苯胺蓝-溴酸钾体系催化分光光度法测定水中痕量亚硝酸盐

在硫酸介质中,亚硝酸盐对溴酸钾氧化苯胺蓝褪色反应有明显的催化作用,据此提出了测定痕量亚硝酸盐催化分光光度方法。优化的试验条件如下:1 1.0mol·L-1硫酸溶液的用量为1.8mL;2 3×10-4 mol·L-1苯胺蓝溶液用量为1.5mL;3 0.02mol·L-1溴酸钾溶液用量为1.1mL;4反应温度为30℃。该方法的线性范围分别为0.01~0.2mg·L-1和0.2~1.0mg·L-1,检出限(3s/k)为4.6×10-6g·L-1。方法用于水样的分析,回收率在96.0%~104%之间,测定值的相对标准偏差(n=6)在1.6%~2.3%之间。     

我国注蒸汽采油研究进展

注蒸汽采油方法是提高原油采收率的有效手段之一,我国蒸汽驱油和蒸汽吞吐技术已相对成熟,取得了较大发展,本文概述了注蒸汽采油主要方法,从基础理论研究、室内实验研究、现场试验及推广应用等方面对我国近年来注蒸汽采油研究现状进行综述,提出在进一步的研究中,要重视降低蒸汽成本、改善注入环境污染等问题。     

激光驱动磁重联过程中的喷流演化和电子能谱测量

利用神光Ⅱ激光器和日本大阪大学Gekko激光器构建了激光驱动等离子体磁重联过程. 在垂直于磁重联平面方向发现了高速喷流, 从不同观测方向实验证实了该喷流的存在并测量了喷流的流体力学演化过程, 对其中的电子能谱进行了诊断分析.     

一种含有咔唑功能基团的有机聚磷腈的合成与表征

采用传统的亲核取代反应的方法合成了一种新有含有咔唑侧基的有机磷腈高分子，并用红外、＾１Ｈ核磁、紫外、热失重、差热分析了其结构，它的玻璃化转变温度为９１．６℃，大大低于聚乙烯咔唑的玻璃化转变温度。     

霍尔位置传感器测量固体材料的杨氏模量

用自制霍尔位置传感器与梁弯曲法测杨氏模量装置相结合，研制成固体材料杨氏模量测定仪，简述仪器结构、原理和实验方法。     

核物理实验中模数转换器选型及其供电方案

分析了核物理实验的特点及其对模数转换器(ADC)的要求,比较了3种ADC芯片的主要技术指标,选取了具有逐次逼近寄存器型架构和16位分辨力的ADS8472作为采集芯片,其微分非线性和积分非线性分别是±0.50 LSB(最低有效位,least significant bit)和±0.65 LSB.根据该芯片在实际电路中的应...     

Improved Photoluminescence in InGaN/GaN Strained Quantum Wells

The influence of strain accumulation on optical properties is investigated for InCaN/CaN-based blue lightemitting diodes grown by metal organic vapor-phase epitaxy. It is found that it is possible to reduce the strain relaxation and hence the nonradiative recombination centers in InCaN multi-quantum wells （MQWs） byadopting more InCaN/CaN MQWs pairs. The alleviation of strain relaxation in a superlattice layer results in the crystalline perfection and effective quality improvement of the epitaxial structures. With suitable control of the crystalline quality and reduced strain relaxation in the MQWs, there shows a 4-fold increase in light output luminous efficiency as compared to their conventional counterparts.     

基于深度学习的混沌加密灰度图像重建方法

混沌加密由于其初始值敏感性、伪随机性和运动轨迹的不可预测性而被广泛应用于图像加密领域。提出了一种通过深度学习来攻击Lorenz混沌加密系统的灰度图像重建方法,通过残差网络实现了对一系列明文-密文对数据集进行训练,从而拟合出密文到明文的过程,然后将训练好的网络应用在独立于训练集的密文上,恢复出与明文非常接近的图像。数值仿真结果验证了这种灰度图像重建方法的有效性。     

A cDNA CLONE WITH ANTIONCOGENE ACTIVITY

A cDNA clone, p14--6, which has an antioncogene activity on the v--Ki--Ras oncogene-transformed malignant cell line DT, was found. This clone was recovered from the revertantR14 cells, which had been isolated by transfections of DT cells with a normal human fibro-blast cDNA library cloned in pcD2, an Okayama-Berg vector. When transfected into DT cells,p14--6 clone gave rise to phenotypical flat reversion in 5--15% of DT transfectant colo-nies. The p14--6--transfected flat cell line, RR, was proven to be a true revertant with signif-icantly reduced malignancy by in ritro and in riro malignancy tests. All other clones recov-ered from R14 cells were unable to cause this reversion. Molecular hybridizations showedthat the p14--6 was inserted into RR genome as tandem repeats, and no structural changewas found in the D--Ki--Ras oncogene in RR genome. These facts suggest that the antioncogeneactivity of the p14--6 clone on the DT cells may be exerted through expression of thecDNA contained in this clone. Possib