四溴双酚A锑铝双金属化合物的合成及其阻燃性能

以四溴双酚Ａ（ＴＢＡ）合成了在水和空气中稳定的四溴双酚Ａ合锑铝双金属化合物（ＴＢＡＳＡ）．通过ＩＲ、１ＨＮＭＲ和元素分析予以表征，并研究了其对聚乙烯（ＰＥ）和聚环氧乙烷（ＰＥＯ）的阻燃性能．结果表明，这种分子中含有溴、锑和铝的化合物，对聚乙烯和聚环氧乙烷等高聚物材料有高的阻燃性能与消烟效果．     

Two New Diterpene Acetylxylosides from Aster veitchianus

Two new acetylxylosides,ent-manool-13-O-β-D-2′-acetylxylopyranoside(1)and entmanool-13-O-β-D-2′,4′-diacetylxylopyranoside(2)were isolated from Aster veitchianus.Their structures were elucidated by spectroscopic methods.     

Relations among eigenvalues of Sturm-Liouville problems with different types of leading coefficient functions

For any Sturm-Liouville problem with a separable boundary condition and whose leading coefficient function changes sign (exactly once), we first give a geometric characterization of its eigenvalues λn using the eigenvalues of some corresponding problems with a definite leading coefficient function. Consequences of this characterization include simple proofs of the existence of the λn's, their Prüfer angle characterization, and a way for determining their indices from the zeros of their eigenfunctions. Then, interlacing relations among the λn's and the eigenvalues of the corresponding problems are obtained. Using these relations, a simple proof of asymptotic formulas for the λn's is given.     

Two New Ionone Derivatives from Rhododendron przewalskii Maxim

Two new ionone derivatives,named rhododendrone and rhododendronside,were isolated from the alcohoilc extract of the aerial parts of Rhododendron przwalskii Maxim.Their structures were elucidated on the basis of spectroscopic analysis.     

Solitary wave solutions of nonlinear financial markets :data-modeling-concept-practicing

This paper seeks to solve the difficult nonlinear problem in financial markets on the complex system theory and the nonlinear dynamics principle, with the data-model-concept-practice issue-oriented reconstruction of the phase space by the high frequency trade data. In theory, we have achieved the differentiable manifold geometry configuration, discovered the Yang-Mills functional in financial markets, obtained a meaningful conserved quantity through corresponding space-time non-Abel localization gauge symmetry transformation, and derived the financial solitons, which shows that there is a strict symmetry between manifold fiber bundle and guage field in financial markets. In practical applications of financial markets, we have repeatedly carried out experimental tests in a fluctuant evolvement, directly simulating and validating the existence of solitons by researching the price fluctuations (society phenomena) using the same methods and criterion as in natural science and in actual trade to test the stock Guangzhou Proprietary and the futures Fuel Oil in China. The results demonstrate that the financial solitons discovered indicates that there is a kind of new substance and form of energy existing in financial trade markets, which likely indicates a new science paradigm in the economy and society domains beyond physics.      

Modulation of Spin Distribution and Spin Transport by a Magnetic Field in a Quasi-One-Dimensional System with Spin--Orbit Coupling

The distributions of spin and currents modulated by magnetic field in a transverse parabolic confined two-dimensional electronic system with a Rashba spin--orbit coupling have been studied numerically. It is shown that the spin accumulation and the spin related current are generated by magnetic field if the spin--orbit coupling is presented. The distributions of charge and spin currents are antisymmetrical along the cross-section of confined system. A transversely applied electric field does not influence the characteristic behaviour of charge- and spin-dependent properties.     

四方相氧化锆纳米粉的低温合成与表征

氧化锆材料是近年来备受关注的陶瓷材料之一.它在许多不同的领域,诸如陶瓷颜料、工程陶瓷、宝石业、压电元件、离子交换器以及固体电解质方面等有着广泛的用途[1].其最常用的性质是其晶相转变时会有效改善陶瓷的脆性,因此在室温下保持其四方相是其中的关键.为此许多研究都侧重在其中加入各种添加剂,利用水热法、包裹法、形成共溶体等方法来阻止其晶格的转化[2-4].但研究也发现:在固定组成陶瓷基体中,ZrO2的相变温度随粉体颗粒直径的减小而降低,当颗粒足够小时能够提高材料强度的四方ZrO2可以保存到室温甚至室温以下.因此,减小ZrO2粉体粒度对于提高材料强度是非常有利的.本实验采用一种新的低温固相反应的方法制备氧化锆超细粉,从而使这种重要的陶瓷原料的制备有了新的思路.     

EAST װ�ñ�Ե����ģϸ˿��ȵĸ���CCD�ɼ������ϵͳ���

The high speed CCD visible-light camera system has been installed to detect the dynamic characteristics of ELMs filaments on EAST tokamak. In order to convert the CCD video imaging coordinates into real space coordinates, the CCD system has calibrated using Tsai’s two-stage calibration technique. A raised spike in the grayscale profile, drawn by selecting the grayscale value of the image in the vertical direction of the ELMs filament in the CCD image, represents an ELMs filament structure whose positional coordinates are determined by the apex of the spike. The Sobel edge detection operator was used to examine the edge profile of the filament to obtain the width of the filament. By analyzing the characteristics of the filament width of the ELMs, it is found that the width of ELMs filaments continuously decreases outward from the outermost magnetic surface. This indicates that the filaments continue to dissipate energy and particles as they propagate outward. The width of filaments of Type-I ELMs is greater than that of Type-III ELMs.     

Mode equation and its solution for dielectric waveguide with parabolic cross-section

The mode equation for the dielectric waveguide with parabolic cross-section is derived using both the effective index method and WKB theory, and the expression of the mode propagation constant or effective index is solved directly from this mode equation, so that the mode-propagation properties of this kind of waveguide can be analysed conveniently with comparative accuracy.     

激光谐振腔内光学元件的热光效应

本文分析了多模激光束加热内腔元件所引起的温度场分布及热聚焦效应。计算得到的LiNbO₃寻常光和非常光的输入功率-输出功率曲线与Konvisar等人的实验结果符合,修正了他们计算的非常光曲线。在实验上,也观测了LiNbO₃的内腔热光滞后现象,并测量了内腔热光聚焦效应。 关键词：