Investigation of the near-threshold cluster resonance in ~(14)C

An experiment for p(~(14)C,~(14)C~*→~(10)Be+α)p inelastic excitation and decay was performed in inverse kinematics at a beam energy of 25.3 Me V/u.A series of~(14)C excited states,including a new one at 18.3(1)Me V,were observed which decay to various states of the final nucleus of~(10)Be.A specially designed telescope system,installed around zero degrees,played an essential role in detecting the resonant states near theα-separation threshold.A state at 14.1(1)Me V is clearly identified,being consistent with the predicted band-head of the molecular rotational band characterized by theπ-bond linear chain configuration.Further clarification of the properties of this exotic state is suggested by using appropriate reaction tools.     

Geometric phase under the Unruh effect with intermediate statistics

Utilizing the geometric phase (GP) acquired in a quantum evolution, we manifest the thermality and quantum nature of the Unruh effect of an accelerating detector. We consider an UDW detector coupling to a conformal field in Minkowski spacetime, whose response spectrum exhibits an intermediate statistics of (1+1) anyon field. We find that comparing to an inertial moving detector, the GP in accelerating frame is modified after the nonunitary evolution of the detector due to the Unruh effect. We show that such modification can distinguish the different thermalizing ways of the detector, which depends on the scaling dimension of the conformal primary field. Finally, we estimate the difference between the GP under the Unruh radiation and that in a thermal bath for a static observer, which reveals the quantum origin of the Unruh effect rather than a conventional thermal noise.     

聚(碳酸酯-co-磷酸酯)的酶促合成及性能

以猪胰脂肪酶或假丝酵母皱褶酶为催化剂, 100℃下通过本体聚合成功地合成了三亚甲基碳酸酯(TMC)和2-乙氧基-2-氧-1,3-二氧磷杂环戊烷(EEP)的无规共聚物(poly(TMC-co-EEP)). 研究了酶浓度, 聚合反应时间以及共聚单体投料比等因素对共聚物分子量和产率的影响. 随着酶(PPL或CL)浓度的增加, 共聚物分子量降低. 同时, 随着EEP投料比的增加, 共聚物的分子量也降低. 共聚物数均分子量最大可达到10200. 随着共聚单体投料摩尔比(EEP/TMC)从0增加到5︰10, 共聚物的玻璃化温度从-28℃降低到-41.7℃. 体外降解实验表明: 共聚物中磷酸酯含量越高, 降解速率越快.     

对巧克力相变迟滞现象的理论解释——朗道-德冯谢亚理论以及铁电相变理论

巧克力作为生活中常见的事物，其储存方法一直是食品科学界研究的重要课题，而由相变产生的巧克力凝固和融化等现象对巧克力的储存产生了决定性的影响；但由于巧克力的成分复杂且晶体结构多变，目前只在生活中实现了控制巧克力保持良好性状的储存，而鲜少有研究分析其背后存在的相变机理。研究中首先基于朗道-德冯谢亚理论，使用序参量描述了影响相变的相关因素，初步解释了巧克力相变当中存在的迟滞现象；而后进行了相关实验，提出了一种对朗道理论的修正来解释实验现象；最后，通过研究巧克力的主要成分可可脂晶体的铁电相变，对德冯谢亚理论中未作出解释的势垒产生做出了阐述。     

基于定边对定角模型的同题异构

1引言定边对定角模型在初中数学阶段是最为常见的构造隐形圆方式之一,通常用于线段最值,面积最值.本文中是在定边对定角模型的背景下,着力对三角形周长最值问题进行同题异构,通过化折为直思想、构造隐形圆的方法完成周长最值的解决.     

模型炭催化加氢气化反应特性研究

在加压热天平中研究了活性炭/烟煤半焦/无烟煤半焦等模型炭催化加氢气化(CHG)的特性,并结合GC、BET等表征对炭的物理结构和化学反应过程的分析,初步获悉了Co对炭-氢反应的催化作用过程.结果表明,炭CHG过程中过渡金属(Fe、Co、Ni)的催化活性明显高于碱金属和碱土金属(K、CaO、MgO),过渡金属催化过程存在低...     

高效液相色谱法测定化妆品中黄芩甙

采用高效液相色谱法测定化妆品中黄芩甙含量。样品经乙醇-水(75+25)溶液萃取,用ZORBAX SB C18色谱柱(4.6 mm×25 cm,5μm)分离,用乙腈与磷酸(0.1+99.9)溶液以体积比22比78组成的混合溶液为流动相进行洗脱,在波长276 nm处检测。黄芩甙的质量浓度在100.0 mg.L-1以内与其峰面积呈线性关系,方法的检出限(3S/N)为4.5 mg.kg-1。方法用于化妆品中黄芩甙的测定,加标回收率在76.8%～104.9%之间。     

Drinfeld Twist and Symmetric Bethe Vectors of Open XYZ Chain with Non-Diagonal Boundary Terms

With the help of the Drinfeld twist or factorizing F-matrix for the eight-vertex solid-on-solid(SOS) model,we find that in the F-basis provided by the twist the two sets of pseudo-particle creation operators simultaneously take completely symmetric and polarization free form.This allows us to obtain the explicit and completely symmetric expressions of the two sets of Bethe states of the model.     

云南富源某地区土壤8种有效态元素的测定

一种DTPA土壤测试被成功开发并应用到云南富源某地区,以识别土壤中的有效锌、铁、锰、铜、铅、钴、镍和镉的含量,用于指导该地区的土壤施肥情况以获得作物的最大产量。提取剂由0.005molL-1DTPA(二乙烯三胺五乙酸)、0.1 molL-1三乙醇胺和0.001molL-1CaCl, pH为7.3。土壤测试包括用20ml的提取剂震荡10g风干土壤2小时,过滤渗滤液,用电感耦合等离子体发射光谱法测定滤液中的锌、铁、锰、铜、铅、钴、镍和镉。根据作物对锌、铁和锰等有效态的反应,土壤测试使用标准化的土壤准备、研磨和提取程序。提取剂在pH值7.30时得到缓冲,选用能有效地提取8种微量元素金属DTPA作为螯合剂。通过大量实验确定最佳的震荡时间是2h,最佳的水土比是2：1。通过实验,方法线性相关系数R＞0.99,国家一级标准物质的准确度、精密度和检出限满足云南富源地区土壤检测要求,确定了该的确的土壤检测方法,并通过加标回收实验,回收率在90%～110%之间。该方法绿色环保,简单快捷,准确度高,适合该地区土壤有效态的分析。