火花熔蚀-电感耦合等离子体光谱法分析地质矿物

火花熔蚀-电感耦合等离子体光谱法(SA-ICP)用于测量锆石中铪-锆比值和锰铁矿瘤中的铈、钴、铁、铅、镍和磷。用信背比和信嗓比的序贯单纯形优化法建立了用于高压火花和氩气ICP系统的六个操作参数。将磨细的样品与铜压成饼,从样品中熔蚀出的分析物和基体元素的原于发射信号的时间相关性给出一种用火花来作选择取样的方法。测量锆石中的铪、锆浓度比的精密度为4%(相对标准偏差)。对于锰铁矿瘤,根据分析线对锰(Ⅱ)257.610纳米线强度比的光谱测量结果达到分析精密度范围为7-14%(相对标准偏差)。分析的准确度用参比物USGS诺得(Nod)P-1的标准物加入法来决定,而与锰浓度的测量无关。     

脉冲星射电光度的估计及其演化规律的研究

本文从极冠模型出发导出辐射束的强度分布和新的光度公式.新的光度公式无需对磁倾角和视线扫过辐射束的部位作出假定,采用新的射电光度值来研究光度的演化规律,发现在周期和周期变率的整个取值范围内射电光度可以用关系式L∝(B/P²)^1.1和L∝Q’^-1.4来描写.这和近几年流行的光度规律不同.     

PROMOTION EFFECT OF PYRIDINE FOR THE DIRECT ELECTROCHEMISTRY OF CYTOCHROME C AT GOLD ELECTRODES

It was found for the first time that the compounds with only one functional group, such as pyridine, can show the promotion effect for the electrochemical reaction of cytochrome C at gold electrodes.     

穆斯堡尔谱学三十年

 穆斯堡尔在阅读自己关于¹⁹¹Ir共振的第一篇文章时突然意识到,他可以直接由多谱勒位移实验来确定自然宽度的谱线--他预见到会有一场竞争.他把文章送到在他看来“没有多少人阅读的德文《自然科学》杂志上”发表.当立即有二百多人来索取复印本时,他“迅速意识到这竟是犯了一个多么大的错误”.他因发现这种“无反冲γ射线共振吸收效应”,获得1961年诺贝尔物理奖.鲁道夫·路德维希·穆斯堡尔生于1929年1月31日.他在一些工业实验室花费了一年时间,后来进入慕尼黑工业大学,1952年完成学位课程,1954年完成了他的论文.1955-1957年,他到马克斯-普朗克医学研究所从事研究工作,1958年在慕尼黑工业大学获得博士学位.     

随机删失下乘积限过程和累积失效率过程振动模的局部渐近性

在随机删失下研究了乘积限过程和累积失效率过程的振动模的局部性质 .给出了这两个过程的振动模的重对数律 ,并应用这些结果得到了几种核密度估计和Bahadur-Kiefer过程的精确收敛速度     

Residual stress profiling of an aluminum alloy by laser ultrasonics

A residual-stress profile along the thickness of an aluminum alloy sheet is determined by laser-ultrasonic technique. Surface acoustic waves are generated by a Nd:YAG pulse laser and detected by a Heterodyne interferometer on a lateral free surface of the sheet. The distribution of residual stress is determined by measuring the relative variation of the wavevelocities at different location of the sample along its thickness. This technique is validated by three different residual stress profiles obtained experimentally.     

PERMANENCE AND GLOBAL STABILITY TO A NONAUTONOMOUS NONLINEAR DISCRETE SINGLE SPECIES SYSTEM

In this paper,we study some permanence and global stability to a nonau- tonomous nonlinear discrete single species system,and obtain some sufficient condition of global stability to the system.     

Characterization of planar photonic crystals using surface coupling techniques at large wavelengths

We report a non-destructive characterization of planar two-dimensional(2D)photonic crystals(PhCs) made in silicon on insulator(SOI)wafers using ellipsometric or Fourier transformed infrared(FTIR) spectroscope.At large wavelengths,devices behave as homogeneous isotropic materials defined by an effective filling factor.The experimental results related to the PhC limited dimensions confirm this characterization.     

OSCILLATION FOR NONAUTONOMOUS NEUTRAL DYNAMIC DELAY EQUATIONS ON TIME SCALES

The article is concerned with oscillation of nonautonomous neutral dynamic delay equations on time scales. Sufficient conditions are established for the existence of bounded positive solutions and for oscillation of all solutions of this equation. Some results extend known results for difference equations when the time scale is the set Z of positive integers and for differential equations when the time scale is the set R of real numbers.     

STABLE SOLUTION OF TIME DOMAIN INTEGRAL EQUATION METHODS USING QUADRATIC B-SPLINE TEMPORAL BASIS FUNCTIONS

This paper is concerned with stable solutions of time domain integral equation （TDIE） methods for transient scattering problems with 3D conducting objects. We use the quadratic B-spline function as temporal basis functions, which permits both the induced currents and induced charges to be properly approximated in terms of completeness. Because the B-spline function has the least support width among all polynomial basis functions of the same order, the resulting system matrices seem to be the sparsest. The TDIE formula-tions using induced electric polarizations as unknown function are adopted and justified. Numerical results demonstrate that the proposed approach is accurate and efficient, and no late-time instability is observed.