热熔还原法制备超硬复合相氮化碳及其工艺探索

本文采用热熔还原法,以聚氯乙烯、氯化铵、氧化铁为原料制备复合超硬相氮化碳(α/β-C3 N4).采用X射线衍射仪(XRD)、扫描电子显微镜(SEM)以及透射电子显微镜(TEM)对样品进行表征.在此基础上分析了不同温度和原料配比下合成复合相C3 N4的物相组成及形貌变化.结果表明样品形貌随着原料配比的不同在颗粒、棒状、纳米线之间转变.当C、N和Fe之间摩尔比为3:4:0.4时,所制备出的样品呈纳米线状,纳米线的直径约为15 nm,结晶性良好.而在其它配比下,只能获得棒状或颗粒状α/β复合相C3 N4.     

A limiting weak type estimate for capacitary maximal function

A capacitary analogue of the limiting weak type estimate of P. Janakiraman for the Hardy–Littlewood maximal function of an L¹(Rⁿ)$L^1({\mathbb{R}}^n)$-function (cf.  and ) is discovered.     

On Ringel–Hall Algebras of Tame Hereditary Algebras

In this paper, the double Ringel–Hall algebras of tame hereditary algebras are decomposed as the quantized enveloping algebras of the infinite-dimensional Lie algebras, which are the central extensions of the affine loop algebras and the infinite-dimensional Heisenberg algebras. The numbers of the generators of the Heisenberg algebras are explicitly given at each dimensional level.     

2005年分析化学与化学分析国际会议(Ⅱ)

本届大会的论文续报如下： （38）乌克兰Chmilenko FA等,合成的和天然的聚合物对偶氮类染料分析性能的影响;（39）乌克兰Fedenko V S,基于显色反应的花青素与金属离子络合的研究;（40）俄罗斯Finkelstein A L等。在X射线荧光光谱技术中所用的粉末状和粉浆状材料的一般描述;（41）俄罗斯Kartsova L A等,应用毛细管区带电泳技术测定绿茶浸出液中多酚对映体;     

Zinc Stannate Nanostructures for Energy Conversion

To date,ternary metal oxide semiconductor materials have attracted extensive attention worldwide due to their unique optoelectronic properties.As a classical ternary oxide,Zn2SnO4 is featured with the high electron mobility,wide band gap,negligible visible light absorption and tailorable electronic band structures.Thus,it is an ideal material for practical use in solar cells,lithium batteries,sensors,and photo-catalysts.In this review,we summarize the recent research progress of this material with the focus on the synthesis methods,nanostructures,and the resulting effects on the crystal structure,optical properties,and photoelectrochemical properties.Moreover,their potential applications in different devices are highlighted and carefully discussed.     

混合染料荧光选择性增强受激拉曼散射Stokes波

报道用不同混合比的罗丹明6G(R6G)和罗丹明B(RB)混合染料荧光选择性放大CCl₄和苯的受激拉曼散射不同阶次Stokes波。CCl₄二至五阶Stokes波分别被混合摩尔比为20∶2,20∶13及20∶40(R6g∶RB)的R6G和RB的混合染料荧光放大;一阶Stokes波强度被混合溶液削弱。这是由于到二至五阶Stokes波分别位于以上三种混合溶液荧光峰附近,并且都远离了R6G和RB的吸收峰,混合溶液的荧光增强作用大于吸收作用,因此这几阶Stokes被混合溶液荧光放大。而CCl₄的一阶Stokes位于RB吸收峰附近,又远离各混合溶液荧光峰,溶液的吸收作用大于荧光增强作用,导致一阶Stokes被混合溶液削弱。文章还报道了苯的一、二和三阶Stokes波分别被不同混合比的R6G和DCM的混合乙醇溶液放大,并预测了该方法应用前景。     

Experimental synchronization of independent entangled photon sources

We report the generation of independent entangled photon pairs from two synchronized but mutually incoherent laser sources. The quality of synchronization is confirmed by observing a violation of Bell's inequality with 3.2 standard deviations in an entanglement swapping experiment. The techniques developed in our experiment are not only important for realistic linear optical quantum-information processing, but also enable new tests of local realism.     

基于BF3正比管的宽量程脉冲中子探测技术

介绍了一种基于BF3正比计数管的宽量程脉冲中子探测技术。该技术采用多通道、组合式的BF3管阵列中子探测器组,以适应产额变化范围较宽的脉冲中子测试场合,并同时兼顾测量下限。基于该技术研制了一套BF3阵列中子探测系统并应用于脉冲中子源的测试,实验结果表明,该系统的脉冲中子测量范围可达5个数量级(56~8106),测量下限低、输出信号清晰,证明了该技术的可行性和有效性。