高温退火工艺对直流反应磁控溅射制备蓝宝石基氮化铝模板的影响

采用直流反应磁控溅射与高温退火工艺大批量制备了膜厚为200 nm、400 nm及800 nm的2英寸蓝宝石基氮化铝模板,并对高温退火前后不同膜厚模板使用各种表征手段进行对比分析.结果 表明:采用磁控溅射制备膜厚为200 nm的模板经高温退火后晶体质量得到显著提升,退火前后整片(0002)面和(10-12)面高分辨率X射线衍射摇摆曲线半高宽分别从632 ～ 658 arcsec和2 580 ～2 734 arcsec下降至70.9 ～ 84.5 arcsec和273.6 ～ 341.6 arcsec;模板5 μm×5μm区域内均方根粗糙度小于1 nm;紫外波段260 ～280 nm吸收系数为14 ～20 cm-1;高温退火前后拉曼图谱E2(high)声子模特征峰半高宽从13.5 cm-1降至5.2 cm-1,峰位从656.6 cm-1移动至657.6 cm-1,表明氮化铝模板内的拉应力经高温退火后得到释放,接近无应力状态.     

高亲和力抗eGFP纳米抗体的筛选与应用

将增强型绿色荧光蛋白（Enhanced Green Fluorescent Protein, eGFP）免疫羊驼后构建纳米抗体免疫库,固相淘选eGFP纳米抗体;构建E.coli Rosetta表达载体,诱导表达纳米抗体,并鉴定其结合活性及特异性;辣根过氧化物酶（Horseradish peroxidase, HRP）标纳米抗体,确定其工作浓度及稳定性;将纳米抗体与纳米磁珠偶联应用于免疫沉淀B13-EGFP融合蛋白。四免后抗血清滴度超过1.28×106,获得库容量为1.85×108 cfu的抗eGFP纳米抗体噬菌体展示文库;原核表达10种独特基因序列的纳米抗体,均为可溶性表达;采用ForteBio Octet确定出纳米抗体4-28与eGFP的亲和常数（KD）最高,达到9.67×10-11M;纳米抗体4-28与eGFP、绿色荧光蛋白（Green Fluorescent Protein, GFP）特异性结合;HRP标记纳米抗体4-28检测范围是1:10 000～1:25 000(浓度100～40 ng·mL-1),比市场上现有的检测二抗（稀释范围1:5 000～1:20 000）灵敏度更高;纳米抗体4-28偶联羧基化纳米磁珠,免疫沉淀B13-eGFP融合蛋白,实现了简单快速分离目的蛋白B13-eGFP。     

锂掺杂提高硫氰酸亚铜的电学特性及在钙钛矿太阳电池中的应用

高效钙钛矿太阳电池中通常采用有机p型半导体材料作为空穴传输层.有机材料在湿度、温度、紫外照射等环境因素下会出现严重的性能衰退,加速钙钛矿太阳电池的老化,成为实现其实际应用的主要障碍之一.本文提出采用无机硫氢酸亚铜(CuSCN)作为空穴传输材料,并通过锂掺杂提高其空穴传输特性;在此基础上采用聚[双(4苯基)(2,4,6-三甲基苯基)胺]修饰CuSCN表面,避免CuSCN和碘化铅(PbI₂)间的相互作用,实现了大晶粒、致密钙钛矿薄膜的制备,最终实现了钙钛矿太阳电池性能的有效提升.本工作为稳定、高效钙钛矿太阳电池的制备提供了可借鉴的策略.     

高精度光学对准测量装置的设计

设计了一套光学对准测量装置,该装置主要由面阵CCD相机、光学镜头、图像处理模块、LED红光光源、球面反光镜组成。介绍了测量原理,测量目标采用等腰三角形排列,通过面阵CCD对目标所反射的图像进行采集,由图像处理模块对该图像进行实时处理,能够同时得到X、Y、Z以及旋转角度等四维坐标数据。推导了光斑图像坐标和被测平面距离等计算公式,并进行了对准精度分析。结果表明,该装置位置误差〈1mm,角度误差为0．24°,实现了高精度、自动、快速对准测量。     

Device research on GaAs-based InAlAs/InGaAs metamorphic high electron mobility transistors grown by metal organic chemical vapour deposition

This paper applies a novel quad-layer resist and e-beam lithography technique to fabricate a GaAs-based InAlAs/InGaAs metamorphic high electron mobility transistor (HEMT) grown by metal organic chemical vapour deposition (MOCVD). The gate length of the metamorphic HEMT was 150~nm, the maximum current density was 330~mA/mm, the maximum transconductance was 470~mS/mm, the threshold voltage was -0.6~V, and the maximum current gain cut-off frequency and maximum oscillation frequency were 102~GHz and 450~GHz, respectively. This is the first report on tri-termination devices whose frequency value is above 400~GHz in China. The excellent frequency performances promise the possibility of metamorphic HEMTs grown by MOCVD for millimetre-wave applications, and more outstanding device performances would be obtained after optimizing the material structure, the elaborate T-gate and other device processes further.     

激光对电视成像跟踪系统的软杀伤效应研究

分析了电视成像跟踪系统的组成原理,在开展脉冲激光干扰CCD的实验基础上,进行了激光对电视成像跟踪系统的软杀伤实验与理论分析。实验指出,激光对电视成像跟踪系统的软杀伤主要是对CCD光电探测系统的软杀伤,软杀伤效果如何与激光成像是否位于跟踪系统的波门之内有很大关系。     

The research on suspended ZnO nanowire field-effect transistor

This paper reports that a novel type of suspended ZnO nanowire field-effect transistors (FETs) were successfully fabricated using a photolithography process, and their electrical properties were characterized by I--V measurements. Single-crystalline ZnO nanowires were synthesized by a hydrothermal method, they were used as a suspended ZnO nanowire channel of back-gate field-effect transistors (FET). The fabricated suspended nanowire FETs showed a p-channel depletion mode, exhibited high on--off current ratio of ～10⁵. When V_DS=2.5 V, the peak transconductances of the suspended FETs were 0.396 μS, the oxide capacitance was found to be 1.547 fF, the pinch-off voltage V_TH was about 0.6 V, the electron mobility was on average 50.17 cm²/Vs. The resistivity of the ZnO nanowire channel was estimated to be 0.96× 10²Ω cm at V_GS = 0 V. These characteristics revealed that the suspended nanowire FET fabricated by the photolithography process had excellent performance. Better contacts between the ZnO nanowire and metal electrodes could be improved through annealing and metal deposition using a focused ion beam.     

夹具对复合材料加筋板剪切试验屈曲载荷的影响

复合材料加筋板在剪切载荷作用下的屈曲和后屈曲性能试验是难度较高的结构试验,载荷通常需要由设计合理的夹具传递到试件上,本文采用的是对拉式的剪切试验夹具.在试验中,由于引入的夹具是弹性体,与试件结合成一体,参与了屈曲过程,所以与理想的约束情况有差异.本文采用数值方法,模拟夹具对试验结果的影响,发现不同的夹持模型,对屈曲载荷...     

基于灰度相关的图像匹配算法的改进

针对目前图像匹配算法中存在的匹配精度不高和匹配速度慢的缺点，对基于灰度相关的2类匹配算法——最小误差法和相关系数法进行了改进。最小误差法采用新的ML距离法，提出动态调整阈值的方法，既保证了匹配精度，又避免了局部噪声的影响；相关系数法对相关系数的计算公式进行了简化，并采用三步搜索策略进行匹配，以达到减少计算量和搜索位置的目的。实验证明：改进后的算法，在保证一定匹配精度的条件下，匹配速度大大提高，能够满足实际应用中的实时性要求。     

Realization of an All-Fibre Self-Organization Intra-Cavity Coherent Erbium-Doped Fibre Laser

An intra-cavity coherent coupling Michelson Er-doped fibre （EDF） laser （MCEDFL） is proposed and demonstrated. Characteristics of the MCEDFL are investigated. It is found that the MCEDFL with a polarizer can be coherent combined effectively. By the experiment based on fibre Bragg gratings （FBGs） with different reflectivity, we find that the reflectivity of the FBG play a vital role in improving the performance of the MCEDFL. This outcome adequately shows many favourable features, such as high efficiency, easy operation, and simple all-fibre configuration.