具有裂纹-碰摩耦合故障转子-轴承系统的动力学研究

以非线性动力学和转子动力学理论为基础，分析了带有碰摩和裂纹耦合故障的弹性转子系统的复杂运动，在考虑轴承油膜力的同时构造了含有裂纹和碰摩故障转子系统的动力学模型。针对短轴承油膜力和碰摩-裂纹转子系统的强非线性特点，采用Runge-Kutta法对该系统由碰摩和裂纹耦合故障导致的非线性动力学行为进行了数值仿真研究，发现该类碰摩转子系统在运行过程中存在周期运动、拟周期运动和混沌运动等丰富的非线性现象，该研究结果为转子-轴承系统故障诊断、动态设计和安全运行提供理论参考。     

TBHP/TEMPO-Mediated Oxidative Synthesis of Imides from Amides

A new protocol for the synthesis of imides has been developed. In the presence of copper catalyst, N‐benzylamides were oxidized to the corresponding imides by TBHP/TEMPO system in moderate to good yields.     

Graphene oxide as a sulfur immobilizer in high performance lithium/sulfur cells

The loss of sulfur cathode material as a result of polysulfide dissolution causes significant capacity fading in rechargeable lithium/sulfur cells. Here, we use a chemical approach to immobilize sulfur and lithium polysulfides via the reactive functional groups on graphene oxide. This approach enabled us to obtain a uniform and thin (around tens of nanometers) sulfur coating on graphene oxide sheets by a simple chemical reaction-deposition strategy and a subsequent low-temperature thermal treatment process. Strong interaction between graphene oxide and sulfur or polysulfides enabled us to demonstrate lithium/sulfur cells with a high reversible capacity of 950-1400 mA h g(-1), and stable cycling for more than 50 deep cycles at 0.1C (1C = 1675 mA g(-1)).     

用原位电镜技术研究银纳米线与硫溶液的液相反应机理

下窗口自对准的功能,而且可以实现在纳米级别控制液体层的厚度.利用该组液体芯片我们成功地观测了液态环境下Ag纳米线与S溶液的化学反应过程.实验结果表明,该反应过程不是简单的一步化合反应形成最终产物硫化银（Ag₂S）,而是在反应过程中先形成可溶解的中间产物多硫化银（Ag₂S₄）.这个中间产物会导致一小部分反应物Ag纳米线的溶解,而大部分Ag纳米线转变成Ag₂S纳米颗粒的聚集物.我们相信这一液体TEM芯片技术可以被广泛应用到液相环境下各种化学反应过程的研究.     

染料激光抽运Nd:YCOB自倍频激光器

Ｎｄ：ＹＣａ４Ｏ（ＢＯ３）３（简称Ｎｄ：ＹＣＯＢ）是一种新型自倍频激光复合功能晶体,利用Ｄａｔａｃｈｒｏｍ－５０００型染料激光器作为抽运源,横向抽运钕离子原子比为８％的Ｎｄ：ＹＣＯＢ获得了５３０．２ｎｍ绿色自倍频激光输出。在样品未镀膜的情况下阈值抽运量小于２ｍＪ,绿光输出能量最大为１．０３ｍＪ,能量转换效率约为３．３％。