含脱羧脱氢松香基的1,2,4-三唑并[3,4-b]-1,3,4-噻二唑衍生物的合成、表征及抑菌活性

用POCl3为催化剂和脱水剂,3-取代-4-氨基-5-巯基-1,2,4-三唑4和10分别与脱氢松香酸1反应制得14种未见文献报道的3-取代-6-(4′-脱羧脱氢松香基)-1,2,4-三唑并[3,4-b-]-1,3,4-噻二唑衍生物]5a~5e和11a~11i;所有化合物的结构均经IR、¹H NMR、¹³C NMR 和MS测试技术分析确认。 抑菌活性测试表明,目标化合物对白色念珠菌(C.Albicans)、大肠杆菌(E.Coli)、藤黄微球菌(M.Luteus)和痢疾志贺杆菌(S.Dysenteriae)均有一定的抑制作用。     

磁流变阻尼器半主动控制方法的实验研究

由于磁流变阻尼器是一种高度非线性的装置,因此建立与之相适应的控制系统是半主动控制问题的关键。本文采用改进的Bingham模型建立了磁流变阻尼器的动力学特性模型,根据天棚阻尼开关控制、天棚阻尼连续控制和模糊控制三种控制方法,确立了从系统速度响应到磁流变阻尼器励磁电流之间的关系,并开发了一套半主动控制系统。在一个两自由度的简化车辆试验平台上进行半主动控制试验,对比研究了三种控制方法的控制效果。实验结果表明,在1.3Hz~2.0Hz的低频段内,开关控制的最佳减振效果为15.1%,连续控制的最佳减振效果为14.9%,模糊控制的最佳减振效果为20.1%。可见,三种控制方法都能有效的减小车体的振动,模糊控制的减振效果最佳。     

非水相酶促肽合成的研究进展

生物活性肽 ,特别是寡肽 ,在免疫调节、激素调节、酶抑制、抗菌、抗病毒等方面有很大的应用潜力[1] .另外 ,调味肽也越来越显示出其在应用上的重要性 .肽作为一种终产品或者前体物质 ,在食品和药物生产上的商业潜力非常巨大 ,从而促进了肽合成的研究和发展 .目前肽合成主要有 3种方法 :化学法、重组DNA技术、酶法 .每种方法都有其优点和缺点 .总体上来说 ,在工业上化学法仍然使用得最多 ,其热力学动力学模型已经很好地建立起来 ;重组 DNA技术 ,由于需要一个长期、昂贵的研究和发展阶段 ,而且在发酵阶段存在表达效率低和产品提取回收困难…     

Linear Chemical Potential Dependence of Two-Quark Condensate

By differentiating the inverse dressed quark propagator at finite chemical potential μ with respect to μ, the linear response of the dressed quark propagato r to the chemical potential can be obtained, From this we extract a modelindependent formula for the linear chemical potential dependence of the in-medium two-quark condensate and show by two independent methods （explicit calculation and Lorentz covariance arguments） that the first-order contribution in μ to the in-medium two-quark condensate vanishes identically. Therefore if one wants to study the in-medium two-quark condensate one should expand to at/east the second order in the chemical potential μ.     

A Modified Approach for Calculating Dressed Quark Propagator at Finite Chemical Potential

Based on the rainbow approximation of Dyson-Schwinger equation and the assumption that the full inverse quark propagator at finite chemical potential is analytic in the neighborhood of μ = 1, it is proved that the dressed quark propagator at finite chemical potential μ can be written as G0^-1 [μ] =iγ·p↑-A（p↑-^2） ＋B（p↑-^2） with p↑-μ= （p↑-p4 ＋iμ）. From the dressed quark propagator at finite chemical potential in Munczek model the bag constant of a baryon and the scalar quark condensate are evaluated. A comparison with previous results is given.     

DBM-FsaA的合成及在热镀锌合金中微量铈分析的应用

锌合金中微量铈含量的测定,由于大量Zn^2 的存在而产生干扰,给选择合适的测定方法带来困难。虽然在分光光度法方面有关铈的微量分析研究已有报道,应用的显色剂主要有偶氮砷类,偶氮氯磷类等。但对于给定锌合金这一材料体系中微量铈的测定却少有报道。     

梨小食心虫性信息素的新法合成

梨小食心虫 (Grapholia molesta)是一种世界性果树害虫 ,主要危害梨、桃和苹果等果树 . 1 96 5年Geroge等 [1] 从该雌蛾腹部分离得到其性信息素 . 1 96 9年 Roelofs等 [2 ] 鉴定其结构为 8(Z/E) -十二碳烯 - 1 -醇乙酸酯 (6 ) .国内外对其生物活性进行了大面积田间试验 ,并用于     

Susceptibilities of QCD Vacuum from Renormalized Dyson-Schwinger Equations

The pion and tensor vacuum susceptibilities are calculated in the framework of the renormalizable Dyson-Schwinger equations. A comparison with the results of other nonperturbative QCD approaches is given.     

石墨炉原子吸收光谱法测定苦黄注射液及其中药材中的铅和镉

应用石墨炉原子吸收光谱（GF-AAS）法测定了苦黄注射液及其生中药材中铅及镉量。试样用浓硝酸及过氧化氢消解。对仪器的工作条件,包括波长、光谱带宽、灰化温度及原子化温度,作了试验和优化。选用柠檬酸作为基体改进剂,对大黄、茵陈、柴胡、苦参及“苦黄”注射液等试样中的铅及镉量作了测定,分析结果的相对标准偏差均小于4．4％。按标准加入法作了回收率试验,测得值在96%～110％之间。     

Linear Chemical Potential Dependence of Two-Quark Condensate

By differentiating the inverse dressed quark propagator at finite chemical potential μ with respect to μ, the linear response of the dressed quark propagator to the chemical potential can be obtained. From this we extract a modelindependent formula for the linear chemical potential dependence of the in-medium two-quark condensate and show by two independent methods (explicit calculation and Lorentz covariance arguments) that the first-order contribution in μto the in-medium two-quark condensate vanishes identically. Therefore if one wants to study the in-medium two-quark condensate one should expand to at least the second order in the chemical potential μ.