发展的有关问题,很有必要。就此谈谈我们的一些看法。一、定义珠心算是讨论珠心算的前提珠心算是珠算式心算的简称。珠算式心算如何准确定义,有各种版本,主要有以下几种。《珠算科技知识》之解释是:"珠算式心算是一种不用算盘的纯意念式的心算。就是以珠算的形象和方法在大脑中进行的一种计算活动。""按照打‘实算盘’的     

Trapping of Neutral^87Rb Atoms on an Atomchip

We report an experiment of trapping of neutral ^87Rb atoms on a self-made atomchip. The H-shaped atomchip is made by magnetron sputtering technology, which is different from the atomchip technology of other teams. We collect 3×10^6 ^87Rb atoms in the mirror magneto-optical trap （MOT） using the external MOT coils, and 1×10^5 ^87 Rb atoms are transferred to U-MOT using U-shaped wire in chip and a pair of bias coils.